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Broadband homonuclear cross polarization in 2D N.M.R. using DIPSI-2
Abstract
We discuss broadband homonuclear cross polarization of J-coupled spin systems in liquids, and compare a new windowless sequence, called DIPSI-2, to the broadband spin decoupling sequences MLEV-16 and WALTZ-16. We find that DISPI-2 leads to more rapid and complete cross polarization for a given expenditure of radiofrequency power. Either longitudinal or transverse magnetization components can be exchanged by DIPSI-2. Using DIPSI-2 as a mixing sequence to induce longitudinal magnetization transfer can give absorption-mode 2D correlation spectra with a minimum of phase cycling steps.
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Cited by
Bax, A., Clore, G. M., & Gronenborn, A. M. (1990) · Journal of Magnetic Resonance (1969) · doi:10.1016/0022-2364(90)90202-k · Cited by 584
Pantarotto, D., Partidos, C. D., Hoebeke, J., Brown, F., Kramer, E., Briand, J.-P., Muller, S., Prato, M., & Bianco, A. (2003) · Chemistry & Biology · doi:10.1016/j.chembiol.2003.09.011 · Cited by 538
Discovery of Potent Nonpeptide Inhibitors of Stromelysin Using SAR by NMR
Hajduk, P. J., Sheppard, G., Nettesheim, D. G., Olejniczak, E. T., Shuker, S. B., Meadows, R. P., Steinman, D. H., Carrera, G. M., Marcotte, P. A., Severin, J., et al. (1997) · Journal of the American Chemical Society · doi:10.1021/ja9702778 · Cited by 317
Jenkins, M. A., Wells, G., Bachman, J., Snyder, J. P., Jenkins, A., Huganir, R. L., Oswald, R. E., & Traynelis, S. F. (2014) · Molecular Pharmacology · doi:10.1124/mol.113.091488 · Cited by 30
NMR as a readout to monitor and restore the integrity of complex chemoenzymatic reactions
Marincin, K. A., Hwang, Y., Kengmana, E. S., Meyers, D. J., & Frueh, D. P. (2022) · Journal of Magnetic Resonance · doi:10.1016/j.jmr.2022.107265
Metadata
- Authors
- Rucker, S. P., & Shaka, A. J.
- Venue
- Molecular Physics
- Publisher
- Informa UK Limited
- Published
- 1989-10-10
- Volume
- 68
- Issue
- 2
- Pages
- 509-517
- ISSN
- 0026-8976 (ISSN-L)
- 1362-3028
- OpenAlex
- W2006731694
- Cited by
- 286
- References
- 0
- FWCI
- 8.11
- Type
- journal article
- Language
- en
- Open access
- closed
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- Rucker, S. P., & Shaka, A. J. (1989). Broadband homonuclear cross polarization in 2D N.M.R. using DIPSI-2. Molecular Physics. https://doi.org/10.1080/00268978900102331
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