Nuclear magnetic resonance measurements in dynamically controlled field pulse
Open accessAbstract
We present the architecture of the versatile nuclear magnetic resonance (NMR) spectrometer with software-defined radio technology and its application to the dynamically controlled pulsed magnetic fields. The pulse-field technology is the only solution to access magnetic fields greater than 50 T, but the NMR experiment in the pulsed magnetic field was difficult because of the continuously changing field strength. The dynamically controlled field pulse allows us to perform NMR experiment in a quasi-steady field condition by creating a constant magnetic field for a short time around the peak of the field pulse. We confirmed the reproducibility of the field pulses using the NMR spectroscopy as a high precision magnetometer. With the highly reproducible field strength, we succeeded in measuring the nuclear spin-lattice relaxation rate 1/T1, which had never been measured by the pulse-field NMR experiment without dynamic field control. We also implement the NMR spectrum measurement with both the frequency-sweep and field-sweep modes and discuss the appropriate choices of these modes depending on the magnetic properties of the sample to be measured. This development, with further improvement at a long-duration field pulse, will innovate the microscopic measurement in extremely high magnetic fields.
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The feedback-controlled flat-top pulse has enabled measurement of a variety of physical quantities under high magnetic fields such as specific heat, NMR, and current-voltage characteristics.
“The feedback-controlled flat-top pulse has enabled us to measure a variety of physical quantities under high magnetic fields such as specific heat, 21,25,26 nuclear magnetic resonance (NMR), 22,24 current-voltage characteristic, 23 etc.”
From Simultaneous measurement of specific heat and thermal conductivity in pulsed magnetic fields (2023) · cites this paper as [22]
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Research works printed but not linked: 5
- 5 J. R. Miller, IEEE Transactions on Applied Superconductivity 13 , 1385 (2003).
- 6 P. Pugnat, R. Barbier, C. Berriaud, R. Berthier, T. Boujet, F. Debray, P. Fazilleau, P. Graffin, P. Hanoux, B. Hervieu, F. Molinié, H. Neyrial, M. Pelloux, C. Peroni, R. Pfister, Y. Queinec, L. Ronayette, B. Vincent, IEEE Transactions on Applied Superconductivity 28 , 4300907 (2017).
- 8 S. Awaji, K. Watanabe, H. Oguro, S. Hanai, H. Miyazaki, M. Takahashi, S. Ioka, M. Sugimoto, H. Tsubouchi, S. Fujita, M. Daibo, Y. Iijima, H. Kumakura, IEEE Transactions on Applied Superconductivity 24 , 4302005 (2013).
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- 19 Y. Kohama, K. Kindo, Review of Scientific Instruments 86 , 104701 (2015).
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Simultaneous measurement of specific heat and thermal conductivity in pulsed magnetic fields
Nomoto, T., Zhong, C., Kageyama, H., Suzuki, Y., Jaime, M., Hashimoto, Y., Katsumoto, S., Matsuyama, N., Dong, C., Matsuo, A., et al. (2023) · arXiv · doi:10.48550/arxiv.2302.01627 · Cited by 5 · see citing works
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- Authors
- Ihara, Y., Hayashi, K., Kanda, T., Matsui, K., Kindo, K., & Kohama, Y.
- Affiliations
- Hokkaido University (JP)
- The Institute for Solid State Physics, The University of Tokyo (JP)
- Corresponding author
- Ihara, Y.
- Venue
- Review of Scientific Instruments
- Publisher
- AIP Publishing
- Published
- 2021-11-01
- Volume
- 92
- Issue
- 11
- Pages
- 114709-114709
- ISSN
- 0034-6748 (ISSN-L)
- 1089-7623
- OpenAlex
- W3213476153
- Cited by
- 19
- References
- 0
- Citations by year
- 2026: 2 · 2025: 6 · 2024: 2 · 2023: 5 · 2022: 4
- FWCI
- 1.00
- Type
- journal article
- Language
- en
- Open access
- green
- arxiv.org
- Locations
- Review of Scientific Instruments (publishedVersion)
- PubMed (publishedVersion)
- arXiv (Cornell University) (submittedVersion)
- Institutional Repositories DataBase (IRDB) (submittedVersion)
- Hokkaido University Collection of Scholarly and Academic Papers (Hokkaido University) (submittedVersion)
- arXiv (Cornell University)
- Funders
- Japan Society for the Promotion of Science (18H01163, 19H01832, 20K20892, 19K14648)
- Futaba Foundation
- ISSP Institutional Collaborative Research Program
- Quantum Science and Technology Fellowship Program
- Topics
- Physical Sciences › Chemistry › Spectroscopy › Advanced NMR Techniques and Applications
- Physical Sciences › Physics and Astronomy › Nuclear and High Energy Physics › NMR spectroscopy and applications
- Physical Sciences › Physics and Astronomy › Atomic and Molecular Physics, and Optics › Atomic and Subatomic Physics Research
- Keywords
- pulsed magnetic field, NMR spectrometer, software-defined radio, spin-lattice relaxation rate
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