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Access and in situ growth of phosphorene-precursor black phosphorus
Open accessAbstract
Abstract Single crystals of orthorhombic black phosphorus can be grown by a short way transport reaction from red phosphorus and Sn/SnI 4 as mineralization additive. Sizes of several millimeters can be realized with high crystal quality and purity, making a large area preparation of single or multilayer phosphorene possible. An in situ neutron diffraction study was performed addressing the formation of black phosphorus. Black phosphorus is formed directly via gas phase without the occurrence of any other intermediate phase. Crystal growth was initiated after cooling the starting materials down from elevated temperatures at 500 °C.
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Cited by
Recent development of two-dimensional transition metal dichalcogenides and their applications
Choi, W., Choudhary, N., Han, G. H., Park, J., Akinwande, D., & Lee, Y. H. (2017) · Materials Today · doi:10.1016/j.mattod.2016.10.002 · Cited by 2,769
Applications of Phosphorene and Black Phosphorus in Energy Conversion and Storage Devices
Pang, J., Bachmatiuk, A., Yin, Y., Trzebicka, B., Zhao, L., Fu, L., Mendes, R. G., Gemming, T., Liu, Z., & Rummeli, M. H. (2018) · Advanced Energy Materials · doi:10.1002/aenm.201702093 · Cited by 518
Phosphorene: Synthesis, Scale-Up, and Quantitative Optical Spectroscopy
Woomer, A. H., Farnsworth, T. W., Hu, J., Wells, R. A., Donley, C. L., & Warren, S. C. (2015) · ACS Nano · doi:10.1021/acsnano.5b02599 · Cited by 498
Liu, B., Köpf, M., Abbas, A. N., Wang, X., Guo, Q., Jia, Y., Xia, F., Weihrich, R., Bachhuber, F., Pielnhofer, F., et al. (2015) · Advanced Materials · doi:10.1002/adma.201501758 · Cited by 473
Self-citationLi, B., Lai, C., Zeng, G., Huang, D., Qin, L., Zhang, M., Cheng, M., Liu, X., Yi, H., Zhou, C., et al. (2019) · Small · doi:10.1002/smll.201804565 · Cited by 367
Metadata
- Authors
- Köpf, M., Eckstein, N., Pfister, D., Grotz, C., Krüger, I., Greiwe, M., Hansen, T., Kohlmann, H., & Nilges, T.
- Venue
- Journal of Crystal Growth
- Publisher
- Elsevier BV
- Published
- 2014-11
- Volume
- 405
- Pages
- 6-10
- ISSN
- 0022-0248 (ISSN-L)
- OpenAlex
- W2052722181
- Cited by
- 371
- References
- 0
- FWCI
- 13.55
- Type
- journal article
- Language
- en
- Open access
- green
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- Köpf, M., Eckstein, N., Pfister, D., Grotz, C., Krüger, I., Greiwe, M., Hansen, T., Kohlmann, H., & Nilges, T. (2014). Access and in situ growth of phosphorene-precursor black phosphorus. Journal of Crystal Growth. https://doi.org/10.1016/j.jcrysgro.2014.07.029
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