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Chemical shift correlation spectroscopy in rotating solids: Radio frequency-driven dipolar recoupling and longitudinal exchange
Abstract
We present a new method of performing chemical shift correlation spectroscopy in solids with magic angle spinning (MAS). Its key feature is a longitudinal mixing period of π pulses that recouples the dipolar interaction. We discuss experimental results for triply-13C-labeled alanine and a theory combining MAS and π pulses.
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Cited by
Magnetically-oriented phospholipid micelles as a tool for the study of membrane-associated molecules
Sanders, C. R., Hare, B. J., Howard, K. P., & Prestegard, J. H. (1994) · Progress in Nuclear Magnetic Resonance Spectroscopy · doi:10.1016/0079-6565(94)80012-x · Cited by 420
Homonuclear radio frequency-driven recoupling in rotating solids
Bennett, A. E., Rienstra, C. M., Griffiths, J. M., Zhen, W., Lansbury, P. T., & Griffin, R. G. (1998) · The Journal of Chemical Physics · doi:10.1063/1.476420 · Cited by 353
Self-citationHou, G., Yan, S., Trébosc, J., Amoureux, J.-P., & Polenova, T. (2013) · Journal of Magnetic Resonance · doi:10.1016/j.jmr.2013.04.009 · Cited by 193
Dickwella Widanage, M. C., Singh, K., Li, J., Yarava, J. R., Scott, F. J., Xu, Y., Gow, N. A. R., Mentink-Vigier, F., Wang, P., Lamoth, F., et al. (2025) · Nature Communications · doi:10.1038/s41467-025-61678-1 · Cited by 51
Bahri, S., Safeer, A., Adler, A., Smedes, H., van Ingen, H., & Baldus, M. (2023) · Journal of Biomolecular NMR · doi:10.1007/s10858-023-00415-6 · Cited by 31
Metadata
- Authors
- Bennett, A. E., Griffin, R. G., Ok, J. H., & Vega, S.
- Venue
- The Journal of Chemical Physics
- Publisher
- AIP Publishing
- Published
- 1992-06-01
- Volume
- 96
- Issue
- 11
- Pages
- 8624-8627
- ISSN
- 0021-9606 (ISSN-L)
- 1089-7690
- OpenAlex
- W1968779811
- Cited by
- 671
- References
- 0
- FWCI
- 15.05
- Type
- journal article
- Language
- en
- Open access
- closed
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- Bennett, A. E., Griffin, R. G., Ok, J. H., & Vega, S. (1992). Chemical shift correlation spectroscopy in rotating solids: Radio frequency-driven dipolar recoupling and longitudinal exchange. The Journal of Chemical Physics. https://doi.org/10.1063/1.462267
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Contains information from the Semantic Scholar Academic Graph Datasets, made available under the ODC Attribution License (ODC-BY 1.0).
Semantic Scholar’s data is described in: Kinney, R., et al. (2023). The Semantic Scholar Open Data Platform. arXiv:2301.10140.
