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The new small-angle X-ray scattering beamline for materials research at PETRA III: SAXSMAT beamline P62
Open accessAbstract
The SAXSMAT beamline P62 (Small-Angle X-ray Scattering beamline for Materials Research) is a new beamline at the high-energy storage ring PETRA III at DESY. This beamline is dedicated to combined small- and wide-angle X-ray scattering (SAXS/WAXS) techniques for both soft and hard condensed matter systems. It works mainly in transmission geometry. The beamline covers an energy range from 3.5 keV to 35.0 keV, which fulfills the requirements of the user community to perform anomalous scattering experiments. Mirrors are used to reduce the intensity of higher harmonics. Furthermore, the mirrors and 2D compound refracting lenses can focus the beam down to a few micrometres at the sample position. This option with the high photon flux enables also SAXS/WAXS tensor tomography experiments to be performed at this new beamline in a relatively short time. The first SAXS/WAXS pattern was collected in August 2021, while the first user experiment was carried out two months later. Since January 2022 the beamline has been in regular user operation mode. In this paper the beamline optics and the SAXS/WAXS instrument are described and two examples are briefly shown.
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WAXS is a widely established technique for identifying crystallite phases and estimating crystallite sizes even in polymeric materials.
“Nevertheless, WAXS is a widely established technique for identifying crystallite phases 44,45 and estimating crystallite sizes even in polymeric materials.[46][47][48]”
From Correlative characterization of stereocomplex formation in blends of aliphatic polyester P(PCL m - b -PLLA n ) multiblock-copolymers and PDLA (2026) · cites this paper as [45]
In “Examples > SAXS-CT of a phantom sample” (page unavailable), the paper uses WAXS peaks to identify crystalline ZnO and the absence of peaks to distinguish amorphous silica. It does not report estimating crystallite sizes from WAXS, including in polymeric materials; the stated nanoparticle sizes are not WAXS-derived crystallite-size estimates. (LLM, conf=0.84)
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Metadata
- Authors
- Haas, S., Sun, X., Conceição, A. L. C., Horbach, J., & Pfeffer, S.
- Affiliations
- Deutsches Elektronen-Synchrotron DESY (DE)
- Corresponding author
- Haas, S.
- Venue
- Journal of Synchrotron Radiation
- Published
- 2023-10-20
- Volume
- 30
- Issue
- 6
- Pages
- 1156-1167
- ISSN
- 0909-0495 (ISSN-L)
- 1600-5775
- PMC
- PMC10624033
- OpenAlex
- W4387799120
- Cited by
- 43
- References
- 29
- Citations by year
- 2026: 12 · 2025: 16 · 2024: 15
- FWCI
- 8.32
- Type
- journal article
- Language
- en
- Open access
- gold
- doi.org
- Licence
- Locations
- Journal of Synchrotron Radiation (publishedVersion, cc-by)
- PubMed Central (publishedVersion, cc-by)
- PubMed (publishedVersion)
- Desy Publications Database (Deutsches Elektronen-Synchrotron DESY) (submittedVersion, cc-by)
- DOAJ (DOAJ: Directory of Open Access Journals) (submittedVersion, cc-by-sa)
- Funders
- Bundesministerium für Bildung und Forschung
- Helmholtz Association
- Deutsches Elektronen-Synchrotron
- Topics
- Physical Sciences › Physics and Astronomy › Radiation › Advanced X-ray Imaging Techniques
- Physical Sciences › Materials Science › Materials Chemistry › X-ray Diffraction in Crystallography
- Physical Sciences › Physics and Astronomy › Radiation › Nuclear Physics and Applications
- Keywords
- small-angle X-ray scattering, wide-angle X-ray scattering, PETRA III, synchrotron beamline optics, resonant scattering, transmission geometry, tensor tomography, soft matter
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