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One-pot synthesis of monodisperse iron oxide nanoparticles for potential biomedical applications
Open accessAbstract
One-pot reaction of iron(III) acetylacetonate, Fe(acac)3, [or Fe(acac)3 and M(acac)2 where M = Mn and Co], with 1,2-alkanediol, oleic acid, and oleylamine in high boiling organic solvent leads to monodisperse ferrite MFe 2 O 4 nanoparticles. Depending on the concentration of the metal precursors, surfactant-to-metal precursor ratio and the solvent used in the reaction, the particle size from this one-pot reaction can be tuned from 4 to 15 nm. The as-synthesized iron oxide nanoparticles have an inverse spinel structure, and their magnetic properties are controlled by particle size and M in the MFe 2 O 4 structure. The hydrophobic iron oxide nanoparticles are readily transformed into hydrophilic ones by functional phospholipid addition to the as-synthesized particles and as a result, the monodisperse nanoparticles are readily functionalized with biotin, -COOH, -SH, and -NH 2, facilitating their link to biomolecules for biomedical applications.
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Cited by
Kim, D., Resasco, J., Yu, Y., Asiri, A. M., & Yang, P. (2014) · Nature Communications · doi:10.1038/ncomms5948 · Cited by 1,374
Monodisperse mesoporous superparamagnetic single-crystal magnetite nanoparticles for drug delivery
Guo, S., Li, D., Zhang, L., Li, J., & Wang, E. (2009) · Biomaterials · doi:10.1016/j.biomaterials.2008.12.042 · Cited by 398
Tromsdorf, U. I., Bruns, O. T., Salmen, S. C., Beisiegel, U., & Weller, H. (2009) · Nano Letters · doi:10.1021/nl902715v · Cited by 396
Mutin, P. H., & Vioux, A. (2009) · Chemistry of Materials · doi:10.1021/cm802348c · Cited by 296
Mourdikoudis, S., Menelaou, M., Fiuza-Maneiro, N., Zheng, G., Wei, S., Pérez-Juste, J., Polavarapu, L., & Sofer, Z. (2022) · Nanoscale Horizons · doi:10.1039/d2nh00111j · Cited by 259
Metadata
- Authors
- Xie, J., Peng, S., Brower, N., Pourmand, N., Wang, S. X., & Sun, S.
- Venue
- Pure and Applied Chemistry
- Publisher
- Walter de Gruyter GmbH
- Published
- 2006-01-01
- Volume
- 78
- Issue
- 5
- Pages
- 1003-1014
- ISSN
- 0033-4545 (ISSN-L)
- 1365-3075
- OpenAlex
- W2144090653
- Cited by
- 161
- References
- 0
- FWCI
- 5.43
- Type
- journal article
- Language
- en
- Open access
- bronze
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- Xie, J., Peng, S., Brower, N., Pourmand, N., Wang, S. X., & Sun, S. (2006). One-pot synthesis of monodisperse iron oxide nanoparticles for potential biomedical applications. Pure and Applied Chemistry. https://doi.org/10.1351/pac200678051003
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