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Nanocrystalline Zeolites and Zeolite Structures: Synthesis, Characterization, and Applications
Abstract
Nanocrystalline zeolites are porous nanomaterials with crystal sizes of less than 100 nm that possess unique external and internal surface reactivity. Nanocrystalline zeolites, such as silicalite, ZSM-5 and Y, were synthesized and extensively characterized by powder X-ray diffraction, nitrogen adsorption isotherms, dynamic light scattering, and electron microscopy. Spectroscopic characterization of the nanocrystalline zeolites by FTIR and solid-state NMR provided detailed structural information about internal and external surface sites. The nanocrystalline zeolites were also used as building blocks to form larger, hollow zeolite structures with encapsulated metal or organic species. The surface properties of nanocrystalline zeolites and hollow zeolite structures were tailored through functionalization of surface silanol groups. Applications of nanocrystalline zeolites and zeolite structures in the selective catalytic reduction of NO x and the photoreduction of Cr(VI) to Cr(III) in aqueous solution were investigated. The unique properties and reactivity of nanocrystalline zeolites and the potential for future applications of these materials will also be discussed.
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Cites
Characterization of nanocrystalline zeolite Beta
Camblor, M. A., Corma, A., & Valencia, S. (1998) · Microporous and Mesoporous Materials · doi:10.1016/s1387-1811(98)00172-3 · Cited by 456
Cited by
Template-free nanosized faujasite-type zeolites
Awala, H., Gilson, J.-P., Retoux, R., Boullay, P., Goupil, J.-M., Valtchev, V., & Mintova, S. (2015) · Nature Materials · doi:10.1038/nmat4173 · Cited by 484
Heavy metal adsorption with zeolites: The role of hierarchical pore architecture
Hong, M., Yu, L., Wang, Y., Zhang, J., Chen, Z., Dong, L., Zan, Q., & Li, R. (2019) · Chemical Engineering Journal · doi:10.1016/j.cej.2018.11.087 · Cited by 452
Insight into CO2 methanation mechanism over NiUSY zeolites: An operando IR study
Westermann, A., Azambre, B., Bacariza, M. C., Graça, I., Ribeiro, M. F., Lopes, J. M., & Henriques, C. (2015) · Applied Catalysis B: Environment and Energy · doi:10.1016/j.apcatb.2015.02.026 · Cited by 288
Porous Organic Cage Nanocrystals by Solution Mixing
Hasell, T., Chong, S. Y., Jelfs, K. E., Adams, D. J., & Cooper, A. I. (2012) · Journal of the American Chemical Society · doi:10.1021/ja209156v · Cited by 273
Metadata
- Authors
- Larsen, S. C.
- Venue
- The Journal of Physical Chemistry C
- Publisher
- American Chemical Society (ACS)
- Published
- 2007-11-07
- Volume
- 111
- Issue
- 50
- Pages
- 18464-18474
- ISSN
- 1932-7447 (ISSN-L)
- 1932-7455
- OpenAlex
- W2012847073
- Cited by
- 323
- References
- 1
- FWCI
- 10.75
- Type
- journal article
- Language
- en
- Open access
- closed
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- Larsen, S. C. (2007). Nanocrystalline Zeolites and Zeolite Structures: Synthesis, Characterization, and Applications. The Journal of Physical Chemistry C. https://doi.org/10.1021/jp074980m
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Contains information from the Semantic Scholar Academic Graph Datasets, made available under the ODC Attribution License (ODC-BY 1.0).
Semantic Scholar’s data is described in: Kinney, R., et al. (2023). The Semantic Scholar Open Data Platform. arXiv:2301.10140.
