The DOI matches its Crossref record; 9 of the 9 references it cites were found in a registry or an index.
Rotary resonance recoupling of dipolar interactions in solid-state nuclear magnetic resonance spectroscopy
Abstract
A new resonance effect in solid-state nuclear magnetic resonance (NMR) is described. The effect involves a combination of magic-angle sample rotation with irradiation of a heteronuclear spin system at the Larmor frequency of one of the spin species. If the irradiation intensity is such as to establish a match between spin nutation and sample rotation, it is shown that the heteronuclear dipolar spin interaction is selectively reintroduced into the spectrum. This allows small dipolar coupling constants to be measured in the presence of large shielding anisotropies. Applications are anticipated for determination of internuclear distances in materials lacking long-range order, such as polycrystalline materials, polymers, and surfaces.
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Citations
Cites
The Principles of Nuclear Magnetism
Abragam, A., & Hebel, L. C. (1961) · American Journal of Physics · doi:10.1119/1.1937646 · Cited by 15,792
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Nuclear Magnetic Resonance Spectra from a Crystal rotated at High Speed
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Coherent Averaging Effects in Magnetic Resonance
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Nuclear Magnetic Resonance Saturation and Rotary Saturation in Solids
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Self-citationSolvent peak saturation with single phase and quadrature fourier transformation
Hoult, D. I. (1976) · Journal of Magnetic Resonance (1969) · doi:10.1016/0022-2364(76)90081-0 · Cited by 226
Theory of broadband spin decoupling
Waugh, J. S. (1982) · Journal of Magnetic Resonance (1969) · doi:10.1016/0022-2364(82)90029-4 · Cited by 181
Resonant rotational broadening of nuclear magnetic resonance spectra
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Cited by
– dipolar-assisted rotational resonance in magic-angle spinning NMR
Takegoshi, K., Nakamura, S., & Terao, T. (2001) · Chemical Physics Letters · doi:10.1016/s0009-2614(01)00791-6 · Cited by 1,012
Nielsen, N. C., Bildso/e, H., Jakobsen, H. J., & Levitt, M. H. (1994) · The Journal of Chemical Physics · doi:10.1063/1.467759 · Cited by 450
Self-citationSchanda, P., & Ernst, M. (2016) · Progress in Nuclear Magnetic Resonance Spectroscopy · doi:10.1016/j.pnmrs.2016.02.001 · Cited by 264
Molecular conformation of a peptide fragment of transthyretin in an amyloid fibril
Jaroniec, C. P., MacPhee, C. E., Astrof, N. S., Dobson, C. M., & Griffin, R. G. (2002) · Proceedings of the National Academy of Sciences · doi:10.1073/pnas.252625999 · Cited by 253
Self-citationFive-Coordinate Silicon in High-Silica Zeolites
Koller, H., Wölker, A., Villaescusa, L. A., Díaz-Cabañas, M. J., Valencia, S., & Camblor, M. A. (1999) · Journal of the American Chemical Society · doi:10.1021/ja9840549 · Cited by 208
Metadata
- Authors
- Oas, T. G., Griffin, R. G., & Levitt, M. H.
- Venue
- The Journal of Chemical Physics
- Publisher
- AIP Publishing
- Published
- 1988-07-15
- Volume
- 89
- Issue
- 2
- Pages
- 692-695
- ISSN
- 0021-9606 (ISSN-L)
- 1089-7690
- OpenAlex
- W2024832918
- Cited by
- 408
- References
- 9
- FWCI
- 4.60
- Type
- journal article
- Language
- en
- Open access
- closed
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- Oas, T. G., Griffin, R. G., & Levitt, M. H. (1988). Rotary resonance recoupling of dipolar interactions in solid-state nuclear magnetic resonance spectroscopy. The Journal of Chemical Physics. https://doi.org/10.1063/1.455191
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Contains information from the Semantic Scholar Academic Graph Datasets, made available under the ODC Attribution License (ODC-BY 1.0).
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