The hydrothermal synthesis of zeolites: Precursors, intermediates and reaction mechanism
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The interaction between BAS zeolites and water governs the synthesis of zeolites from precursor gels containing silica fragments, water and cations.
“(iv) the synthesis of zeolites from precursor gels containing silica fragments, water and cations11”
From A reactive neural network framework for water-loaded acidic zeolites (2024) · cites this paper as [11]
The way in which OSDAs favor the crystallization of a specific structure is not yet fully understood, despite the large research effort put into it.
“The way in which these OSDAs favor the crystallization of a specific structure is not yet fully understood, despite the large research effort put into it.46,47,95,96”
From Zeolites in Adsorption Processes: State of the Art and Future Prospects (2022) · cites this paper as [96]
The mineralizing agent intervenes directly in the breaking and formation of T-O-T bonds and helps to establish a dynamic equilibrium that ends in the formation of the zeolite.
“The mineralizing agent intervenes directly in the breaking and formation of T–O–T bonds and helps to establish a dynamic equilibrium that ends in the formation of the zeolite.96,112”
From Zeolites in Adsorption Processes: State of the Art and Future Prospects (2022) · cites this paper as [96]
When seeds are preserved, they promote crystallization of their same structure because nucleation is skipped and crystals can start to grow immediately.
“When preserved, the seeds promote the crystallization of their same structure, as the nucleation step is skipped and the crystals can start to grow immediately.96”
From Zeolites in Adsorption Processes: State of the Art and Future Prospects (2022) · cites this paper as [96]
Higher crystallization temperatures and longer crystallization times favor the obtention of more dense, usually more stable phases instead of more open phases.
“Higher temperatures and longer crystallization times favor the obtention of more dense, usually more stable phases instead of more open phases.”
From Zeolites in Adsorption Processes: State of the Art and Future Prospects (2022) · cites this paper as [96]
Aging of the gel at lower temperature prior to the hydrothermal process and stirring/rotation speed during crystallization have a remarkable influence on the product obtained.
“Other synthesis parameters that have a remarkable influence on the product obtained are aging of the gel at lower temperature prior to the hydrothermal process and stirring/rotation speed during the crystallization.96,112”
From Zeolites in Adsorption Processes: State of the Art and Future Prospects (2022) · cites this paper as [96]
Cites
Zones, S. I. (1991) · Journal of the Chemical Society, Faraday Transactions · doi:10.1039/ft9918703709 · Cited by 219 · see citing works
Thermochemistry of Pure-Silica Zeolites
Piccione, P. M., Laberty, C., Yang, S., Camblor, M. A., Navrotsky, A., & Davis, M. E. (2000) · The Journal of Physical Chemistry B · doi:10.1021/jp002148a · Cited by 214 · see citing works
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Zeolites in Adsorption Processes: State of the Art and Future Prospects
Pérez-Botella, E., Valencia, S., & Rey, F. (2022) · Chemical Reviews · doi:10.1021/acs.chemrev.2c00140 · Cited by 1,126 · see citing works
Accelerated crystallization of zeolites via hydroxyl free radicals
Feng, G., Cheng, P., Yan, W., Boronat, M., Li, X., Su, J.-H., Wang, J., Li, Y., Corma, A., Xu, R., et al. (2016) · Science · doi:10.1126/science.aaf1559 · Cited by 443 · see citing works
Structuring adsorbents and catalysts by processing of porous powders
Akhtar, F., Andersson, L., Ogunwumi, S., Hedin, N., & Bergström, L. (2014) · Journal of the European Ceramic Society · doi:10.1016/j.jeurceramsoc.2014.01.008 · Cited by 363 · see citing works
Verboekend, D., Nuttens, N., Locus, R., Van Aelst, J., Verolme, P., Groen, J. C., Pérez-Ramírez, J., & Sels, B. F. (2016) · Chemical Society Reviews · doi:10.1039/c5cs00520e · Cited by 355 · see citing works
Tosca, N. J., Guggenheim, S., & Pufahl, P. K. (2016) · Geological Society of America Bulletin · doi:10.1130/b31339.1 · Cited by 241 · see citing works
Synthesis of Zeolites via Interzeolite Transformations without Organic Structure-Directing Agents
Goel, S., Zones, S. I., & Iglesia, E. (2015) · Chemistry of Materials · doi:10.1021/cm504510f · Cited by 209 · see citing works
Ke, X., Bernal, S. A., Provis, J. L., & Lothenbach, B. (2020) · Cement and Concrete Research · doi:10.1016/j.cemconres.2020.106158 · Cited by 117 · see citing works
Treps, L., Gomez, A., de Bruin, T., & Chizallet, C. (2020) · ACS Catalysis · doi:10.1021/acscatal.9b05103 · Cited by 63 · see citing works
Shah, M. S., Tsapatsis, M., & Siepmann, J. I. (2015) · Langmuir · doi:10.1021/acs.langmuir.5b03015 · Cited by 46 · see citing works
A reactive neural network framework for water-loaded acidic zeolites
Erlebach, A., Šípka, M., Saha, I., Nachtigall, P., Heard, C. J., & Grajciar, L. (2024) · Nature Communications · doi:10.1038/s41467-024-48609-2 · Cited by 47 · see citing works
“…and thus acidity 7,8 , (ii) hydrolytic bond dissociation and defect formation, which controls catalyst durability and activity 9 , (iii) water mobility and clustering in zeolite pores 10 , and (iv) the synthesis of zeolites from precursor gels containing silica fragments, water and cations 11 .”
BackgroundPérez-Botella, E., Palomino, M., Valencia, S., & Rey, F. (2019) · Green Energy and Technology · doi:10.1007/978-981-13-3504-4_7 · Cited by 29 · see citing works
de Pietre, M. K., & Freitas, J. C. C. (2022) · Environmental Earth Sciences · doi:10.1007/s12665-021-10130-w · Cited by 27 · see citing works
Gross-Lorgouilloux, M., Caullet, P., Soulard, M., Patarin, J., Moleiro, E., & Saude, I. (2010) · Microporous and Mesoporous Materials · doi:10.1016/j.micromeso.2010.01.022 · Cited by 25 · see citing works
Pressure-induced chemistry for the 2D to 3D transformation of zeolites
Mazur, M., Arévalo-López, A. M., Wheatley, P. S., Bignami, G. P. M., Ashbrook, S. E., Morales-García, Á., Nachtigall, P., Attfield, J. P., Čejka, J., & Morris, R. E. (2018) · Journal of Materials Chemistry A · doi:10.1039/c7ta09248b · Cited by 23 · see citing works
Molecular Intermediate in the Directed Formation of a Zeolitic Metal–Organic Framework
Sinnwell, M. A., Miller, Q. R. S., Palys, L., Barpaga, D., Liu, L., Bowden, M. E., Han, Y., Ghose, S., Sushko, M. L., Schaef, H. T., et al. (2020) · Journal of the American Chemical Society · doi:10.1021/jacs.0c07862 · Cited by 21 · see citing works
- Authors
- Cundy, C. S., & Cox, P. A.
- Affiliations
- University of Manchester (GB)
- University of Portsmouth (GB)
- Corresponding author
- Cundy, Colin S.
- ORCID
- Cox, Paul A.
- Venue
- Microporous and Mesoporous Materials
- Publisher
- Elsevier BV
- Published
- 2005-07
- Volume
- 82
- Issue
- 1-2
- Pages
- 1-78
- ISSN
- 1387-1811 (ISSN-L)
- OpenAlex
- W2012948478
- Cited by
- 1,590
- References
- 2
- Citations by year
- 2026: 63 · 2025: 94 · 2024: 95 · 2023: 85 · 2022: 92 · 2021: 114 · 2020: 96 · 2019: 84 · 2018: 92 · 2017: 98 · 2016: 84 · 2015: 89 · 2014: 74 · 2013: 68 · 2012: 55
- FWCI
- 32.75
- Type
- journal article
- Language
- en
- Open access
- closed
- Locations
- Microporous and Mesoporous Materials (publishedVersion)
- Topics
- Physical Sciences › Chemistry › Inorganic Chemistry › Zeolite Catalysis and Synthesis
- Physical Sciences › Environmental Science › Waste Management and Disposal › Chemical Synthesis and Characterization
- Physical Sciences › Materials Science › Biomaterials › Clay minerals and soil interactions
- Keywords
- zeolite synthesis, hydrothermal synthesis, reaction mechanism, nucleation, crystal growth, induction period, solid-state phase transitions
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