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Hydrogen and Oxygen Evolution on Boron‐Doped Diamond Electrodes
Open accessAbstract
The evolution of hydrogen and oxygen was studied on diamond electrodes containing approximately 10 21 boron atom/cm 3 . Voltammetry showed a wide potential window [−1.25 to +2.3 V vs. standard hydrogen electrode (SHE)] without significant water decomposition. This window was much narrower for poor quality diamond films with appreciable sp 2 content. A redox couple observed at +1.7 V indicates oxidation of the diamond surface prior to oxygen evolution. The extent of surface oxidation increased with sp 2 content. Anodic polarization made the diamond surface hydrophilic; x‐ray photoelectron spectroscopy showed an increase in oxygen coverage and the presence of carbon‐oxygen bonds. The estimated capacitance of the interface ranged from 0.05 μF/cm 2 for high quality diamond to 5 μF/cm 2 for low quality diamond. Preliminary measurements of the exchange current densities for oxygen and hydrogen evolution indicated slow kinetics compared to metals or highly oriented pyrolytic graphite.
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Citations
Cited by
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A Materials Roadmap to Functional Neural Interface Design
Wellman, S. M., Eles, J. R., Ludwig, K. A., Seymour, J. P., Michelson, N. J., McFadden, W. E., Vazquez, A. L., & Kozai, T. D. Y. (2018) · Advanced Functional Materials · doi:10.1002/adfm.201701269 · Cited by 389
Metadata
- Authors
- Martin, H. B., Argoitia, A., Landau, U., Anderson, A. B., & Angus, J. C.
- Venue
- Journal of The Electrochemical Society
- Publisher
- The Electrochemical Society
- Published
- 1996-06-01
- Volume
- 143
- Issue
- 6
- Pages
- L133-L136
- ISSN
- 0013-4651 (ISSN-L)
- 1945-7111
- OpenAlex
- W2022199489
- Cited by
- 430
- References
- 0
- FWCI
- 21.30
- Type
- journal article
- Language
- en
- Open access
- bronze
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- Martin, H. B., Argoitia, A., Landau, U., Anderson, A. B., & Angus, J. C. (1996). Hydrogen and Oxygen Evolution on Boron‐Doped Diamond Electrodes. Journal of The Electrochemical Society. https://doi.org/10.1149/1.1836901
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