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Ordered Mesoporous Alumina-Supported Metal Oxides
Abstract
The one-pot synthesis of alumina-supported metal oxides via self-assembly of a metal precursor and aluminum isopropoxide in the presence of triblock copolymer (as a structure directing agent) is described in detail for nickel oxide. The resulting mesoporous mixed metal oxides possess p6 mm hexagonal symmetry, well-developed mesoporosity, relatively high BET surface area, large pore widths, and crystalline pore walls. In comparison to pure alumina, nickel aluminum oxide samples exhibited larger mesopores and improved thermal stability. Also, long-range ordering of the aforementioned samples was observed for nickel molar percentages as high as 20%. The generality of the recipe used for the synthesis of mesoporous nickel aluminum oxide was demonstrated by preparation of other alumina-supported metal oxides such as MgO, CaO, TiO 2, and Cr 2O 3. This method represents an important step toward the facile and reproducible synthesis of ordered mesoporous alumina-supported materials for various applications where large and accessible pores with high loading of catalytically active metal oxides are needed.
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Cites
Generalized syntheses of large-pore mesoporous metal oxides with semicrystalline frameworks
Yang, P., Zhao, D., Margolese, D. I., Chmelka, B. F., & Stucky, G. D. (1998) · Nature · doi:10.1038/24132 · Cited by 2,493
What is a green solvent? A comprehensive framework for the environmental assessment of solvents
Capello, C., Fischer, U., & Hungerbühler, K. (2007) · Green Chemistry · doi:10.1039/b617536h · Cited by 1,917
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Synthesis of non-siliceous mesoporous oxides
Gu, D., & Schüth, F. (2014) · Chem. Soc. Rev. · doi:10.1039/c3cs60155b · Cited by 584
Large-pore ordered mesoporous materials templated from non-pluronic amphiphilic block copolymers
Deng, Y., Wei, J., Sun, Z., & Zhao, D. (2013) · Chem. Soc. Rev. · doi:10.1039/c2cs35426h · Cited by 447
Ma, J., Ren, Y., Zhou, X., Liu, L., Zhu, Y., Cheng, X., Xu, P., Li, X., Deng, Y., & Zhao, D. (2018) · Advanced Functional Materials · doi:10.1002/adfm.201705268 · Cited by 351
Marinho, A. L. A., Toniolo, F. S., Noronha, F. B., Epron, F., Duprez, D., & Bion, N. (2021) · Applied Catalysis B: Environmental · doi:10.1016/j.apcatb.2020.119459 · Cited by 257
Metadata
- Authors
- Morris, S. M., Fulvio, P. F., & Jaroniec, M.
- Venue
- Journal of the American Chemical Society
- Publisher
- American Chemical Society (ACS)
- Published
- 2008-10-16
- Volume
- 130
- Issue
- 45
- Pages
- 15210-15216
- ISSN
- 0002-7863 (ISSN-L)
- 1520-5126
- OpenAlex
- W2010578002
- Cited by
- 384
- References
- 2
- FWCI
- 7.92
- Type
- journal article
- Language
- en
- Open access
- closed
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- Morris, S. M., Fulvio, P. F., & Jaroniec, M. (2008). Ordered Mesoporous Alumina-Supported Metal Oxides. Journal of the American Chemical Society. https://doi.org/10.1021/ja806429q
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