The DOI matches its Crossref record; 63 of the 63 references it cites were found in a registry or an index.
One MAX phase, different MXenes: A guideline to understand the crucial role of etching conditions on Ti3C2Tx surface chemistry
Open accessAbstract
Abstract MXenes are a new, and growing, family of 2D materials with very promising properties for a wide variety of applications. Obtained from the etching of MAX phases, numerous properties can be targeted thanks to the chemical richness of the precursors. Herein, we highlight how etching agents govern surface chemistries of Ti3C2Tx, the most widely studied MXene to date. By combining characterization tools such as X-ray diffraction, X-ray photoelectron, Raman and electron energy loss spectroscopies, scanning and transmission electron microscopies and a surface sensitive electrochemical reaction – the hydrogen evolution reaction, HER – we clearly demonstrate that the etching agent (HF, LiF/HCl or FeF3/HCl) strongly modifies the nature of surface terminal groups (F, OH and/or O), oxidation sensitivity, delamination ability, nature of the inserted species, interstratification, concentration of defects and size of flakes. Beyond showing how using these different characterization tools to analyze MXenes, this work highlights that the MXene synthesis routes can influence targeted applications.
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Cites
Two‐Dimensional Nanocrystals Produced by Exfoliation of Ti3AlC2
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Self-citationThe Li-Ion Rechargeable Battery: A Perspective
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2D metal carbides and nitrides (MXenes) for energy storage
Anasori, B., Lukatskaya, M. R., & Gogotsi, Y. (2017) · Nature Reviews Materials · doi:10.1038/natrevmats.2016.98 · Cited by 7,440
25th Anniversary Article: MXenes: A New Family of Two‐Dimensional Materials
Naguib, M., Mochalin, V. N., Barsoum, M. W., & Gogotsi, Y. (2014) · Advanced Materials · doi:10.1002/adma.201304138 · Cited by 6,414
Self-citationConductive two-dimensional titanium carbide ‘clay’ with high volumetric capacitance
Ghidiu, M., Lukatskaya, M. R., Zhao, M.-Q., Gogotsi, Y., & Barsoum, M. W. (2014) · Nature · doi:10.1038/nature13970 · Cited by 5,997
Self-citationElectromagnetic interference shielding with 2D transition metal carbides (MXenes)
Shahzad, F., Alhabeb, M., Hatter, C. B., Anasori, B., Man Hong, S., Koo, C. M., & Gogotsi, Y. (2016) · Science · doi:10.1126/science.aag2421 · Cited by 5,201
Guidelines for Synthesis and Processing of Two-Dimensional Titanium Carbide (Ti3C2Tx MXene)
Alhabeb, M., Maleski, K., Anasori, B., Lelyukh, P., Clark, L., Sin, S., & Gogotsi, Y. (2017) · Chemistry of Materials · doi:10.1021/acs.chemmater.7b02847 · Cited by 5,045
X-ray photoelectron spectroscopy of select multi-layered transition metal carbides (MXenes)
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Self-citationNovel Electronic and Magnetic Properties of Two‐Dimensional Transition Metal Carbides and Nitrides
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Applications of 2D MXenes in energy conversion and storage systems
Pang, J., Mendes, R. G., Bachmatiuk, A., Zhao, L., Ta, H. Q., Gemming, T., Liu, H., Liu, Z., & Rummeli, M. H. (2019) · Chemical Society Reviews · doi:10.1039/c8cs00324f · Cited by 1,951
Cited by
Two-dimensional MXene-based and MXene-derived photocatalysts: Recent developments and perspectives
Zhong, Q., Li, Y., & Zhang, G. (2021) · Chemical Engineering Journal · doi:10.1016/j.cej.2020.128099 · Cited by 466
Monitoring Ti3C2Tx MXene Degradation Pathways Using Raman Spectroscopy
Adomaviciute-Grabusove, S., Popov, A., Ramanavicius, S., Sablinskas, V., Shevchuk, K., Gogotsi, O., Baginskiy, I., Gogotsi, Y., & Ramanavicius, A. (2024) · ACS Nano · doi:10.1021/acsnano.4c02150 · Cited by 283
Kim, J. Y., Hong, W. T., Phu, T. K. C., Cho, S. C., Kim, B., Baeck, U., Oh, H., Koh, J. H., Yu, X., Choi, C. H., et al. (2024) · Advanced Science · doi:10.1002/advs.202405154 · Cited by 41
Metadata
- Authors
- Benchakar, M., Loupias, L., Garnero, C., Bilyk, T., Morais, C., Canaff, C., Guignard, N., Morisset, S., Pazniak, H., Hurand, S., Chartier, P., Pacaud, J., Mauchamp, V., Barsoum, M. W., Habrioux, A., & Célérier, S.
- Venue
- Applied Surface Science
- Publisher
- Elsevier BV
- Published
- 2020-11
- Volume
- 530
- Pages
- 147209
- ISSN
- 0169-4332 (ISSN-L)
- OpenAlex
- W3044354659
- Cited by
- 384
- References
- 63
- FWCI
- 15.10
- Type
- journal article
- Language
- en
- Open access
- bronze
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- Benchakar, M., Loupias, L., Garnero, C., Bilyk, T., Morais, C., Canaff, C., Guignard, N., Morisset, S., Pazniak, H., Hurand, S., Chartier, P., Pacaud, J., Mauchamp, V., Barsoum, M. W., Habrioux, A., & Célérier, S. (2020). One MAX phase, different MXenes: A guideline to understand the crucial role of etching conditions on Ti3C2Tx surface chemistry. Applied Surface Science. https://doi.org/10.1016/j.apsusc.2020.147209
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