Cited by 203Advancements in Battery MaterialsAdvanced Battery Materials and TechnologiesBattery Modeling and Management

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Ethylene‐Carbonate‐Free Electrolytes for Rechargeable Li‐Ion Pouch Cells at Sub‐Freezing Temperatures

Yao, Yu‐Xing, Yao, Nan, Zhou, Xi‐Rui, Li, Ze‐Heng, Yue, Xin‐Yang, Yan, Chong, Zhang, Qiang·2022·Advanced Materials

DOI 10.1002/adma.202206448

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Abstract

Sub‐freezing temperature presents a significant challenge to the survival of current Li‐ion batteries (LIBs) as it leads to low capacity retention and poor cell rechargeability. The electrolyte in commercial LIBs relies too heavily on ethylene carbonate (EC) to produce a stable solid electrolyte interphase (SEI) on graphite (Gr) anodes, but its high melting point (36.4 °C) severely restricts ion transport below 0 °C, causing energy loss and Li plating. Here, a class of EC‐free electrolytes that exhibits remarkable low‐temperature performance without compromising cell lifespan is reported. It is found that at sub‐zero temperatures, EC forms highly resistive SEI that seriously impedes electrode kinetics, whereas EC‐free electrolytes create a highly stable, low‐impedance SEI through anion decomposition, which boosts capacity retention and eliminates Li plating during charging. Pouch‐type LiCoO 2 (LCO)|Gr cells with EC‐free electrolytes sustain 900 cycles at 25 °C with 1 C charge/discharge, and LiNi 0.85 Co 0.10 Al 0.05 O 2 (NCA)|Gr cells last 300 cycles at −15 °C with 0.3 C charge, both among the best‐performing in the literature under comparable conditions. Even at −50 °C, the NCA|Gr cell with EC‐free electrolytes still delivers 76% of its room‐temperature capacity, outperforming EC‐based electrolytes.

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Authors: Yao, Y., Yao, N., Zhou, X., Li, Z., Yue, X., Yan, C., & Zhang, Q.
Affiliations: Beijing Key Laboratory of Green Chemical Reaction Engineering and Technology Department of Chemical Engineering Tsinghua University Beijing 100084 China
Tsinghua University (CN)
Corresponding author: Zhang, Qiang
ORCID: Yao, Nan
Yan, Chong
Zhang, Qiang
Venue: Advanced Materials
Publisher: Wiley
Published: 2022-10-06
Volume: 34
Issue: 45
Pages: e2206448-e2206448
ISSN: 0935-9648 (ISSN-L)
1521-4095
DOI: 10.1002/adma.202206448
OpenAlex: W4295762463
Cited by: 203
References: 0
Citations by year: 2026: 43 · 2025: 64 · 2024: 56 · 2023: 40
FWCI: 10.96
Type: journal article
Language: en
Open access: closed
Licence: onlinelibrary.wiley.com/termsAndConditions#vor (vor)
Locations: Advanced Materials (publishedVersion)
PubMed (publishedVersion)
Funders: National Basic Research Program of China (2021YFB2500300)
Topics: Physical Sciences › Engineering › Electrical and Electronic Engineering › Advancements in Battery Materials
Physical Sciences › Engineering › Electrical and Electronic Engineering › Advanced Battery Materials and Technologies
Physical Sciences › Engineering › Automotive Engineering › Battery Modeling and Management
Keywords: rechargeable lithium-ion batteries, pouch cells, solid electrolyte interphase, anion decomposition, lithium plating, LiCoO2 cathode, NCA cathode, graphite anode, low-temperature cycling stability, capacity retention

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Ethylene‐Carbonate‐Free Electrolytes for Rechargeable Li‐Ion Pouch Cells at Sub‐Freezing Temperatures

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