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Mechanism of Zeolite A Nanocrystal Growth from Colloids at Room Temperature
Abstract
The formation and growth of crystal nuclei of zeolite A from clear solutions at room temperature were studied with low-dose, high-resolution transmission electron microscopy in field emission mode and with in situ dynamic light scattering. Single zeolite A crystals nucleated in amorphous gel particles of 40 to 80 nanometers within 3 days at room temperature. The resulting nanoscale single crystals (10 to 30 nanometers) were embedded in the amorphous gel particles. The gel particles were consumed during further crystal growth at room temperature, forming a colloidal suspension of zeolite A nanocrystals of 40 to 80 nanometers. On heating this suspension at 80°C, solution-mediated transport resulted in additional substantial crystal growth.
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Cited by
The hydrothermal synthesis of zeolites: Precursors, intermediates and reaction mechanism
Cundy, C. S., & Cox, P. A. (2005) · Microporous and Mesoporous Materials · doi:10.1016/j.micromeso.2005.02.016 · Cited by 1,590
Size dependence of nanostructures: Impact of bond order deficiency
Sun, C. Q. (2007) · Progress in Solid State Chemistry · doi:10.1016/j.progsolidstchem.2006.03.001 · Cited by 873
Hierarchically Structured Zeolites: From Design to Application
Chen, L.-H., Sun, M.-H., Wang, Z., Yang, W., Xie, Z., & Su, B.-L. (2020) · Chemical Reviews · doi:10.1021/acs.chemrev.0c00016 · Cited by 724
New Stories of Zeolite Structures: Their Descriptions, Determinations, Predictions, and Evaluations
Li, Y., & Yu, J. (2014) · Chemical Reviews · doi:10.1021/cr500010r · Cited by 603
Zhang, Z., Wang, H., Provis, J. L., Bullen, F., Reid, A., & Zhu, Y. (2012) · Thermochimica Acta · doi:10.1016/j.tca.2012.03.021 · Cited by 494
Metadata
- Authors
- Mintova, S., Olson, N. H., Valtchev, V., & Bein, T.
- Venue
- Science
- Published
- 1999-02-12
- Volume
- 283
- Issue
- 5404
- Pages
- 958-960
- ISSN
- 0036-8075 (ISSN-L)
- 1095-9203
- OpenAlex
- W2035176265
- Cited by
- 649
- References
- 0
- FWCI
- 13.81
- Type
- journal article
- Language
- en
- Open access
- closed
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- Mintova, S., Olson, N. H., Valtchev, V., & Bein, T. (1999). Mechanism of Zeolite A Nanocrystal Growth from Colloids at Room Temperature. Science. https://doi.org/10.1126/science.283.5404.958
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Contains information from the Semantic Scholar Academic Graph Datasets, made available under the ODC Attribution License (ODC-BY 1.0).
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