Cited by 198Advanced Cellulose Research StudiesIonic liquids properties and applicationsBiofuel production and bioconversion

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Cellulose extraction from wood chip in an ionic liquid 1-allyl-3-methylimidazolium chloride (AmimCl)

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Wang, Xuejing, Li, Huiquan, Cao, Yan, Tang, Qing·2011·Bioresource Technology

DOI 10.1016/j.biortech.2011.05.064

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Abstract

In the present study, 1-allyl-3-methylimidazolium chloride (AmimCl), an ionic liquid (IL), was used to extract cellulose from pine, poplar, Chinese parasol, and catalpa wood chips. Results show that pine is the most suitable wood species for cellulose extraction with ILs. Its cellulose extraction rate can reach as high as 62% under optimized conditions and its cellulose content is as high as 85% when DMSO/water is used as the precipitant. The dissolution process can be clearly observed by hot stage optical microscopy, and the reaction time can be significantly reduced by microwave irradiation. (13)C CP/MAS NMR, FTIR, XRD, and SEM were used to analyze the cellulose-rich extracts of pine. Results show that IL dissolves pine wood by destroying inter and intramolecular hydrogen bonds between lignocelluloses. The major component of pine extract is cellulose with a homogeneous and dense structure. After extraction, AmimCl can be easily recycled and reused.

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Myllymaeki, V., Aksela, R., Myllymaki, V., 2005. Method for dissolving lignocellulosic material, such as wood, involves mixing lignocellulosic material with ionic liquid solvent under microwave irradiation and/or pressure in absence of water for complete dissolution. pp. 1654307-A1654301, Kemira Oyj (Kemh).

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Authors: Wang, X., Li, H., Cao, Y., & Tang, Q.
Affiliations: Chinese Academy of Sciences (CN)
Corresponding author: Li, Huiquan
ORCID: Li, Huiquan
Cao, Yan
Tang, Qing
Venue: Bioresource Technology
Publisher: Elsevier BV
Published: 2011-09
Volume: 102
Issue: 17
Pages: 7959-7965
ISSN: 0960-8524 (ISSN-L)
DOI: 10.1016/j.biortech.2011.05.064
OpenAlex: W2047922947
Cited by: 198
References: 27
Citations by year: 2026: 8 · 2025: 10 · 2024: 9 · 2023: 9 · 2022: 12 · 2021: 12 · 2020: 17 · 2019: 13 · 2018: 14 · 2017: 18 · 2016: 11 · 2015: 17 · 2014: 20 · 2013: 18 · 2012: 9
FWCI: 6.28
Type: journal article
Language: en
Open access: green
ir.ipe.ac.cn
Licence: cc-by-nc-sa
www.elsevier.com/tdm/userlicense/1.0/ (tdm)
Locations: Bioresource Technology (publishedVersion)
PubMed (publishedVersion)
Institute of Process Engineering, CAS Institutional Repository (submittedVersion, cc-by-nc-sa)
Funders: Major Project of Chinese National Programs for Fundamental Research and Development (2009CB219901)
Chinese National Natural Science Foundation (21006118)
Topics: Physical Sciences › Materials Science › Biomaterials › Advanced Cellulose Research Studies
Physical Sciences › Chemistry › Physical and Theoretical Chemistry › Ionic liquids properties and applications
Physical Sciences › Engineering › Biomedical Engineering › Biofuel production and bioconversion
Keywords: cellulose extraction, ionic liquids, 1-allyl-3-methylimidazolium chloride, pine forest, poplar, Catalpa, wood chips, microwave-assisted extraction, hydrogen bond breaking, ionic liquid recycling
MeSH terms: Allyl Compounds, Cellulose, Imidazoles, Microwaves, Magnetic Resonance Spectroscopy, Temperature, Wood, Spectroscopy, Fourier Transform Infrared

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Cellulose extraction from wood chip in an ionic liquid 1-allyl-3-methylimidazolium chloride (AmimCl)

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