Hexafluoroisopropanol/Brij-35 based supramolecular solvent for liquid-phase microextraction of parabens in different matrix samples

Chen, Jia; Deng, Wenwen; Li, Xiao; Wang, Xuanxuan; Xiao, Yuxiu

doi:10.1016/j.chroma.2019.01.030

Cited by 51Analytical chemistry methods developmentSurfactants and Colloidal SystemsIonic liquids properties and applications

Hexafluoroisopropanol/Brij-35 based supramolecular solvent for liquid-phase microextraction of parabens in different matrix samples

Chen, Jia, Deng, Wenwen, Li, Xiao, Wang, Xuanxuan, Xiao, Yuxiu·2019·Journal of Chromatography A

DOI 10.1016/j.chroma.2019.01.030

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Abstract

A novel supramolecular solvent (SUPRAS) based on hexafluoroisopropanol (HFIP)/Brij-35 was proposed for liquid-phase microextraction (LPME) of parabens in water samples, pharmaceuticals and personal care products. Brij-35 is a cost-effective and non-toxic non-ionic surfactant, but it has a high cloud point (>100 °C). HFIP, with the features of strong hydrogen-bond donor, high density and powerful hydrophobicity, was used as the cloud point-reducing agent and self-assembling and density-regulating solvent of Brij-35. Upon adding HFIP into the Brij-35 aqueous solution, the cloud point of Brij-35 was decreased to below room temperature, and the SUPRAS was formed in the bottom over a wide range of HFIP and Brij-35 concentrations at room temperature. The SUPRAS was composed of Brij-35, HFIP and water, having a density larger than water, and it showed a large spherical structure of positive micellar aggregates (2-8 μm). The HFIP/ Brij-35 SUPRAS-based LPME procedure was non-thermodependent and could be performed at room temperature with centrifugation using normal centrifuge tubes, being very simple. In the extraction of six parabens, the HFIP/ Brij-35 SUPRAS-based LPME method showed short extraction time (3.3 min), low solvent consumption (0.3 mL), and large enrichment factor (26-193). The method of HFIP/ Brij-35 SUPRAS-based LPME with HPLC-DAD gave good linearity for the quantification of parabens with correlation coefficients larger than 0.9990. The limits of detection based on a signal-to-noise ratio of 3 were from 0.042 to 0.167 μg L-1. The recoveries for the spiked real samples were in the range of 90.2-112.4% with relative standard deviation less than 8.9%. Except for tap water, one or several paraben (s) were detected in all the other real samples.

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During 2019, Chen et al. created a SUPRA of Brij 35 to extract parabens from different types of matrices due to its different hydrophobic and hydrophilic binding sites.
“During 2019, Chen et al. [48] created a SUPRA of Brij 35 to extract parabens from different types of matrices due to its different hydrophobic and hydrophilic binding sites.”
From Use of green alternative solvents in dispersive liquid‐liquid microextraction: A review (2022) · cites this paper as [48]
In Chen et al.'s work, HFIP was used to reduce cloud point temperature of Brij 35 and increase density of resulting SUPRA.
“In this work, HFIP was used to reduce the cloud point temperature of Brij 35 and to increase the density of the resulting SUPRA.”
From Use of green alternative solvents in dispersive liquid‐liquid microextraction: A review (2022) · cites this paper as [48]

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Self-citation

Authors: Chen, J., Deng, W., Li, X., Wang, X., & Xiao, Y.
Affiliations: Wuhan University (CN)
Corresponding author: Xiao, Yuxiu
ORCID: Chen, Jia
Deng, Wenwen
Wang, Xuanxuan
Xiao, Yuxiu
Venue: Journal of Chromatography A
Publisher: Elsevier BV
Published: 2019-04
Volume: 1591
Pages: 33-43
ISSN: 0021-9673 (ISSN-L)
DOI: 10.1016/j.chroma.2019.01.030
OpenAlex: W2910484435
Cited by: 51
References: 49
Citations by year: 2026: 2 · 2025: 2 · 2024: 5 · 2023: 11 · 2022: 4 · 2021: 9 · 2020: 11 · 2019: 7
FWCI: 4.34
Type: journal article
Language: en
Open access: closed
Licence: www.elsevier.com/tdm/userlicense/1.0/ (tdm)
Locations: Journal of Chromatography A (publishedVersion)
PubMed (publishedVersion)
Funders: National Natural Science Foundation of China (81673394, 81373045)
Provincial Natural Science Foundation of Hubei of China (2015CFA139)
Large-scale Instrument and Equipment Sharing Foundation of Wuhan University (LF20170838)
Topics: Physical Sciences › Chemistry › Analytical Chemistry › Analytical chemistry methods development
Physical Sciences › Chemistry › Organic Chemistry › Surfactants and Colloidal Systems
Physical Sciences › Chemical Engineering › Catalysis › Ionic liquids properties and applications
Keywords: parabens, hexafluoroisopropanol, Brij 35, supramolecular solvents, liquid-phase microextraction, nonionic surfactants, micellar aggregates, pharmaceuticals and personal care products, water samples, preconcentration, HPLC-DAD, surfactant self-assembly, enrichment factor
MeSH terms: Analysis of Variance, Chromatography, High Pressure Liquid, Pharmaceutical Preparations, Hydrocarbons, Fluorinated, Parabens, Polyethylene Glycols, Reference Standards, Solvents, Water, Water Pollutants, Chemical, Reproducibility of Results, Propanols, Phase Transition, Hydrophobic and Hydrophilic Interactions, Liquid Phase Microextraction

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Hexafluoroisopropanol/Brij-35 based supramolecular solvent for liquid-phase microextraction of parabens in different matrix samples

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