The DOI matches its Crossref record; 1 of the 1 references it cites were found in a registry or an index.
Characterization of nonderivatized plant cell walls using high‐resolution solution‐state NMR spectroscopy
Open accessAbstract
A recently described plant cell wall dissolution system has been modified to use perdeuterated solvents to allow direct in‐NMR‐tube dissolution and high‐resolution solution‐state NMR of the whole cell wall without derivatization. Finely ground cell wall material dissolves in a solvent system containing dimethylsulfoxide‐d6 and 1‐methylimidazole‐d6 in a ratio of 4:1 (v/v), keeping wood component structures mainly intact in their near‐native state. Two‐dimensional NMR experiments, using gradient‐HSQC (heteronuclear single quantum coherence) 1‐bond 13 C1 H correlation spectroscopy, on nonderivatized cell wall material from a representative gymnosperm pinus taeda (loblolly pine), an angiosperm Populus tremuloides (quaking aspen), and a herbaceous plant Hibiscus cannabinus (kenaf) demonstrate the efficacy of the system. We describe a method to synthesize 1‐methylimidazole‐d6 with a high degree of perdeuteration, thus allowing cell wall dissolution and NMR characterization of nonderivatized plant cell wall structures. Copyright © 2008 John Wiley & Sons, Ltd.
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Cites
Wood: Chemistry, ultrastructure, reactions
(1983) · doi:10.1515/9783110839654 · Cited by 2,846
Cited by
Lignin Biosynthesis and Structure
Vanholme, R., Demedts, B., Morreel, K., Ralph, J., & Boerjan, W. (2010) · Plant Physiology · doi:10.1104/pp.110.155119 · Cited by 2,664
Self-citationWhole plant cell wall characterization using solution-state 2D NMR
Mansfield, S. D., Kim, H., Lu, F., & Ralph, J. (2012) · Nature Protocols · doi:10.1038/nprot.2012.064 · Cited by 720
Self-citationBioethanol Production from Lignocellulosic Biomass—Challenges and Solutions
Broda, M., Yelle, D. J., & Serwańska, K. (2022) · Molecules · doi:10.3390/molecules27248717 · Cited by 357
Self-citationCarbohydrate-aromatic interface and molecular architecture of lignocellulose
Kirui, A., Zhao, W., Deligey, F., Yang, H., Kang, X., Mentink-Vigier, F., & Wang, T. (2022) · Nature Communications · doi:10.1038/s41467-022-28165-3 · Cited by 290
Understanding the impact of ionic liquid pretreatment on eucalyptus
Çetinkol, Ö. P., Dibble, D. C., Cheng, G., Kent, M. S., Knierim, B., Auer, M., Wemmer, D. E., Pelton, J. G., Melnichenko, Y. B., Ralph, J., et al. (2010) · Biofuels · doi:10.4155/bfs.09.5 · Cited by 135
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Metadata
- Authors
- Yelle, D. J., Ralph, J., & Frihart, C. R.
- Venue
- Magnetic Resonance in Chemistry
- Publisher
- Wiley
- Published
- 2008-03-28
- Volume
- 46
- Issue
- 6
- Pages
- 508-517
- ISSN
- 0749-1581 (ISSN-L)
- 1097-458X
- OpenAlex
- W2020597418
- Cited by
- 175
- References
- 1
- FWCI
- 14.65
- Type
- journal article
- Language
- en
- Open access
- green
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- Yelle, D. J., Ralph, J., & Frihart, C. R. (2008). Characterization of nonderivatized plant cell walls using high‐resolution solution‐state NMR spectroscopy. Magnetic Resonance in Chemistry. https://doi.org/10.1002/mrc.2201
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