Multi-frequency power ultrasound green extraction of polyphenols from Pingyin rose: Optimization using the response surface methodology and exploration of the underlying mechanism
Open accessAbstract
The effect of multi-frequency power ultrasound (MFPU) on the extraction of Pingyin rose polyphenols (PRP) and underlying mechanisms were studied. The MFPU included mono-, dual-, and tri-frequency ultrasound. Working modes for the dual- and tri-frequency were in sequential and simultaneous ways. The extraction parameter was firstly optimized by RSM (response surface methodology). It was found that the optimum conditions were 50% for ethanol concentration, 63 °C for extraction temperature, 31 min for extraction time, and 1:46 g/mL for solid-liquid ratio with a PRP extraction yield of 156.81 mg/g. The extraction yields of PRP assisted with ultrasound in different power levels and frequencies were further investigated. Compared to non-ultrasound, the extraction yields of PRP assisted with ultrasound were significantly (p < 0.05) increased. The tri-frequency ultrasound in sequential working mode (20/28/40 kHz) showed the most promising extraction efficiencies for PRP (187.13 mg/g), which was 19.33% higher than that of non-ultrasound. Besides, signal results of the MFPU field collected by a hydrophone and damage degree of aluminum foil paper showed that the ultrasonic fields with stronger noise signals, and more uniform broken holes had higher extraction yield of PRP. Conclusively, the MFPU is demonstrated as a green protocol for the valuable extraction of PRP.
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Triple-frequency ultrasonic yielded a higher rose polyphenol yield (187.13 mg/g) than single-frequency ultrasonic (167.92 mg/g).
“The results showed that the yield of rose polyphenols under single-frequency ultrasonic is 167.92 mg/g, and the yield of rose polyphenols under triple-frequency ultrasonic is 187.13 mg/g.”
From A comprehensive review of ultrasonic assisted extraction (UAE) for bioactive components: Principles, advantages, equipment, and combined technologies (2023) · cites this paper as [105]
The Abstract reports a triple-frequency yield of 187.13 mg/g, and the Conclusion says that multi-frequency ultrasound outperformed mono-frequency ultrasound under some conditions. The passages retrieved from section 3.3 and elsewhere do not establish the claimed single-frequency yield of 167.92 mg/g (searched for that value and the single-frequency comparison). (LLM, conf=0.86)
Experimental — accuracy not yet measuredMulti-frequency ultrasonic exhibited a higher extraction rate than single-frequency ultrasonic, and the hydrophone recorded a more robust sound signal.
“Compared to single-frequency ultrasonic, multi-frequency ultrasonic exhibited a higher extraction rate, and concurrently, the hydrophone recorded a more robust sound signal.”
From A comprehensive review of ultrasonic assisted extraction (UAE) for bioactive components: Principles, advantages, equipment, and combined technologies (2023) · cites this paper as [105]
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Shen, L., Pang, S., Zhong, M., Sun, Y., Qayum, A., Liu, Y., Rashid, A., Xu, B., Liang, Q., Ma, H., et al. (2023) · Ultrasonics Sonochemistry · doi:10.1016/j.ultsonch.2023.106646 · Cited by 892 · see citing works
“Xu et al. [105] studied the extraction of rose polyphenols under the influence of multi-frequency power ultrasonics.”
BackgroundSelf-citation
- Authors
- Xu, B., Feng, M., Tiliwa, E. S., Yan, W., Wei, B., Zhou, C., Ma, H., Wang, B., & Chang, L.
- Affiliations
- Jiangsu University (CN)
- Shanghai Academy of Agricultural Sciences (CN)
- Corresponding author
- Xu, Baoguo
- Zhou, Cunshan
- Venue
- LWT
- Publisher
- Elsevier BV
- Published
- 2022-02
- Volume
- 156
- Pages
- 113037
- ISSN
- 0023-6438 (ISSN-L)
- OpenAlex
- W4200581134
- Cited by
- 66
- References
- 54
- Citations by year
- 2026: 17 · 2025: 14 · 2024: 15 · 2023: 7 · 2022: 13
- FWCI
- 2.66
- Type
- journal article
- Language
- en
- Open access
- hybrid
- doi.org
- Licence
- Locations
- LWT (publishedVersion, cc-by-nc-nd)
- Funders
- China Postdoctoral Science Foundation (2020T130261, 2019T120401, SZ-HZ202002)
- National Natural Science Foundation of China (31801561)
- Topics
- Physical Sciences › Materials Science › Materials Chemistry › Ultrasound and Cavitation Phenomena
- Health Sciences › Medicine › Biochemistry › Phytochemicals and Antioxidant Activities
- Life Sciences › Agricultural and Biological Sciences › Food Science › Agricultural and Biological Research
- Keywords
- ultrasound-assisted extraction, extraction optimization, dual-frequency ultrasound, ethanol concentration, extraction temperature, extraction time, solid-to-liquid ratio, green extraction, extraction yield
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