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Preparation of graphene by a low-temperature thermal reduction at atmosphere pressure
Abstract
It is still a challenge to prepare graphene from graphene oxide (GO) under a mild thermal reduction. Here we report that GO can even be reduced at a low temperature (below 150 degrees C) at atmospheric pressure in a mixture of N,N-dimethylacetamide (DMAc) and water (10 : 3, v/v) under the protection of nitrogen gas. FT-IR, XRD, XPS, Raman, and AFM studies confirmed the thermal reduction of GO and the formation of graphene. The as-prepared graphene can be fully dispersed in pure DMAc to form an organic suspension, and the suspension is stable for at least two months at room temperature.
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Cited by
Pang, Y., Zhang, K., Yang, Z., Jiang, S., Ju, Z., Li, Y., Wang, X., Wang, D., Jian, M., Zhang, Y., et al. (2018) · ACS Nano · doi:10.1021/acsnano.7b07613 · Cited by 774
Synthesis and characterization of sulfophenyl-functionalized reduced graphene oxide sheets
Ossonon, B. D., & Bélanger, D. (2017) · RSC Advances · doi:10.1039/c6ra28311j · Cited by 496
The Chemistry of Graphene Oxide
Gao, W. (2015) · Graphene Oxide · doi:10.1007/978-3-319-15500-5_3 · Cited by 459
Supramolecular Hydrogel of Chitosan in the Presence of Graphene Oxide Nanosheets as 2D Cross-Linkers
Han, D., & Yan, L. (2014) · ACS Sustainable Chemistry & Engineering · doi:10.1021/sc400352a · Cited by 130
Self-citation
Metadata
- Authors
- Chen, W., & Yan, L.
- Venue
- Nanoscale
- Publisher
- Royal Society of Chemistry (RSC)
- Published
- 2010
- Volume
- 2
- Issue
- 4
- Pages
- 559
- ISSN
- 2040-3364 (ISSN-L)
- 2040-3372
- OpenAlex
- W2122840814
- Cited by
- 367
- References
- 0
- FWCI
- 10.35
- Type
- journal article
- Language
- en
- Open access
- closed
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