Optimization of the Process for Green Jujube Vinegar and Organic Acid and Volatile Compound Analysis during Brewing
Open accessAbstract
Healthy fruit vinegar has become very popular recently in China. This study aimed to produce fruit vinegar with a good taste, high nutritional value, and strong functional properties from green jujube. This study investigated the optimization of the process for green jujube vinegar using response surface methodology. The optimum fermentation parameters for green jujube vinegar were determined as follows: initial alcoholicity 6%, acetobacter 8%, fermentation temperature 32 °C, and time 7 d. The organic acids of the optimized sample were evaluated by HPLC, and the volatile substances were identified and analyzed by HS-SPME and GC-MS during the fermentation and aging of the green jujube vinegar. The results showed that the variation trends of the different organic acids during the making of the green jujube vinegar were significantly different. Organic acids are the key flavor compounds of green jujube vinegar, and their changes were mainly attributed to microbial metabolism. In particular, the green jujube vinegar stood out in terms of volatile aroma compounds, including a total of 61 volatile compounds whose major components were acetic acid, isoamyl acetate, ethyl acetate, 3-hydroxy-2-butanone, methyl palmitate, and ethanol. The results can provide theoretical support for the production of green jujube vinegar.
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During the initial fermentation stage of vinegar production, yeast serves as the primary fermentative agent, metabolizing sugars to produce alcohol and generating flavor compounds such as esters, aldehydes, and higher alcohols that form the foundation for the characteristic aroma and taste of fruit vinegar.
“During the initial fermentation stage of vinegar production, yeast serves as the primary fermentative agent. It metabolizes the sugars present in the raw materials to produce alcohol. Concurrently, this process generates flavor compounds such as esters, aldehydes, and higher alcohols, which form the foundation for the characteristic aroma and taste of fruit vinegar [10].”
From The Metabolic Pathways of Yeast and Acetic Acid Bacteria During Fruit Vinegar Fermentation and Their Influence on Flavor Development (2025) · cites this paper as [10]
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Ge, Y., Wu, Y., Aihaiti, A., Wang, L., Wang, Y., Xing, J., Zhu, M., & Hong, J. (2025) · Microorganisms · doi:10.3390/microorganisms13030477 · Cited by 49 · see citing works
- Authors
- Li, G., Yan, N., Li, G., & Wang, J.
- Affiliations
- Shanxi Normal University (CN)
- Corresponding author
- Li, Guifeng
- Venue
- Foods
- Publisher
- MDPI AG
- Published
- 2023-08-23
- Volume
- 12
- Issue
- 17
- Pages
- 3168
- ISSN
- 2304-8158 (ISSN-L)
- PMC
- PMC10486836
- OpenAlex
- W4386091460
- Cited by
- 10
- References
- 4
- Citations by year
- 2026: 6 · 2025: 3 · 2024: 1
- FWCI
- 1.44
- Type
- journal article
- Language
- en
- Open access
- gold
- doi.org
- Licence
- Locations
- Foods (publishedVersion, cc-by)
- PubMed Central (publishedVersion, cc-by)
- PubMed (publishedVersion)
- DOAJ (DOAJ: Directory of Open Access Journals) (submittedVersion, cc-by-sa)
- Funders
- Shanxi Normal University (2018YZKC-07, 20210302124515)
- Fundamental Research Program of Shanxi Province (2018YZKC-07, 20210302124515)
- Topics
- Life Sciences › Agricultural and Biological Sciences › Food Science › Ziziphus Jujuba Studies and Applications
- Life Sciences › Agricultural and Biological Sciences › Food Science › Fermentation and Sensory Analysis
- Life Sciences › Agricultural and Biological Sciences › Food Science › Food and Agricultural Sciences
- Keywords
- fruit vinegar, organic acids, volatile flavor compounds, Acetobacter, fermentation parameters, vinegar aging, isoamyl acetate, acetic acid, flavor compounds
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