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Cellulose extraction from wood chip in an ionic liquid 1-allyl-3-methylimidazolium chloride (AmimCl)
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In the present study, 1-allyl-3-methylimidazolium chloride (AmimCl), an ionic liquid (IL), was used to extract cellulose from pine, poplar, Chinese parasol, and catalpa wood chips. Results show that pine is the most suitable wood species for cellulose extraction with ILs. Its cellulose extraction rate can reach as high as 62% under optimized conditions and its cellulose content is as high as 85% when DMSO/water is used as the precipitant. The dissolution process can be clearly observed by hot stage optical microscopy, and the reaction time can be significantly reduced by microwave irradiation. (13)C CP/MAS NMR, FTIR, XRD, and SEM were used to analyze the cellulose-rich extracts of pine. Results show that IL dissolves pine wood by destroying inter and intramolecular hydrogen bonds between lignocelluloses. The major component of pine extract is cellulose with a homogeneous and dense structure. After extraction, AmimCl can be easily recycled and reused.
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“An increase of the amount of recovered pulp was observed after the 4th cycle; the lignin content in the recovered solid remained constant over the course of the experiment.”
From Deconstruction of lignocellulosic biomass with ionic liquids (2013) · cites this paper as [140]
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“Another study reused [C 4 C 1 im]Cl 7 times for fractionation of legume straw with ionic liquid water mixtures.140”
From Deconstruction of lignocellulosic biomass with ionic liquids (2013) · cites this paper as [140]
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- Myllymaeki, V., Aksela, R., Myllymaki, V., 2005. Method for dissolving lignocellulosic material, such as wood, involves mixing lignocellulosic material with ionic liquid solvent under microwave irradiation and/or pressure in absence of water for complete dissolution. pp. 1654307-A1654301, Kemira Oyj (Kemh).
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Özkan, B. Ç., & GÜNER, M. (2022) · Cellulose · doi:10.1007/s10570-022-04682-8 · Cited by 21
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Optimizing lignin extraction from Kraft black liquor using protic Ionic liquids
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Metadata
- Authors
- Wang, X., Li, H., Cao, Y., & Tang, Q.
- Affiliations
- Chinese Academy of Sciences (CN)
- Corresponding author
- Li, Huiquan
- Venue
- Bioresource Technology
- Publisher
- Elsevier BV
- Published
- 2011-09
- Volume
- 102
- Issue
- 17
- Pages
- 7959-7965
- ISSN
- 0960-8524 (ISSN-L)
- OpenAlex
- W2047922947
- Cited by
- 198
- References
- 27
- Citations by year
- 2026: 8 · 2025: 10 · 2024: 9 · 2023: 9 · 2022: 12 · 2021: 12 · 2020: 17 · 2019: 13 · 2018: 14 · 2017: 18 · 2016: 11 · 2015: 17 · 2014: 20 · 2013: 18 · 2012: 9
- FWCI
- 6.28
- Type
- journal article
- Language
- en
- Open access
- green
- ir.ipe.ac.cn
- Licence
- cc-by-nc-sa
- www.elsevier.com/tdm/userlicense/1.0/ (tdm)
- Locations
- Bioresource Technology (publishedVersion)
- PubMed (publishedVersion)
- Institute of Process Engineering, CAS Institutional Repository (submittedVersion, cc-by-nc-sa)
- Funders
- Major Project of Chinese National Programs for Fundamental Research and Development (2009CB219901)
- Chinese National Natural Science Foundation (21006118)
- Topics
- Physical Sciences › Materials Science › Biomaterials › Advanced Cellulose Research Studies
- Physical Sciences › Chemistry › Physical and Theoretical Chemistry › Ionic liquids properties and applications
- Physical Sciences › Engineering › Biomedical Engineering › Biofuel production and bioconversion
- Keywords
- cellulose extraction, ionic liquids, 1-allyl-3-methylimidazolium chloride, pine forest, poplar, Catalpa, wood chips, microwave-assisted extraction, hydrogen bond breaking, ionic liquid recycling
- MeSH terms
- Allyl Compounds, Cellulose, Imidazoles, Microwaves, Magnetic Resonance Spectroscopy, Temperature, Wood, Spectroscopy, Fourier Transform Infrared
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