Mixed 1T–2H Phase MoS2/Reduced Graphene Oxide as Active Electrode for Enhanced Supercapacitive Performance

Gigot, Arnaud; Fontana, Marco; Serrapede, Mara; Castellino, Micaela; Bianco, Stefano; Armandi, Marco; Bonelli, Barbara; Pirri, Candido Fabrizio; Tresso, Elena; Rivolo, Paola

doi:10.1021/acsami.6b11290

Cited by 164Supercapacitor Materials and FabricationMXene and MAX Phase MaterialsElectrocatalysts for Energy Conversion

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Mixed 1T–2H Phase MoS2/Reduced Graphene Oxide as Active Electrode for Enhanced Supercapacitive Performance

Gigot, Arnaud, Fontana, Marco, Serrapede, Mara, Castellino, Micaela, Bianco, Stefano, Armandi, Marco, Bonelli, Barbara, Pirri, Candido Fabrizio, Tresso, Elena, Rivolo, Paola·2016·ACS Applied Materials & Interfaces

DOI 10.1021/acsami.6b11290

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Abstract

A hybrid aerogel, composed of MoS 2 sheets of 1T (distorted octahedral) and 2H (trigonal prismatic) phases, finely mixed with few layers of reduced graphene oxide (rGO) and obtained by means of a facile environment-friendly hydrothermal cosynthesis, is proposed as electrode material for supercapacitors. By electrochemical characterizations in three- and two-electrode configurations and symmetric planar devices, unique results have been obtained, with specific capacitance values up to 416 F g -1 and a highly stable capacitance behavior over 50000 charge-discharge cycles. The in-depth morphological and structural characterizations through field emission scanning electron microscopy, Raman, X-ray photoelectron spectroscopy, X-ray diffraction, Brunauer-Emmett-Teller, and transmission electron microscopy analysis provides the proofs of the unique assembly of such 3D structured matrix. The unpacked MoS 2 structure exhibits an excellent distribution of 1T and 2H phase sheets that are highly exposed to interaction with the electrolyte, and so available for surface/near-surface redox reactions, notwithstanding the quite low overall content of MoS 2 embedded in the reduced graphene oxide (rGO) matrix. A comparison with other "more conventional" hybrid rGO-MoX 2 electrochemically active materials, synthesized in the same conditions, is provided to support the outstanding behavior of the cosynthesized rGO-MoS 2 .

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Graphene-based nanocomposites have the potential to ameliorate energy storage devices by leveraging the ample specific surface area of graphene and Faradaic redox reactions of TMDs or LDHs.
“Such graphene-based nanocomposites have the potential to ameliorate energy storage devices by leveraging the ample specific surface area of graphene and Faradaic redox reactions of TMDs or LDHs.27−32”
From Integrated Energy Aerogel of N,S-rGO/WSe 2 /NiFe-LDH for Both Energy Conversion and Storage (2017) · cites this paper as [27]

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Authors: Gigot, A., Fontana, M., Serrapede, M., Castellino, M., Bianco, S., Armandi, M., Bonelli, B., Pirri, C. F., Tresso, E., & Rivolo, P.
Affiliations: Politecnico di Torino (IT)
Italian Institute of Technology (IT)
Corresponding author: Rivolo, Paola
ORCID: Fontana, Marco
Serrapede, Mara
Castellino, Micaela
Bianco, Stefano
Armandi, Marco
Bonelli, Barbara
Pirri, Candido Fabrizio
Tresso, Elena
Rivolo, Paola
Venue: ACS Applied Materials & Interfaces
Publisher: American Chemical Society (ACS)
Published: 2016-11-21
Volume: 8
Issue: 48
Pages: 32842-32852
ISSN: 1944-8244 (ISSN-L)
1944-8252
DOI: 10.1021/acsami.6b11290
OpenAlex: W2553462613
Cited by: 164
References: 54
Citations by year: 2026: 9 · 2025: 14 · 2024: 14 · 2023: 17 · 2022: 19 · 2021: 10 · 2020: 25 · 2019: 19 · 2018: 30 · 2017: 7
FWCI: 5.87
Type: journal article
Language: en
Open access: closed
Locations: ACS Applied Materials & Interfaces (publishedVersion)
PubMed (publishedVersion)
PORTO@Iris (submittedVersion)
PORTO Publications Open Repository TOrino (Politecnico di Torino) (submittedVersion)
Topics: Physical Sciences › Materials Science › Electronic, Optical and Magnetic Materials › Supercapacitor Materials and Fabrication
Physical Sciences › Materials Science › Materials Chemistry › MXene and MAX Phase Materials
Physical Sciences › Energy › Renewable Energy, Sustainability and the Environment › Electrocatalysts for Energy Conversion
Keywords: MoS2, reduced graphene oxide, supercapacitor electrodes, hybrid aerogels, specific capacitance, cycling stability, MoS2/rGO composite

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Mixed 1T–2H Phase MoS2/Reduced Graphene Oxide as Active Electrode for Enhanced Supercapacitive Performance

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