Electrodialytic Removal of Tungsten and Arsenic from Secondary Mine Resources—Deep Eutectic Solvents Enhancement
Open accessAbstract
Tungsten is a critical raw material for European and U.S. economies. Tungsten mine residues, usually considered an environmental burden due to e.g. arsenic content, are also secondary tungsten resources. The electrodialytic (ED) process and deep eutectic solvents (DES) have been successfully and independently applied for the extraction of metals from different complex environmental matrices. In this study a proof of concept demonstrates that coupling DES in a two-compartment ED set-up enhances the removal and separation of arsenic and tungsten from Panasqueira mine secondary resources. Choline chloride with malonic acid (1:2), and choline chloride with oxalic acid (1:1) were the DES that in batch extracted the average maximum contents of arsenic (16%) and tungsten (9%) from the residues. However, when ED was operated at a current intensity of 100 mA for 4 days, the extraction yields increased 22% for arsenic and 11% for tungsten, comparing to the tests with no current. From the total arsenic and tungsten extracted, 82% and 77% respectively were successfully removed from the matrix compartment, as they electromigrated to the anolyte compartment, from where these elements can be further separated. This achievement potentiates circular economy, as the final treated residue could be incorporated in construction materials production, mitigating current environmental problems in both mining and construction sectors.
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Acidic DESs have shown strong capability in leaching heavy metals and rare earth elements from solid waste materials.
“In particular, acidic DESs have shown strong capability in the leaching of heavy metals and rare earth elements from solid waste materials [37].”
From Eco-Friendly Deep Eutectic Solvent-Based Extraction Technologies: A Comprehensive Review of Principles, Applications, and Comparative Insights (2026) · cites this paper as [37]
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Almeida, J., Faria, P., Silva, A. S., Mateus, E. P., & Ribeiro, A. B. (2021) · doi:10.1002/9781119670186.ch4 · Cited by 1 · see citing works
Self-citationYan, Y., Jenkin, G. R. T., Abbott, A. P., Tanciongco, A. M., Arcilla, C. A., Gibaga, C. R., Smith, D. J., Tungpalan, K., Chambers, J. E., Gervasio, J. H., et al. (2026) · Chemical Engineering Journal · doi:10.1016/j.cej.2026.174859
Dańczak, M., & Sobianowska-Turek, A. (2026) · GAZ WODA I TECHNIKA SANITARNA · doi:10.65545/gwits.2026.02.02
Kumar, P., Banerjee, K., Kumar, Y., & Vikal, M. (2026) · Biointerface Research in Applied Chemistry · doi:10.33263/briac162.051
Poduval, A., Bone, S., Brownlow, J. W., Longbottom, T., & Jew, A. D. (2026) · Energy & Fuels · doi:10.1021/acs.energyfuels.6c00713
Case studies of successful implementations
Ishaq, R., Bakar, A., Ashraf, A., Ahmad, N., & Afzal, U. (2026) · Developments in environmental science · doi:10.1016/b978-0-443-41688-0.00018-9
Wen, B. (2026) · SSRN Electronic Journal · doi:10.2139/ssrn.7065683
Ghosh, B., & Ghosh, A. K. (2026) · Bulletin of Materials Science · doi:10.1007/s12034-026-03761-x
Lignin separation modification and high-value utilization based on low eutectic solvents: a review
Sun, R., Li, C., Liang, R., Zhang, Y., & Xu, R. (2026) · Bioresources and Bioprocessing · doi:10.1186/s40643-026-01144-y
- Authors
- Almeida, J., Craveiro, R., Faria, P., Silva, A. S., Mateus, E. P., Barreiros, S., Paiva, A., & Ribeiro, A. B.
- Affiliations
- Civil Engineering Research and Innovation for Sustainability (PT)
- LAQV Requimte (PT)
- Universidade Nova de Lisboa (PT)
- National Laboratory for Civil Engineering (PT)
- Corresponding author
- Almeida, J.
- Ribeiro, A.B.
- Venue
- Science of The Total Environment
- Publisher
- Elsevier BV
- Published
- 2020-03
- Volume
- 710
- Pages
- 136364
- ISSN
- 0048-9697 (ISSN-L)
- OpenAlex
- W2998002466
- Cited by
- 65
- References
- 37
- Citations by year
- 2026: 12 · 2025: 9 · 2024: 4 · 2023: 6 · 2022: 11 · 2021: 14 · 2020: 9
- FWCI
- 3.06
- Type
- journal article
- Language
- en
- Open access
- bronze
- doi.org
- Licence
- Locations
- The Science of The Total Environment (publishedVersion)
- PubMed (publishedVersion)
- arXiv (Cornell University) (submittedVersion)
- Portuguese National Funding Agency for Science, Research and Technology (RCAAP Project by FCT) (submittedVersion, other-oa)
- Repositório Cientifico do LNEC (submittedVersion)
- arXiv (Cornell University)
- Funders
- Horizon 2020 (778045)
- FCT
- MCTES (UID/AMB/04085/2019)
- Associate Laboratory for Green Chemistry (UID/QUI/50006/2019)
- Topics
- Physical Sciences › Engineering › Electrical and Electronic Engineering › Electrokinetic Soil Remediation Techniques
- Physical Sciences › Engineering › Mechanical Engineering › Extraction and Separation Processes
- Physical Sciences › Environmental Science › Environmental Chemistry › Mine drainage and remediation techniques
- Keywords
- electrodialysis, deep eutectic solvents, tungsten recovery, arsenic removal, mine tailings, choline chloride, malonic acid, oxalic acid, electromigration, critical raw materials, circular economy, Panasqueira mine
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