Single‐Crystalline Ultrathin Nickel Nanosheets Array from In Situ Topotactic Reduction for Active and Stable Electrocatalysis

Kuang, Yun; Feng, Guang; Li, Pengsong; Bi, Yongmin; Li, Yaping; Sun, Xiaoming

doi:10.1002/anie.201509616

Cited by 259Electrocatalysts for Energy ConversionElectrochemical sensors and biosensorsCatalytic Processes in Materials Science

Single‐Crystalline Ultrathin Nickel Nanosheets Array from In Situ Topotactic Reduction for Active and Stable Electrocatalysis

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Kuang, Yun, Feng, Guang, Li, Pengsong, Bi, Yongmin, Li, Yaping, Sun, Xiaoming·2016·Angewandte Chemie International Edition

DOI 10.1002/anie.201509616PMC PMC4706644

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Abstract

Simultaneously synthesizing and structuring atomically thick or ultrathin 2D non-precious metal nanocrystal may offer a new class of materials to replace the state-of-art noble-metal electrocatalysts; however, the synthetic strategy is the bottleneck which should be urgently solved. Here we report the synthesis of an ultrathin nickel nanosheet array (Ni-NSA) through in situ topotactic reduction from Ni(OH)2 array precursors. The Ni nanosheets showed a single-crystalline lamellar structure with only ten atomic layers in thickness and an exposed (111) facet. Combined with a superaerophobic (low bubble adhesive) arrayed structure the Ni-NSAs exhibited a dramatic enhancement on both activity and stability towards the hydrazine-oxidation reaction (HzOR) relative to platinum. Furthermore, the partial oxidization of Ni-NSAs in ambient atmosphere resulted in effective water-splitting electrocatalysts for the hydrogen-evolution reaction (HER).

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2D CoP nanosheets are more feasible for enhancing HER catalytic activity because 2D nanostructures expose catalytically active sites that promote interfacial charge transfer.
“Among them, 2D CoP nanosheets are more feasible to enhance HER catalytic activity, since the 2D nanostructures enable to expose catalytically active sites which promote interfacial charge transfer.”
From Sub‐1.5 nm Ultrathin CoP Nanosheet Aerogel: Efficient Electrocatalyst for Hydrogen Evolution Reaction at All pH Values (2018) · cites this paper as [23]
The indexed copy (section labeled Abstract; page unavailable) links ultrathin 2D nickel nanosheets to abundant active sites and lower charge-transfer resistance, and reports improved HER performance for partially oxidized Ni/NiO nanosheets. It does not study CoP nanosheets or establish that their exposed sites promote interfacial charge transfer during HER. (LLM, conf=0.86)
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Authors: Kuang, Y., Feng, G., Li, P., Bi, Y., Li, Y., & Sun, X.
Affiliations: State Key Laboratory of Chemical Resource Engineering (CN)
Corresponding author: Sun, Xiaoming
ORCID: Kuang, Yun
Feng, Guang
Li, Pengsong
Li, Yaping
Sun, Xiaoming
Venue: Angewandte Chemie International Edition
Publisher: Wiley
Published: 2015-11-19
Volume: 55
Issue: 2
Pages: 693-697
ISSN: 1433-7851 (ISSN-L)
1521-3773
DOI: 10.1002/anie.201509616
PMC: PMC4706644
OpenAlex: W2173150847
Cited by: 259
References: 41
Citations by year: 2026: 4 · 2025: 15 · 2024: 13 · 2023: 19 · 2022: 20 · 2021: 39 · 2020: 32 · 2019: 30 · 2018: 32 · 2017: 35 · 2016: 20
FWCI: 8.59
Type: journal article
Language: en
Open access: hybrid
doi.org
Licence: other-oa
onlinelibrary.wiley.com/termsAndConditions#vor (vor)
Locations: Angewandte Chemie International Edition (publishedVersion, other-oa)
PubMed Central (publishedVersion, cc-by-nc)
PubMed (publishedVersion)
Funders: Funded Access
National Natural Science Foundation of China
973 Program (2011CBA00503, 2011CB932403)
Program for Changjiang Scholars and Innovative Research Team in the University
Topics: Physical Sciences › Energy › Renewable Energy, Sustainability and the Environment › Electrocatalysts for Energy Conversion
Physical Sciences › Engineering › Electrical and Electronic Engineering › Electrochemical sensors and biosensors
Physical Sciences › Materials Science › Materials Chemistry › Catalytic Processes in Materials Science
Keywords: topotactic reduction, superaerophobic surfaces, hydrazine oxidation, hydrogen evolution reaction, water splitting, non-precious metal electrocatalysts, catalyst stability

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Single‐Crystalline Ultrathin Nickel Nanosheets Array from In Situ Topotactic Reduction for Active and Stable Electrocatalysis

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