The DOI matches its Crossref record; 10 of the 10 references it cites were found in a registry or an index.
Double-quantum homonuclear rotary resonance: Efficient dipolar recovery in magic-angle spinning nuclear magnetic resonance
Abstract
We describe an efficient method for the recovery of homonuclear dipole–dipole interactions in magic-angle spinning NMR. Double-quantum homonuclear rotary resonance (2Q-HORROR) is established by fulfilling the condition ωr=2ω1, where ωr is the sample rotation frequency and ω1 is the nutation frequency around an applied resonant radio frequency (rf) field. This resonance can be used for double-quantum filtering and measurement of homonuclear dipolar interactions in the presence of magic-angle spinning. The spin dynamics depend only weakly on crystallite orientation allowing good performance for powder samples. Chemical shift effects are suppressed to zeroth order. The method is demonstrated for singly and doubly 13C labeled L-alanine.
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Citations
Cites
NMR Basic principles and progress
Bothner, A. A. (1973) · Journal of Magnetic Resonance (1969) · doi:10.1016/0022-2364(73)90052-8 · Cited by 2,051
Coherent Averaging Effects in Magnetic Resonance
Haeberlen, U., & Waugh, J. S. (1968) · Physical Review · doi:10.1103/physrev.175.453 · Cited by 1,083
Selection of coherence-transfer pathways in NMR pulse experiments
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Natural abundance carbon-13-carbon-13 coupling observed via double-quantum coherence
Bax, A., Freeman, R., & Kempsell, S. P. (1980) · Journal of the American Chemical Society · doi:10.1021/ja00534a056 · Cited by 745
Oas, T. G., Griffin, R. G., & Levitt, M. H. (1988) · The Journal of Chemical Physics · doi:10.1063/1.455191 · Cited by 408
Self-citationSelective detection of multiple quantum transitions in NMR by two-dimensional spectroscopy
Wokaun, A., & Ernst, R. R. (1977) · Chemical Physics Letters · doi:10.1016/0009-2614(77)80476-4 · Cited by 379
Determination of Membrane Protein Structure by Rotational Resonance NMR: Bacteriorhodopsin
Creuzet, F., McDermott, A., Gebhard, R., van der Hoef, K., Spijker-Assink, M. B., Herzfeld, J., Lugtenburg, J., Levitt, M. H., & Griffin, R. G. (1991) · Science · doi:10.1126/science.1990439 · Cited by 245
Self-citationResonant rotational broadening of nuclear magnetic resonance spectra
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Pseudo-spin rotational resonance and homonuclear dipolar N.M.R. of rotating solids
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Cited by
Structure of a protein determined by solid-state magic-angle-spinning NMR spectroscopy
Castellani, F., van Rossum, B., Diehl, A., Schubert, M., Rehbein, K., & Oschkinat, H. (2002) · Nature · doi:10.1038/nature01070 · Cited by 910
Investigation of Molecular Motions by Lee-Goldburg Cross-Polarization NMR Spectroscopy
Hong, M., Yao, X., Jakes, K., & Huster, D. (2002) · The Journal of Physical Chemistry B · doi:10.1021/jp0156064 · Cited by 137
Metadata
- Authors
- Nielsen, N. C., Bildso/e, H., Jakobsen, H. J., & Levitt, M. H.
- Venue
- The Journal of Chemical Physics
- Publisher
- AIP Publishing
- Published
- 1994-08-01
- Volume
- 101
- Issue
- 3
- Pages
- 1805-1812
- ISSN
- 0021-9606 (ISSN-L)
- 1089-7690
- OpenAlex
- W2009048792
- Cited by
- 450
- References
- 10
- FWCI
- 5.81
- Type
- journal article
- Language
- en
- Open access
- closed
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- Nielsen, N. C., Bildso/e, H., Jakobsen, H. J., & Levitt, M. H. (1994). Double-quantum homonuclear rotary resonance: Efficient dipolar recovery in magic-angle spinning nuclear magnetic resonance. The Journal of Chemical Physics. https://doi.org/10.1063/1.467759
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Bibliographic data: Semantic Scholar, OpenAlex, Crossref.
Contains information from the Semantic Scholar Academic Graph Datasets, made available under the ODC Attribution License (ODC-BY 1.0).
Semantic Scholar’s data is described in: Kinney, R., et al. (2023). The Semantic Scholar Open Data Platform. arXiv:2301.10140.
