Fe 3 O 4 nanoparticles and ultrasound assisted dispersive liquid–liquid microextraction of lead( ii ) for its microsampling flame atomic absorption spectrometric determination in food and environmental samples
Abstract
A method for the isolation of lead from aqueous samples as a Chicago sky blue 6B chelate, based on the combination of Fe 3 O 4 nanoparticles and ultrasound assisted dispersive liquid–liquid microextraction (NPU-DLLME) prior to flame atomic absorption spectrometry, was developed.
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The LOD of 0.008 μg L−1 for the developed DES-ME was between those of other microextraction methods.
“The limits of detection of 0.008 µg L−1 for the developed DES-ME were between those of the other methods, as shown in Table 5.”
From Deep Eutectic Solvent-Based Microextraction of Lead(II) Traces from Water and Aqueous Extracts before FAAS Measurements (2020) · cites this paper as [23]
The separation and extraction of heavy metal ions from a sample solution depends on the pH of the medium due to complexation between metal ions and the ligand.
“The separation and extraction of heavy metal ions from a sample solution depends on the pH of the medium due to the complexation between metal ions and the ligand [23,43].”
From Deep Eutectic Solvent-Based Microextraction of Lead(II) Traces from Water and Aqueous Extracts before FAAS Measurements (2020) · cites this paper as [23]
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Self-citation
- Authors
- Habila, M. A., Alothman, Z. A., & Soylak, M.
- Affiliations
- King Saud University (SA)
- Erciyes University (TR)
- Corresponding author
- Soylak, M.
- Venue
- RSC Adv.
- Publisher
- Royal Society of Chemistry (RSC)
- Published
- 2014
- Volume
- 4
- Issue
- 98
- Pages
- 55610-55614
- ISSN
- 2046-2069 (ISSN-L)
- OpenAlex
- W1976859173
- Cited by
- 18
- References
- 34
- Citations by year
- 2024: 1 · 2023: 2 · 2021: 1 · 2020: 3 · 2018: 2 · 2016: 4 · 2015: 5
- FWCI
- 2.69
- Type
- journal article
- Language
- en
- Open access
- closed
- Locations
- RSC Advances (publishedVersion)
- Funders
- King Saud University
- Topics
- Physical Sciences › Chemistry › Analytical Chemistry › Analytical chemistry methods development
- Physical Sciences › Environmental Science › Water Science and Technology › Environmental and Analytical Chemistry Studies
- Physical Sciences › Chemistry › Spectroscopy › Analytical Chemistry and Chromatography
- Keywords
- Fe3O4 nanoparticles, ultrasound-assisted dispersive liquid-liquid microextraction, lead determination, flame atomic absorption spectrometry, microsampling, food samples, environmental samples, preconcentration
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