Ultrasonic-assisted synthesis and characterization of layered double hydroxides intercalated with bioactive N,N′-(pyromellitoyl)-bis-l-α-amino acids
Abstract
In this study Mg/Al layered double hydroxides (LDHs) and organo-modified chiral LDHs were synthesized in one step under green conditions. Co-precipitation reaction of the Al(NO3)3·9H2O, Mg(NO3)2·6H2O and different biocompatible N,N-(pyromellitoyl)-bis-L-amino acids was carried out in aqueous solution in a short time by an ultrasonic technique. Field emission scanning electron microscopy and transmission electron microscopy techniques showed that the resulting products have good crystallinity and uniform morphology. The presence of the bioactive surfactants in the interlayer space of LDH was confirmed by Fourier transform infrared spectroscopy, X-ray diffraction (XRD) and thermogravimetry analysis techniques. As expected, the positions of the basal reflections in the XRD patterns of modified samples are shifted to higher d value indicating the expansion of the interlayer distance. Thermal properties were investigated by the thermogravimetric analysis technique.
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The modified wood possesses improved thermal and mechanical properties and dimensional stability with increasing load of inorganic TiO2 gels, as ultrasonic treatment facilitates chemical reactions between liquid and solid phases.
“The modified wood possesses improved the thermal and mechanical properties and dimensional stability with increasing load of inorganic TiO 2 gels, as ultrasonic treatment facilitates chemical reactions between liquid and solid phases 88,89”
From Sustainable hybrid photocatalysts: titania immobilized on carbon materials derived from renewable and biodegradable resources (2016) · cites this paper as [89]
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- Authors
- Mallakpour, S., Dinari, M., & Behranvand, V.
- Affiliations
- Isfahan University of Technology (IR)
- Corresponding author
- Mallakpour, Shadpour
- Venue
- RSC Advances
- Publisher
- Royal Society of Chemistry (RSC)
- Published
- 2013
- Volume
- 3
- Issue
- 45
- Pages
- 23303
- ISSN
- 2046-2069 (ISSN-L)
- OpenAlex
- W1969292702
- Cited by
- 55
- References
- 28
- Citations by year
- 2025: 2 · 2022: 3 · 2021: 5 · 2020: 5 · 2019: 7 · 2018: 1 · 2017: 9 · 2016: 7 · 2015: 9 · 2014: 7
- FWCI
- 3.46
- Type
- journal article
- Language
- en
- Open access
- closed
- Locations
- RSC Advances (publishedVersion)
- Funders
- Iran Nanotechnology Initiative Council
- Isfahan University of Technology
- Topics
- Physical Sciences › Materials Science › Materials Chemistry › Layered Double Hydroxides Synthesis and Applications
- Physical Sciences › Materials Science › Biomaterials › Clay minerals and soil interactions
- Physical Sciences › Environmental Science › Waste Management and Disposal › Chemical Synthesis and Characterization
- Keywords
- layered double hydroxides, Mg-Al layered double hydroxide, sonochemical synthesis, chiral amino acids, intercalation, interlayer spacing expansion, co-precipitation, green synthesis, thermal stability
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