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Preparation, Structure, and Electrochemical Properties of Reduced Graphene Sheet Films

Tang, Longhua, Wang, Ying, Li, Yueming, Feng, Hongbing, Lu, Jin, Li, Jinghong·2009·Advanced Functional Materials

Abstract

This paper describes the preparation, characterization, and electrochemical properties of reduced graphene sheet films (rGSFs), investigating especially their electrochemical behavior for several redox systems and electrocatalytic properties towards oxygen and some small molecules. The reduced graphene sheets (rGSs) are produced in high yield by a soft chemistry route involving graphite oxidation, ultrasonic exfoliation, and chemical reduction. Transmission electron microscopy (TEM), X‐ray diffraction (XRD), scanning electron microscopy (SEM), X‐ray photoelectron spectroscopy (XPS) and Raman spectroscopy clearly demonstrate that graphene was successfully synthesized and modified at the surface of a glassy carbon electrode. Several redox species, such as Ru(NH 3)63+/2+, Fe(CN)63−/4−, Fe 3+/2+ and dopamine, are used to probe the electrochemical properties of these graphene films by using the cyclic voltammetry method. The rGSFs demonstrate fast electron‐transfer (ET) kinetics and possess excellent electrocatalytic activity toward oxygen reduction and certain biomolecules. In our opinion, this microstructural and electrochemical information can serve as an important benchmark for graphene‐based electrode performances.

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Metadata

Authors
Tang, L., Wang, Y., Li, Y., Feng, H., Lu, J., & Li, J.
Venue
Advanced Functional Materials
Publisher
Wiley
Published
2009-09
Volume
19
Issue
17
Pages
2782-2789
ISSN
  • 1616-301X (ISSN-L)
  • 1616-3028
OpenAlex
W1998704602
Cited by
1,178
References
4
FWCI
38.92
Type
journal article
Language
en
Open access
closed

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CoChat. (2026). Citation check: Preparation, Structure, and Electrochemical Properties of Reduced Graphene Sheet Films. https://app.cochat.ai/papers/10.1002/adfm.200900377
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Tang, L., Wang, Y., Li, Y., Feng, H., Lu, J., & Li, J. (2009). Preparation, Structure, and Electrochemical Properties of Reduced Graphene Sheet Films. Advanced Functional Materials. https://doi.org/10.1002/adfm.200900377

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Contains information from the Semantic Scholar Academic Graph Datasets, made available under the ODC Attribution License (ODC-BY 1.0).

Semantic Scholar’s data is described in: Kinney, R., et al. (2023). The Semantic Scholar Open Data Platform. arXiv:2301.10140.