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Mesostructure Design with Gemini Surfactants: Supercage Formation in a Three-Dimensional Hexagonal Array
Abstract
At low temperatures, liquid crystal-like arrays made up of inorganic-cluster and organic molecular units readily undergo reversible lyotropic transformations. Gemini surfactants, with two quaternary ammonium head groups separated by a methylene chain of variable length and with each head group attached to a hydrophobic tail, can be used to control organic charge sitting relative to the bivariable hydrophobic tail configurations. This approach has led to the synthesis of a mesophase (SBA-2) that has three-dimensional hexagonal ( P 6 3 / mmc ) symmetry, regular supercages that can be dimensionally tailored, and a large inner surface area. This mesostructure analog of a zeolite cage structure does not appear to have a lyotropic surfactant or lipid liquid crystal mesophase counterpart. Through the modification of gemini charge separation and each of the two organic tails, these syntheses can be used to optimize templating effects, including the synthesis of MCM-48 at room temperature.
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Sing, K. S. W. (1985) · Pure and Applied Chemistry · doi:10.1351/pac198557040603 · Cited by 24,485
Cited by
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Ordered mesoporous materials in catalysis
Taguchi, A., & Schüth, F. (2005) · Microporous and Mesoporous Materials · doi:10.1016/j.micromeso.2004.06.030 · Cited by 2,119
Ciesla, U., & Schüth, F. (1999) · Microporous and Mesoporous Materials · doi:10.1016/s1387-1811(98)00249-2 · Cited by 1,084
Block copolymer based nanostructures: Materials, processes, and applications to electronics
Kim, H.-C., Park, S.-M., & Hinsberg, W. D. (2010) · Chemical Reviews · doi:10.1021/cr900159v · Cited by 1,017
Hierarchically Structured Zeolites: From Design to Application
Chen, L.-H., Sun, M.-H., Wang, Z., Yang, W., Xie, Z., & Su, B.-L. (2020) · Chemical Reviews · doi:10.1021/acs.chemrev.0c00016 · Cited by 724
Metadata
- Authors
- Huo, Q., Leon, R., Petroff, P. M., & Stucky, G. D.
- Venue
- Science
- Published
- 1995-06-02
- Volume
- 268
- Issue
- 5215
- Pages
- 1324-1327
- ISSN
- 0036-8075 (ISSN-L)
- 1095-9203
- OpenAlex
- W2006991115
- Cited by
- 719
- References
- 1
- FWCI
- 27.13
- Type
- journal article
- Language
- en
- Open access
- closed
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- Huo, Q., Leon, R., Petroff, P. M., & Stucky, G. D. (1995). Mesostructure Design with Gemini Surfactants: Supercage Formation in a Three-Dimensional Hexagonal Array. Science. https://doi.org/10.1126/science.268.5215.1324
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Contains information from the Semantic Scholar Academic Graph Datasets, made available under the ODC Attribution License (ODC-BY 1.0).
Semantic Scholar’s data is described in: Kinney, R., et al. (2023). The Semantic Scholar Open Data Platform. arXiv:2301.10140.
