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The Effect of Cold-Work Distortion on X-Ray Patterns
Abstract
With modern experimental technique, it is possible to measure a peak shape with sufficient accuracy to justify an interpretation based on the precise shape of the reflection. The corrected shape is represented by a cosine Fourier series and a set of An coefficients determined. A plot of the An coefficients vs. n will distinguish between distortion and particle size broadening. From the An coefficients, root mean square values of strain averaged over lengths na3 are obtained. The decrease in these values for increasing length na3 is a direct indication of the non-uniform nature of the strains in cold-worked metal. By measuring several orders of a given plane, it is theoretically possible to obtain a distribution function of the strains directly from a Fourier transform of the An coefficients.
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Cited by
Ordered mesoporous α-MoO3 with iso-oriented nanocrystalline walls for thin-film pseudocapacitors
Brezesinski, T., Wang, J., Tolbert, S. H., & Dunn, B. (2010) · Nature Materials · doi:10.1038/nmat2612 · Cited by 3,359
Delhez, R., de Keijser, T. H., & Mittemeijer, E. J. (1982) · Fresenius' Zeitschrift für analytische Chemie · doi:10.1007/bf00482725 · Cited by 420
Koch, F. P. V., Rivnay, J., Foster, S., Müller, C., Downing, J. M., Buchaca-Domingo, E., Westacott, P., Yu, L., Yuan, M., Baklar, M., et al. (2013) · Progress in Polymer Science · doi:10.1016/j.progpolymsci.2013.07.009 · Cited by 337
Pitfalls in the characterization of nanoporous and nanosized materials
Weidenthaler, C. (2011) · Nanoscale · doi:10.1039/c0nr00561d · Cited by 256
Ascarelli, P., Contini, V., & Giorgi, R. (2002) · Journal of Applied Physics · doi:10.1063/1.1453495 · Cited by 63
Metadata
- Authors
- Warren, B. E., & Averbach, B. L.
- Venue
- Journal of Applied Physics
- Publisher
- AIP Publishing
- Published
- 1950-06-01
- Volume
- 21
- Issue
- 6
- Pages
- 595-599
- ISSN
- 0021-8979 (ISSN-L)
- 1089-7550
- OpenAlex
- W1997652591
- Cited by
- 1,406
- References
- 0
- FWCI
- 12.08
- Type
- journal article
- Language
- en
- Open access
- closed
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