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High-Rate, Gas-Phase Growth of MoS 2 Nested Inorganic Fullerenes and Nanotubes
Abstract
The gas-phase reaction between MoO 3- x and H 2 S in a reducing atmosphere at elevated temperatures (800° to 950°C) has been used to synthesize large quantities of an almost pure nested inorganic fullerene (IF) phase of MoS 2 . A uniform IF phase with a relatively narrow size distribution was obtained. The synthesis of IFs appears to require, in addition to careful control over the growth conditions, a specific turbulent flow regime. The x-ray spectra of the different samples show that, as the average size of the IF decreases, the van der Waals gap along the c axis increases, largely because of the strain involved in folding of the lamella. Large quantities of quite uniform nanotubes were obtained under modified preparation conditions.
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Citations
Cited by
Synthesis of Large‐Area MoS2 Atomic Layers with Chemical Vapor Deposition
Lee, Y., Zhang, X., Zhang, W., Chang, M., Lin, C., Chang, K., Yu, Y., Wang, J. T., Chang, C., Li, L., et al. (2012) · Advanced Materials · doi:10.1002/adma.201104798 · Cited by 3,422
Synthesis of MoS 2 and MoSe 2 Films with Vertically Aligned Layers
Kong, D., Wang, H., Cha, J. J., Pasta, M., Koski, K. J., Yao, J., & Cui, Y. (2013) · Nano Letters · doi:10.1021/nl400258t · Cited by 2,250
Controlled Synthesis of Highly Crystalline MoS 2 Flakes by Chemical Vapor Deposition
Wang, X., Feng, H., Wu, Y., & Jiao, L. (2013) · Journal of the American Chemical Society · doi:10.1021/ja4013485 · Cited by 748
Samadi, M., Sarikhani, N., Zirak, M., Zhang, H., Zhang, H.-L., & Moshfegh, A. Z. (2018) · Nanoscale Horizons · doi:10.1039/c7nh00137a · Cited by 408
Ma, C.-B., Qi, X., Chen, B., Bao, S., Yin, Z., Wu, X.-J., Luo, Z., Wei, J., Zhang, H.-L., & Zhang, H. (2014) · Nanoscale · doi:10.1039/c3nr04975b · Cited by 331
Metadata
- Authors
- Feldman, Y., Wasserman, E., Srolovitz, D. J., & Tenne, R.
- Venue
- Science
- Published
- 1995-01-13
- Volume
- 267
- Issue
- 5195
- Pages
- 222-225
- ISSN
- 0036-8075 (ISSN-L)
- 1095-9203
- OpenAlex
- W2052471006
- Cited by
- 1,214
- References
- 0
- FWCI
- 16.87
- Type
- journal article
- Language
- en
- Open access
- closed
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- Feldman, Y., Wasserman, E., Srolovitz, D. J., & Tenne, R. (1995). High-Rate, Gas-Phase Growth of MoS 2 Nested Inorganic Fullerenes and Nanotubes. Science. https://doi.org/10.1126/science.267.5195.222
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Contains information from the Semantic Scholar Academic Graph Datasets, made available under the ODC Attribution License (ODC-BY 1.0).
Semantic Scholar’s data is described in: Kinney, R., et al. (2023). The Semantic Scholar Open Data Platform. arXiv:2301.10140.
