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Aminated hydrophilic ordered mesoporous carbons
Abstract
This paper describes a single step procedure by which primary amine groups are anchored onto ordered mesoporous carbon in a one step reaction. Ordered carbon materials with functional groups residing at the pore surface are prepared using SBA-15 silica as template in combination with hydrothermal carbonisation at mild temperatures (180 °C). These functional groups are afterwards reacted with 3-chloropropylamine leading to amino-modified hexagonally ordered carbons. Transmission electron microscopy (TEM) and small angle X-ray scattering (SAXS) experiments proved that the resulting carbon materials exhibit hexagonal frameworks. Nitrogen adsorption revealed that the materials are micropore free, possessing narrow mesopores size distributions and high surface areas. The surface functionality and hydrophilicity of the carbonaceous materials were assessed by Fourier transform IR spectroscopy (FTIR), X-ray photoelectron analysis (XPS) and water porosimetry. The presence of accessible amino groups in considerable amounts was proved by elemental microanalysis, FTIR spectroscopy and thermogravimetrical analysis.
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Citations
Cites
Starbons: New Starch‐Derived Mesoporous Carbonaceous Materials with Tunable Properties
Budarin, V., Clark, J. H., Hardy, J. J. E., Luque, R., Milkowski, K., Tavener, S. J., & Wilson, A. J. (2006) · Angewandte Chemie · doi:10.1002/ange.200600460 · Cited by 255
Cited by
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Dai, L., Xue, Y., Qu, L., Choi, H.-J., & Baek, J.-B. (2015) · Chemical Reviews · doi:10.1021/cr5003563 · Cited by 2,380
Funke, A., & Ziegler, F. (2010) · Biofuels Bioproducts and Biorefining · doi:10.1002/bbb.198 · Cited by 2,001
Engineering carbon materials from the hydrothermal carbonization process of biomass
Hu, B., Wang, K., Wu, L., Yu, S., Antonietti, M., & Titirici, M. (2010) · Advanced Materials · doi:10.1002/adma.200902812 · Cited by 1,765
Self-citationDevelopment of biochar-based functional materials: toward a sustainable platform carbon material
Liu, W.-J., Jiang, H., & Yu, H.-Q. (2015) · Chemical Reviews · doi:10.1021/acs.chemrev.5b00195 · Cited by 1,754
Chemistry and materials options of sustainable carbon materials made by hydrothermal carbonization
Titirici, M.-M., & Antonietti, M. (2010) · Chem. Soc. Rev. · doi:10.1039/b819318p · Cited by 1,255
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Metadata
- Authors
- Titirici, M.-M., Thomas, A., & Antonietti, M.
- Venue
- Journal of Materials Chemistry
- Publisher
- Royal Society of Chemistry (RSC)
- Published
- 2007
- Volume
- 17
- Issue
- 32
- Pages
- 3412
- ISSN
- 0959-9428 (ISSN-L)
- 1364-5501
- OpenAlex
- W2015091109
- Cited by
- 177
- References
- 1
- FWCI
- 5.48
- Type
- journal article
- Language
- en
- Open access
- closed
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Contains information from the Semantic Scholar Academic Graph Datasets, made available under the ODC Attribution License (ODC-BY 1.0).
Semantic Scholar’s data is described in: Kinney, R., et al. (2023). The Semantic Scholar Open Data Platform. arXiv:2301.10140.
