Cited by 652Electrocatalysts for Energy ConversionNanomaterials for catalytic reactionsHydrogen Storage and Materials

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Monodispersed nickel phosphide nanocrystals with different phases: synthesis, characterization and electrocatalytic properties for hydrogen evolution

Pan, Yuan, Liu, Yanru, Zhao, Jinchong, Yang, Kang, Liang, Jilei, Liu, Dandan, Hu, Wenhui, Liu, Dapeng, Liu, Yunqi, Liu, Chenguang·2015·Journal of Materials Chemistry A

DOI 10.1039/c4ta04867a

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Abstract

Monodispersed nickel phosphide nanocrystals (NCs) with different phases were successfully synthesized. The Ni 5 P 4 NCs, with a solid structure, exhibited higher catalytic activity than the Ni 12 P 5 and Ni 2 P NCs.

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Synthesis of Ni2P/Ni12P5 composite for a highly efficient hydrogen production from formaldehyde solution
Peng, S.-Q., Wu, L., Huang, M., & Li, Y.-X. (2021) · Reaction Kinetics, Mechanisms and Catalysis · doi:10.1007/s11144-021-01984-z · Cited by 5
“Pan et al. reported that Ni2P and Ni12P5 have similar survey spectrum [34], the Ni 2p peaks (Fig.”
BackgroundInfluential
Mechanistic Study of Monolayer NiP2 (100) toward Solar Hydrogen Production
Hu, J., Zhao, X. Y., Chen, W., Zheng, S., & Chen, Z. (2019) · Solar RRL · doi:10.1002/solr.201900360 · Cited by 8
Electro-catalytic hydrogen evolution and magnetic behavior of N-doped-rGO supported NixPy
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“S3 shows that the major diffraction rings of NixPy indicate the presence of both hexagonal Ni2P with (111) and (211) crystal planes [10, 47] and hexagonal Ni5P4 with (110) crystal plane [48].”
BackgroundInfluential
Unexpected sintering of small supported Ni2P under real feed conditions
Du, Y., Wooler, B., Kliewer, C., Miseo, S., & Soled, S. (2020) · doi:10.1039/c9cy02284h · Cited by 5
Preparation of an Ni5P4/Ni porous composite using a Ni foam as the skeleton and its application in the treatment of large-volume effluent with a high concentration of 4-nitrophenol at room temperature
Liu, X., Dou, X., Li, X.-Q., Qin, L.-X., Han, S., & Kang, S.-Z. (2019) · New Journal of Chemistry · doi:10.1039/c9nj01079c · Cited by 5
Mo-doping directed nanoflower architecture in NiFe phosphide for ultralow-overpotential oxygen evolution catalysis
Li, K., Xiang, J., Ma, X.-X., Wu, J., Tao, Z.-W., Zheng, J.-Q., & Xue, J.-S. (n.d.) · Materials Chemistry and Physics · doi:10.1016/j.matchemphys.2025.131578 · Cited by 5
NiCoP/CoP2 nanoparticles supported on sugarcane bagasse carbon as the electrocatalyst with excellent catalytic performance towards the hydrogen evolution reaction
Qi, P., Jia, Z., Jia, Z., Wang, Y., Wang, Y., Xu, C., Tian, L., & Qi, T. (2024) · International Journal of Hydrogen Energy · doi:10.1016/j.ijhydene.2024.10.012 · Cited by 5
Phase-control synthesis and catalytic property of nickel phosphide nanospheres
Geng, T., Wang, H.-Y., Wu, H., & Zhang, S. (2020) · Journal of nanoparticle research · doi:10.1007/s11051-020-04962-z · Cited by 4
High-entropy NiCoFeMnCrP as anode materials for high-performance lithium-ion batteries
Zhang, F., Zhao, J., Cai, G., & Zhao, H. (2025) · Journal of Physics and Chemistry of Solids · doi:10.1016/j.jpcs.2025.113161 · Cited by 3
Self-citation
Zn-triggered synthesis of NiP/NiP microflower arrays for efficient alkaline overall water splitting
Zhao, Y., Huang, J.-F., Li, X., Cao, L.-Y., Li, J., Chen, Q., Zhang, Y., Kajiyoshi, K., & Feng, L.-L. (2024) · Molecular Catalysis · doi:10.1016/j.mcat.2023.113793 · Cited by 3
Ultrafine Ni 2 P Nanoparticle-Decorated r-GO: A Novel Liquid-Phase Approach and Dibenzothiophene Hydro-desulfurization
Tzitzios, V. K., Pillai, V. V., Gioti, C., Katsiotis, M. S., Karagiannis, T., Gournis, D., Karakassides, M. A., & Alhassan, S. M. (2021) · Industrial & Engineering Chemistry Research · doi:10.1021/acs.iecr.0c05544 · Cited by 3
Hierarchical Ni–Co–O–C–P hollow tetragonal microtubes grown on Ni foam for efficient overall water splitting in alkaline media
Hu, W., Jiang, Q., Wang, L., Hu, S., Huang, Z.-X., Zhou, T.-F., Yang, H.-J., Hu, J.-C., & Tang, N.-F. (2019) · RSC Advances · doi:10.1039/c9ra05165a · Cited by 3
Self-citation
Noble Metal Phosphide Electrocatalysts and Their Synchrotron-based X-ray Absorption Spectroscopy
Zhou, Y., Zhang, Y., & Song, L. (2020) · Journal of Inorganic Materials · doi:10.15541/jim20200224 · Cited by 3
“不同的 M 与 P 的化学计量比会导致明显的结构变化和电子环境的差异,对电催化性能也会产生影响,研究贵金属磷化物的结构对电催化活性的影响有助于指导未来催化剂的设计。通常认为,富磷 TMP 的 HER 性能优于富金属 TMP。例如,Liu 等([80])利用液相的方法制备了一系列单分散的磷化镍纳米晶体, 包括 Ni5P4、Ni2P 和 Ni12P5。测试结果发现,这些纳米晶体对 HER 的电催化活性遵循以下顺序: Ni5P4>Ni2P>Ni12P5。由于 Ni 具有较高的正电荷和较强的 P 聚集效应,富磷 Ni5P4 显示出更好的性能。然而贵金属磷化物催化剂对 HER 显示出不同的规律, 从实验和理论计算结果来看,缺磷…”
Toward Scalable Water Electrolysis Catalysts: Mechanistic Insights, Structure‐Activity Relationships and Multiscale Design
Zeng, K., Liang, X., Hu, R., Zhou, M., Sun, J., Li, S., Tao, H., Li, Y., Hu, H., He, Z., et al. (2026) · Advanced Energy Materials · doi:10.1002/aenm.71510 · Cited by 1
“For instance, Pan and colleagues [ 171 ] successfully synthesized a series of monodispersed nickel phosphides (Ni 12 P 5 , Ni 2 P and Ni 5 P 4 ) through thermal decomposition method.”
Electrodeposited amorphous NiCoP LDH nanocomposites as efficient and affordable catalysts for hydrogen evolution
Abd-Elrahim, A. G., Ali, M. A., & Chun, D. (2026) · International Journal of Hydrogen Energy · doi:10.1016/j.ijhydene.2026.156045 · Cited by 2
Pt/flaky graphite–NiO composite electrocatalyst for the alkaline hydrogen evolution reaction
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Hierarchical nickel phosphide-MXene nanosheets composite as durable electrocatalyst for electrochemical hydrogen production via water-splitting
Mohili, R., Mahabari, K., Patel, M., Jadhav, A. H., Lee, K., & Chaudhari, N. K. (2025) · Nanotechnology · doi:10.1088/1361-6528/ade15d · Cited by 4
“Additionally, satellite peaks at 880.7 and 861.7 eV, associated with Ni 2p 3 / 2 and 2p 1 / 2 , were also present [18].”
Influential
ZSM-23-Supported Nickel Phosphide Catalysts for n-Alkane Hydroisomerization
Bogomolova, T. S., Smirnova, M., Parfenov, M. V., Cherepanova, S., Panafidin, M., Klimov, O., & Noskov, A. S. (2025) · Catalysis Letters · doi:10.1007/s10562-024-04895-5 · Cited by 2
“S5) [28–30].”
Ni phosphide catalysts on Al2O3‐zeolite prepared by phosphidation for methyl palmitate hydroconversion
Shamanaev, I., Vlasova, E., Tsaplin, D. E., Danilova, I., Pakharukova, V., Gerasimov, E., Yakovlev, I., Fedorov, A. Y., Maximov, A., & Bukhtiyarova, G. (2024) · Journal of Chemical Technology & Biotechnology · doi:10.1002/jctb.7766 · Cited by 2
High-capacity, high-rate, and dendrite-free lithium metal anodes based on a 3D mixed electronic-ionic conductive and lithiophilic scaffold
Zhang, T., Sang, Z.-Y., Yin, L., Han, Y., Si, W.-P., Yin, Y., & Hou, F. (2022) · Science China Materials · doi:10.1007/s40843-022-2082-y · Cited by 2
Investigations on the Formation of Transition Metal Phosphides during the Hydrotreating of Light Cycle Oil
Golubeva, M., & Maximov, A. (2021) · Russian journal of applied chemistry · doi:10.1134/s1070427221110082 · Cited by 2
Preparation of Ni 2 P Decorated Black Phosphorus Nanosheets Supported on Two‐Dimensional α‐Zirconium Phosphate and Its Catalysis for Hydrodesulfurization of Dibenzothiophene
Li, J., Ma, H., Wang, J., Luo, X., Yu, L., & Gao, J. (2021) · ChemistrySelect · doi:10.1002/slct.202100701 · Cited by 2
“Even though Ni2P exhibits an extraordinary HDS activity, it is unexpected to bring about some disadvantages: i) Ni2P nanoparticles with a large surface-to-volume ratio, possessing high surface energy, inevitably bond with other atoms resulting in agglomeration [15].”
Background
Improved charge transfer via in situ photodeposition of NixP cocatalyst on g-C3N4 for dye-sensitized photocatalytic H2 Evolution
Xu, J., Han, Z.-Y., Tu, S., Ju, Y., Peng, S.-Q., & Li, Y.-X. (2026) · Materials Science in Semiconductor Processing · doi:10.1016/j.mssp.2026.110523 · Cited by 2
Highly Efficient Electrocatalytic Water Splitting
Liu, M., Lee, L. Y. S., & Wong, K. (2020) · Springer eBooks · doi:10.1007/978-3-030-11155-7_131-1
Transition Metal Phosphide As Cocatalysts for Semiconductor-Based Photocatalytic Hydrogen Evolution Reaction
Zhang, J., Tian, B., Wang, L., Xing, M., & Lei, J. (2018) · Lecture notes in chemistry · doi:10.1007/978-981-13-2113-9_16 · Cited by 3
Ligand Engineering of Colloidal Nanocrystals for Electrocatalysis
Yang, G., Xu, X., Li, Q., & Chen, D. (2026) · Advanced Energy and Sustainability Research · doi:10.1002/aesr.70217 · Cited by 1
Surfactant-Mediated Synthesis of Nickel Oxide Catalysts Combined with Semi-Interpenetrating Network-Type PEMs for Water Electrolyzers
Sharma, V., Mishra, S., Mishra†, S., Hota, A., & Kulshrestha, V. (2026) · ACS Applied Energy Materials · doi:10.1021/acsaem.6c00436 · Cited by 1
Ligand Electronic Properties Dictate Composition of Ni-Based Nanocrystals
Zaza, L., Boulanger, C., Kumar, K., Agrachev, M., Bornet, A., Leemans, J., Jeschke, G., & Buonsanti, R. (2025) · Journal of the American Chemical Society · doi:10.1021/jacs.5c15844 · Cited by 1
Structural insights into thermal behavior and vibrational properties of Ni5P4
Vereshchagin, O., Pankin, D., Gorelova, L. A., Sagatov, N., Khmelnitskaya, M. O., Vlasenko, N. S., Gavryushkin, P., & Britvin, S. (2025) · Materials Chemistry and Physics · doi:10.1016/j.matchemphys.2025.131642 · Cited by 1
Nanocomposite of Graphene–Phosphorene Structures with Cobalt Phosphide as an Effective Electrocatalyst for Hydrogen Evolution in Acidic Medium
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“The high-resolution XPS spectrum P 2 p contains three peaks at 129.5, 130.4, and 133.1 eV, which can be attributed to P 2 p 3/2 , P 2 p 1/2 , and to the oxidized forms of P, which form on the nanocomposite surface under exposure to air [37], respectively.”
Influential
Deposition of Iron, Cobalt, and Nickel Phosphides on the Surface of Highly Porous Silica
Tarasyuk, I. A., Filippov, D. V., & Вашурин, А. С. (2023) · Russian Journal of General Chemistry · doi:10.1134/s1070363223090128 · Cited by 1
CoP/EEBP/N-FLGS Nanocomposite as an Efficient Electrocatalyst of Hydrogen Evolution Reaction in Alkaline Media
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Ultra-Fine Ni2P Nanoparticles Decorated R-GO: Novel Phosphidation Approach and Dibenzothiophene HydrodesulfurizationPreprint
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Indium‐Induced Electronic Structure Engineering of In 3 Ni 2 /NiP x for Alleviating Kinetic Mismatch in Alkaline Hydrogen Evolution
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Nanoconfined Se Anions in 2D CoP/Co2P as High-Performance Bifunctional Electrocatalysts for Efficient H2 Production with Urea-Assisted Alkaline Seawater Electrolysis
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Codoping of phosphorus and nickel enhance electrocatalytic dechlorination performance of Pd-based catalyst
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Self-citation
Electroactive Materials
Samantara, A. K., & Ratha, S. (2019) · SpringerBriefs in materials · doi:10.1007/978-3-030-24861-1_4

Authors: Pan, Y., Liu, Y., Zhao, J., Yang, K., Liang, J., Liu, D., Hu, W., Liu, D., Liu, Y., & Liu, C.
Affiliations: China University of Petroleum, Beijing (CN)
State Key Laboratory of Heavy Oil Processing
Corresponding author: Liu, Yunqi
Liu, Chenguang
ORCID: Pan, Yuan
Liu, Yanru
Zhao, Jinchong
Liang, Jilei
Liu, Dandan
Hu, Wenhui
Liu, Dapeng
Liu, Yunqi
Liu, Chenguang
Venue: Journal of Materials Chemistry A
Publisher: Royal Society of Chemistry (RSC)
Published: 2015
Volume: 3
Issue: 4
Pages: 1656-1665
ISSN: 2050-7488 (ISSN-L)
2050-7496
DOI: 10.1039/c4ta04867a
OpenAlex: W2091075909
Cited by: 652
References: 62
Citations by year: 2026: 17 · 2025: 40 · 2024: 53 · 2023: 48 · 2022: 62 · 2021: 66 · 2020: 86 · 2019: 90 · 2018: 62 · 2017: 61 · 2016: 44 · 2015: 22
FWCI: 14.08
Type: journal article
Language: en
Open access: closed
Locations: Journal of Materials Chemistry A (publishedVersion)
Funders: National Natural Science Foundation of China (21006128)
Topics: Physical Sciences › Energy › Renewable Energy, Sustainability and the Environment › Electrocatalysts for Energy Conversion
Physical Sciences › Chemistry › Organic Chemistry › Nanomaterials for catalytic reactions
Physical Sciences › Materials Science › Materials Chemistry › Hydrogen Storage and Materials
Keywords: nickel phosphide, nanocrystals, monodisperse nanoparticles, phase control, Ni5P4, Ni12P5, hydrogen evolution reaction, electrocatalysis

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Monodispersed nickel phosphide nanocrystals with different phases: synthesis, characterization and electrocatalytic properties for hydrogen evolution

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