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Facile synthesis of MOF-177 by a sonochemical method using 1-methyl-2-pyrrolidinone as a solvent
Abstract
High quality MOF-177 crystals in the size range of 5-20 microm were successfully synthesized via a sonochemical route in a substantially reduced synthesis time (40 min) in the presence of low-cost NMP (1-methyl-2-pyrrolidone) as a solvent. Microwave heating in NMP also produced MOF-177 under similar conditions (35 min, 5-50 microm) but exhibited inferior crystallinity. In comparison, a conventional solvothermal route in DEF (diethylformamide) took 48 h to produce MOF-177 crystals 0.5-1.5 mm in size. The BET surface areas of the MOF-177 samples decreased in the order of sonochemical (4898 m(2) g(-1)) > conventional (4833 m(2) g(-1)) > microwave route (4197 m(2) g(-1)). In line with this trend, MOF-177 prepared via the sonochemical route resulted in the highest CO(2) adsorption capacity, 1315 mg g(-1) at 30 bar and 298 K. The product yield of MOF-177 synthesized via the sonochemical route was 95.6%, and was significantly higher than the product yields of other methods.
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Millward, A. R., & Yaghi, O. M. (2005) · Journal of the American Chemical Society · doi:10.1021/ja0570032 · Cited by 2,876
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Kaur, H., Devi, N., Siwal, S. S., Alsanie, W. F., Thakur, M. K., & Thakur, V. K. (2023) · ACS Omega · doi:10.1021/acsomega.2c07719 · Cited by 273
Abdi, J., Sisi, A. J., Hadipoor, M., & Khataee, A. (2022) · Journal of Hazardous Materials · doi:10.1016/j.jhazmat.2021.127558 · Cited by 144
Aerogels and metal–organic frameworks for environmental remediation and energy production
Kumar, A., Rana, A., Sharma, G., Sharma, S., Naushad, M., Mola, G. T., Dhiman, P., & Stadler, F. J. (2018) · Environmental Chemistry Letters · doi:10.1007/s10311-018-0723-x · Cited by 75
Metadata
- Authors
- Jung, D.-W., Yang, D.-A., Kim, J., Kim, J., & Ahn, W.-S.
- Venue
- Dalton Transactions
- Publisher
- Royal Society of Chemistry (RSC)
- Published
- 2010
- Volume
- 39
- Issue
- 11
- Pages
- 2883
- ISSN
- 1477-9226 (ISSN-L)
- 1477-9234
- OpenAlex
- W2170515159
- Cited by
- 264
- References
- 1
- FWCI
- 6.41
- Type
- journal article
- Language
- en
- Open access
- closed
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- Jung, D.-W., Yang, D.-A., Kim, J., Kim, J., & Ahn, W.-S. (2010). Facile synthesis of MOF-177 by a sonochemical method using 1-methyl-2-pyrrolidinone as a solvent. Dalton Transactions. https://doi.org/10.1039/b925088c
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