Bottom-up fabrication of two-dimensional carbon nitride and highly sensitive electrochemical sensors for mercuric ions

Sadhukhan, Mriganka; Barman, Sudip

doi:10.1039/c3ta01523h

Cited by 144Carbon and Quantum Dots ApplicationsElectrochemical Analysis and ApplicationsElectrochemical sensors and biosensors

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Bottom-up fabrication of two-dimensional carbon nitride and highly sensitive electrochemical sensors for mercuric ions

Sadhukhan, Mriganka, Barman, Sudip·2013·Journal of Materials Chemistry A

DOI 10.1039/c3ta01523h

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Abstract

We report microwave assisted bottom-up fabrication of flat two-dimensional carbon nitride from formamide (HCONH2). Microwave irradiation of HCONH2 produces carbon nitride dots (CNDs) which are used as precursors for synthesis of carbon nitride (C3N4). The two-dimensional (2D) carbon nitride sheets are formed by evaporation induced self-assembly and condensation of CNDs on a solid substrate. The drying of CND solution generates different morphologies such as 0D carbon nitride quantum dots, 2D carbon nitride sheets and 3D carbon nitride, depending on the concentration of CNDs. The carbon nitrides are well characterized by TEM, AFM, SEM, XRD, XPS, FT-IR, FT-Raman Spectroscopy and TGA, CHN analysis. In addition, the C3N4 modified glassy carbon electrode can be used as a highly sensitive electrochemical sensor for mercuric ions in aqueous solution. The lower detection limit of Hg2+ is found to be 9.1 × 10−11 M, which is far below the WHO guideline for drinking water (10−8 M). The simultaneous electrochemical detection of Pb2+, Cu2+ and Hg2+ using a C3N4 modified GC electrode is also described.

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p-XRD peak at 2θ 27.30 corresponds to (002) plane of g-CNx with interlayer d-spacing 3.27 Å.
“Peak positioned at 2θ value of 27.30 corresponds to (002) plane of g-CNx with interlayer d-spacing 3.27Å which was reported previously by our group52, 53.”
From Gold aerogel supported on graphitic carbon nitride: an efficient electrocatalyst for oxygen reduction reaction and hydrogen evolution reaction (2015) · cites this paper as [53]

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Authors: Sadhukhan, M., & Barman, S.
Affiliations: National Institute of Science Education and Research (IN)
Corresponding author: Barman, Sudip
ORCID: Sadhukhan, Mriganka
Barman, Sudip
Venue: Journal of Materials Chemistry A
Publisher: Royal Society of Chemistry (RSC)
Published: 2013
Volume: 1
Issue: 8
Pages: 2752
ISSN: 2050-7488 (ISSN-L)
2050-7496
DOI: 10.1039/c3ta01523h
OpenAlex: W2046216572
Cited by: 144
References: 34
Citations by year: 2026: 4 · 2025: 5 · 2024: 5 · 2023: 9 · 2022: 13 · 2021: 10 · 2020: 12 · 2019: 16 · 2018: 14 · 2017: 12 · 2016: 13 · 2015: 13 · 2014: 15 · 2013: 3
FWCI: 6.61
Type: journal article
Language: en
Open access: closed
Locations: Journal of Materials Chemistry A (publishedVersion)
Funders: Department of Science and Technology, Ministry of Science and Technology, India
Topics: Physical Sciences › Materials Science › Materials Chemistry › Carbon and Quantum Dots Applications
Physical Sciences › Chemistry › Electrochemistry › Electrochemical Analysis and Applications
Physical Sciences › Chemistry › Analytical Chemistry › Electrochemical sensors and biosensors
Keywords: two-dimensional carbon nitride, C3N4, formamide, microwave-assisted synthesis, bottom-up fabrication, carbon nitride quantum dots, evaporation-induced self-assembly, modified glassy carbon electrode, electrochemical sensor, mercury ion detection, heavy metal detection, lead ion detection, Cu2+ detection, drinking water

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Bottom-up fabrication of two-dimensional carbon nitride and highly sensitive electrochemical sensors for mercuric ions

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