Development of homogeneous liquid–liquid extraction combined with dispersive liquid–liquid microextraction based on solidification of floating droplets of a ternary component deep eutectic solvent for the analysis of antibiotic residues in sausage samples prior to ion mobility spectrometry
Abstract
A combination of homogeneous liquid–liquid extraction and dispersive liquid–liquid microextraction based on solidification of a deep eutectic solvent is used for the extraction of 3 widely used antibiotics (oxytetracycline, penicillin G and tilmicosin) from sausage samples.
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For antibiotic residues (oxytetracycline, penicillin G, tilmicosin) in sausage (20 g), a DES-DLLME-SFOD method combined with HLLE using PChCl:dichloroacetic acid:dodecanoic acid (1:1:1) as extractant and acetonitrile as disperser achieved enrichment factors of 1260-1580 and LODs of 0.00152-0.00273 μg/g with RSD <8% [50].
“| IMS | Antibiotic residues (oxytetracycline, penicillin G, tilmicosin) | HLLE | Sausage (20 g) | PChCl: dichloroacetic acid: dodecanoic acid (1:1:1), (70 µL) | Acetonitrile (2 mL) | 1260-1580 | 0.00152-0.00273 µg/g | <8 | [50] |”
A homogeneous LLE (HLLE) technique was combined with DES-DLLME-SFOD for the extraction of three antibiotics (oxytetracycline, penicillin G, and tilmicosin) from sausage samples [50].
“A homogeneous LLE (HLLE) technique was combined with DES-DLLME-SFOD for the extraction of three antibiotics (oxytetracycline, penicillin G, and tilmicosin) from sausage samples [50].”
The method showed low LOD, in the ranges of 1.52-2.73ng/g, demonstrating an %RSD of less than 8%.
“The method showed low LOD, in the ranges of 1.52-2.73ng/g, demonstrating an %RSD of less than 8%.”
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“The DESs that consisted of either quaternary ammonium or phosphonium salts (as HBA) with straight-chain monobasic acids or alcohols (as HBD) were found to be useful in applications determining aromatic amines from water [49], antibiotic residue from sausage [50], pesticides from tomato juice [51], antibiotic residues…”
BackgroundMethodKolawole, O., Thammakhet-Buranachai, C., Petchkongkaew, A., Sooksimuang, T., Elliott, C., & Karoonuthaisiri, N. (2024) · Green Chemistry Letters and Reviews · doi:10.1080/17518253.2024.2427797 · Cited by 10 · see citing works
- Authors
- Saei, A., Javadi, A., Afshar Mogaddam, M. R., Mirzaei, H., & Nemati, M.
- Affiliations
- Islamic Azad University, Tehran (IR)
- Food and Drug Safety Research Center
- Tabriz University of Medical Sciences (IR)
- Corresponding author
- Javadi, Afshin
- Venue
- Analytical Methods
- Publisher
- Royal Society of Chemistry (RSC)
- Published
- 2020
- Volume
- 12
- Issue
- 34
- Pages
- 4220-4228
- ISSN
- 1759-9660 (ISSN-L)
- 1759-9679
- OpenAlex
- W3043124049
- Cited by
- 24
- References
- 33
- Citations by year
- 2026: 4 · 2025: 6 · 2024: 1 · 2023: 5 · 2022: 3 · 2021: 5
- FWCI
- 1.68
- Type
- journal article
- Language
- en
- Open access
- closed
- Locations
- Analytical Methods (publishedVersion)
- PubMed (publishedVersion)
- Funders
- Tabriz University of Medical Sciences
- Islamic Azad University, Tabriz Branch
- Topics
- Physical Sciences › Chemistry › Analytical Chemistry › Analytical chemistry methods development
- Life Sciences › Agricultural and Biological Sciences › Food Science › Pesticide Residue Analysis and Safety
- Physical Sciences › Chemical Engineering › Catalysis › Ionic liquids properties and applications
- Keywords
- homogeneous liquid-liquid extraction, dispersive liquid-liquid microextraction, deep eutectic solvents, ternary deep eutectic solvents, antibiotic residues, sausage, oxytetracycline, ion mobility spectrometry
- MeSH terms
- Ion Mobility Spectrometry, Anti-Bacterial Agents, Iran, Solvents, Liquid-Liquid Extraction, Liquid Phase Microextraction
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