Silicon-29 NMR study of dehydrated/rehydrated silica gel using cross polarization and magic-angle spinning
Abstract
ADVERTISEMENT RETURN TO ISSUEPREVArticleNEXTSilicon-29 NMR study of dehydrated/rehydrated silica gel using cross polarization and magic-angle spinningDean W. Sindorf and Gary E. MacielCite this: J. Am. Chem. Soc. 1983, 105, 6, 1487–1493Publication Date (Print):March 1, 1983Publication History Published online1 May 2002Published inissue 1 March 1983https://pubs.acs.org/doi/10.1021/ja00344a012https://doi.org/10.1021/ja00344a012research-articleACS PublicationsRequest reuse permissionsArticle Views1706Altmetric-Citations346LEARN ABOUT THESE METRICSArticle Views are the COUNTER-compliant sum of full text article downloads since November 2008 (both PDF and HTML) across all institutions and individuals. These metrics are regularly updated to reflect usage leading up to the last few days.Citations are the number of other articles citing this article, calculated by Crossref and updated daily. Find more information about Crossref citation counts.The Altmetric Attention Score is a quantitative measure of the attention that a research article has received online. Clicking on the donut icon will load a page at altmetric.com with additional details about the score and the social media presence for the given article. Find more information on the Altmetric Attention Score and how the score is calculated. Share Add toView InAdd Full Text with ReferenceAdd Description ExportRISCitationCitation and abstractCitation and referencesMore Options Share onFacebookTwitterWechatLinked InRedditEmail Other access optionsGet e-Alertsclose Get e-Alerts
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The breadth and chemical shifts of additional peaks in 29Si CP NMR are consistent with formation of an amorphous silicate phase.
“The breadth of additional peaks and their chemical shifts are consistent with the formation of an amorphous silicate phase [5, 29, 30].”
From Mechanochemical formation of highly stable amorphous calcium carbonate in calcium silicates: Potential long-term storage of CO2 in cement (2024) · cites this paper as [30]
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- Authors
- Sindorf, D. W., & Maciel, G. E.
- Venue
- Journal of the American Chemical Society
- Publisher
- American Chemical Society (ACS)
- Published
- 1983-03
- Volume
- 105
- Issue
- 6
- Pages
- 1487-1493
- ISSN
- 0002-7863 (ISSN-L)
- 1520-5126
- OpenAlex
- W2072302124
- Cited by
- 398
- References
- 0
- Citations by year
- 2026: 3 · 2025: 2 · 2024: 2 · 2023: 5 · 2022: 6 · 2021: 3 · 2020: 4 · 2019: 9 · 2018: 10 · 2017: 6 · 2016: 8 · 2015: 9 · 2014: 12 · 2013: 10 · 2012: 15
- FWCI
- 5.23
- Type
- journal article
- Language
- en
- Open access
- closed
- Locations
- Journal of the American Chemical Society (publishedVersion)
- Topics
- Physical Sciences › Chemistry › Spectroscopy › Advanced NMR Techniques and Applications
- Physical Sciences › Physics and Astronomy › Nuclear and High Energy Physics › NMR spectroscopy and applications
- Physical Sciences › Chemistry › Inorganic Chemistry › Zeolite Catalysis and Synthesis
- Keywords
- silica gel, rehydration, 29Si NMR, cross-polarization, magic angle spinning, silanol groups, surface hydroxyl groups
About these checks
Registry, retraction, Cites and statistics results are computed, not judged, with one exception: a printed reference that no index lists is read once by a model before it counts as a citation error. Claims are extracted by a model and kept only when their quote appears verbatim in the text; each cited source is then checked, with a model’s help, for whether it says what the claim relies on. Those verdicts can be wrong — read the claim’s quote and the cited source before relying on one.
Statistics and arithmetic are recomputed, not judged.
Confidence bands are shown only for fields calibrated on our annotated test set. None is calibrated yet, so no band is shown.
What counts as a claim ›How we measure confidence ›How we check this ›
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