The DOI matches its Crossref record; 4 of the 4 references it cites were found in a registry or an index.
Nonhydrolytic Synthesis of High-Quality Anisotropically Shaped Brookite TiO2 Nanocrystals
Open accessAbstract
A surfactant-assisted nonaqueous strategy, relying on high-temperature aminolysis of titanium carboxylate complexes, has been developed to access anisotropically shaped TiO2 nanocrystals selectively trapped in the metastable brookite phase. Judicious temporal manipulation of precursor supply to the reaction mixture enables systematic tuning of the nanostructure geometric features over an exceptionally wide dimensional range (30-200 nm). Such degree of control is rationalized within the frame of a self-regulated phase-changing seed-catalyzed mechanism, in which homogeneous nucleation, on one side, and heterogeneous nucleation/growth processes, on the other side, are properly balanced while switching from the anatase to the brookite structures, respectively, in a continuous unidirectional crystal development regime. The time variation of the chemical potential for the monomer species in the solution, the size dependence of thermodynamic structural stability of the involved titania polymorphs, and the reduced activation barrier for brookite nucleation onto initially formed anatase seeds play decisive roles in the crystal-phase- and shape-tailored growth of titania nanostructures by the present approach.
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Citations
Cites
Surface Science Studies of the Photoactivation of TiO 2 New Photochemical Processes
Thompson, T. L., & Yates, J. T. (2006) · Chemical Reviews · doi:10.1021/cr050172k · Cited by 2,064
Nonaqueous sol–gel routes to metal oxide nanoparticles
Niederberger, M. (2007) · Accounts of Chemical Research · doi:10.1021/ar600035e · Cited by 761
Synthesis of TiO2 Nanocrystals by Nonhydrolytic Solution-Based Reactions
Trentler, T. J., Denler, T. E., Bertone, J. F., Agrawal, A., & Colvin, V. L. (1999) · Journal of the American Chemical Society · doi:10.1021/ja983361b · Cited by 382
Aminolysis Route to Monodisperse Titania Nanorods with Tunable Aspect Ratio
Zhang, Z., Zhong, X., Liu, S., Li, D., & Han, M. (2005) · Angewandte Chemie International Edition · doi:10.1002/anie.200500410 · Cited by 236
Cited by
Han, X., Kuang, Q., Jin, M., Xie, Z., & Zheng, L. (2009) · Journal of the American Chemical Society · doi:10.1021/ja8092373 · Cited by 1,636
Facet Effect of Single-Crystalline Ag3PO4 Sub-microcrystals on Photocatalytic Properties
Bi, Y., Ouyang, S., Umezawa, N., Cao, J., & Ye, J. (2011) · Journal of the American Chemical Society · doi:10.1021/ja2002132 · Cited by 1,316
Titanium Dioxide Crystals with Tailored Facets
Liu, G., Yang, H. G., Pan, J., Yang, Y. Q., Lu, G. Q. (., & Cheng, H.-M. (2014) · Chemical Reviews · doi:10.1021/cr400621z · Cited by 1,084
Liu, L., Zhao, H., Andino, J. M., & Li, Y. (2012) · ACS Catalysis · doi:10.1021/cs300273q · Cited by 870
Colloidal heterostructured nanocrystals: Synthesis and growth mechanisms
Carbone, L., & Cozzoli, P. D. (2010) · Nano Today · doi:10.1016/j.nantod.2010.08.006 · Cited by 691
Self-citationZhao, Y., Wang, L. P., Sougrati, M. T., Feng, Z., Leconte, Y., Fisher, A., Srinivasan, M., & Xu, Z. (2017) · Advanced Energy Materials · doi:10.1002/aenm.201601424 · Cited by 586
Solution-Phase Synthesis of Titanium Dioxide Nanoparticles and Nanocrystals
Cargnello, M., Gordon, T. R., & Murray, C. B. (2014) · Chemical Reviews · doi:10.1021/cr500170p · Cited by 406
Nonaqueous Chemistry of Group 4 Oxo Clusters and Colloidal Metal Oxide Nanocrystals
Van den Eynden, D., Pokratath, R., & De Roo, J. (2022) · Chemical Reviews · doi:10.1021/acs.chemrev.1c01008 · Cited by 83
Metadata
- Authors
- Buonsanti, R., Grillo, V., Carlino, E., Giannini, C., Kipp, T., Cingolani, R., & Cozzoli, P. D.
- Venue
- Journal of the American Chemical Society
- Publisher
- American Chemical Society (ACS)
- Published
- 2008-07-23
- Volume
- 130
- Issue
- 33
- Pages
- 11223-11233
- ISSN
- 0002-7863 (ISSN-L)
- 1520-5126
- OpenAlex
- W2023248380
- Cited by
- 252
- References
- 4
- FWCI
- 10.56
- Type
- journal article
- Language
- en
- Open access
- green
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