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Sideband intensities in NMR spectra of samples spinning at the magic angle
Abstract
General integral and series expressions are derived for the intensities of sidebands observed in the magic angle spectra of inhomogeneously broadened I=1/2 systems. The expressions are evaluated for a wide range of shift parameters and the results used to construct graphical and numerical methods for extracting the principal values of chemical shift tensors from the intensities of just a few sidebands. The methods are illustrated by application to 31P spectra of barium diethyl phosphate. The results agree well with previous single crystal measurements.
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Cited by
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Koller, H., Wölker, A., Villaescusa, L. A., Díaz-Cabañas, M. J., Valencia, S., & Camblor, M. A. (1999) · Journal of the American Chemical Society · doi:10.1021/ja9840549 · Cited by 208
Stumber, M., Geyer, M., Graf, R., Robert Kalbitzer, H., Scheffzek, K., & Haeberlen, U. (2002) · Journal of Molecular Biology · doi:10.1016/s0022-2836(02)01010-0 · Cited by 22
Metadata
- Authors
- Herzfeld, J., & Berger, A. E.
- Venue
- The Journal of Chemical Physics
- Publisher
- AIP Publishing
- Published
- 1980-12-15
- Volume
- 73
- Issue
- 12
- Pages
- 6021-6030
- ISSN
- 0021-9606 (ISSN-L)
- 1089-7690
- OpenAlex
- W1966235885
- Cited by
- 1,585
- References
- 0
- FWCI
- 7.15
- Type
- journal article
- Language
- en
- Open access
- closed
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- CoChat. (2026). Citation check: Sideband intensities in NMR spectra of samples spinning at the magic angle. https://app.cochat.ai/papers/10.1063/1.440136
- The paper
- Herzfeld, J., & Berger, A. E. (1980). Sideband intensities in NMR spectra of samples spinning at the magic angle. The Journal of Chemical Physics. https://doi.org/10.1063/1.440136
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Bibliographic data: Semantic Scholar, OpenAlex, Crossref.
Contains information from the Semantic Scholar Academic Graph Datasets, made available under the ODC Attribution License (ODC-BY 1.0).
Semantic Scholar’s data is described in: Kinney, R., et al. (2023). The Semantic Scholar Open Data Platform. arXiv:2301.10140.
