Cited by 393Electrocatalysts for Energy ConversionCO2 Reduction Techniques and CatalystsAdvanced Photocatalysis Techniques

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Enhanced electrocatalytic activity for hydrogen evolution reaction from self-assembled monodispersed molybdenum sulfidenanoparticles on an Au electrode

Wang, Tanyuan, Liu, Lu, Zhu, Zhiwei, Papakonstantinou, Pagona, Hu, Jingbo, Liu, Hongyun, Li, Meixian·2013·Energy Environ. Sci.

DOI 10.1039/c2ee23513g

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Abstract

Ultrasmall molybdenum sulfide nanoparticles with diameters of 1.47 ± 0.16 nm were fabricated from bulk MoS2 by a combination of ultrasonication and centrifugation. The nanoparticles were then assembled on an Au surface to form a film with high electrocatalytic activity for hydrogen evolution reaction (HER). A Tafel slope of 69 mV per decade was measured for this film and the onset potential was estimated to be −0.09 V. The small loading (1.03 μg cm−2) and the high current density (0.92 mA cm−2 at η = 0.15 V) demonstrated extremely high catalytic efficiency. X-ray photoelectron spectroscopic results revealed that the assembled nanoparticle film was sulfur enriched with abundant S edges and a structural rearrangement of the S rich particles might occur during the self-assembly process, resulting in significantly enhanced electrocatalytic activity for HER. Electrochemical impedance measurements suggested that the assembling process optimized the conductivity of the nanoparticle film, which contributed to the enhanced HER catalytic activity. Our research has provided a new way to synthesize active molybdenum sulfide nanoparticles for HER and a new approach to achieve enrichment of S edges on molybdenum sulfide, which might have potential use not only for electrocatalytic HER, but also for photoelectrocatalytic HER and plasmon-enhanced water splitting.

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Authors: Wang, T., Liu, L., Zhu, Z., Papakonstantinou, P., Hu, J., Liu, H., & Li, M.
Affiliations: Peking University (CN)
University of Ulster (GB)
Beijing Normal University (CN)
Corresponding author: Li, Meixian
ORCID: Wang, Tanyuan
Liu, Lu
Zhu, Zhiwei
Papakonstantinou, Pagona
Hu, Jingbo
Liu, Hongyun
Li, Meixian
Venue: Energy Environ. Sci.
Publisher: Royal Society of Chemistry (RSC)
Published: 2013
Volume: 6
Issue: 2
Pages: 625-633
ISSN: 1754-5692 (ISSN-L)
1754-5706
DOI: 10.1039/c2ee23513g
OpenAlex: W1991875973
Cited by: 393
References: 27
Citations by year: 2026: 2 · 2025: 13 · 2024: 12 · 2023: 13 · 2022: 17 · 2021: 25 · 2020: 33 · 2019: 32 · 2018: 34 · 2017: 58 · 2016: 47 · 2015: 47 · 2014: 39 · 2013: 21
FWCI: 13.12
Type: journal article
Language: en
Open access: closed
Locations: Energy & Environmental Science (publishedVersion)
Funders: National Natural Science Foundation of China
Topics: Physical Sciences › Energy › Renewable Energy, Sustainability and the Environment › Electrocatalysts for Energy Conversion
Physical Sciences › Energy › Renewable Energy, Sustainability and the Environment › CO2 Reduction Techniques and Catalysts
Physical Sciences › Energy › Renewable Energy, Sustainability and the Environment › Advanced Photocatalysis Techniques
Keywords: hydrogen evolution reaction, electrocatalysis, self-assembly, gold electrode, sonochemical synthesis, water splitting, photoelectrocatalysis

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Enhanced electrocatalytic activity for hydrogen evolution reaction from self-assembled monodispersed molybdenum sulfidenanoparticles on an Au electrode

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