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Synthesis and Solid-State NMR Structural Characterization of 13 C-Labeled Graphite Oxide
Abstract
The detailed chemical structure of graphite oxide (GO), a layered material prepared from graphite almost 150 years ago and a precursor to chemically modified graphenes, has not been previously resolved because of the pseudo-random chemical functionalization of each layer, as well as variations in exact composition. Carbon-13 ( 13 C) solid-state nuclear magnetic resonance (SSNMR) spectra of GO for natural abundance 13 C have poor signal-to-noise ratios. Approximately 100% 13 C-labeled graphite was made and converted to 13 C-labeled GO, and 13 C SSNMR was used to reveal details of the chemical bonding network, including the chemical groups and their connections. Carbon-13–labeled graphite can be used to prepare chemically modified graphenes for 13 C SSNMR analysis with enhanced sensitivity and for fundamental studies of 13 C-labeled graphite and graphene.
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Cites
Graphene-based composite materials
Stankovich, S., Dikin, D. A., Dommett, G. H. B., Kohlhaas, K. M., Zimney, E. J., Stach, E. A., Piner, R. D., Nguyen, S. T., & Ruoff, R. S. (2006) · Nature · doi:10.1038/nature04969 · Cited by 12,922
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The chemistry of graphene oxide
Dreyer, D. R., Park, S., Bielawski, C. W., & Ruoff, R. S. (2010) · Chem. Soc. Rev. · doi:10.1039/b917103g · Cited by 11,653
Self-citationMechanical Properties of Monolayer Graphene Oxide
Suk, J. W., Piner, R. D., An, J., & Ruoff, R. S. (2010) · ACS Nano · doi:10.1021/nn101781v · Cited by 1,194
Self-citationTien, H.-W., Huang, Y.-L., Yang, S.-Y., Wang, J.-Y., & Ma, C.-C. M. (2011) · Carbon · doi:10.1016/j.carbon.2010.12.022 · Cited by 384
Zhang, L., Yang, W., Jiang, Z., He, F., Zhang, K., Fan, J., & Wu, J. (2017) · Applied Energy · doi:10.1016/j.apenergy.2017.04.041 · Cited by 183
Characterization of partially reduced graphene oxide as room temperature sensor for H2
Zhang, L.-S., Wang, W. D., Liang, X.-Q., Chu, W.-S., Song, W.-G., Wang, W., & Wu, Z.-Y. (2011) · Nanoscale · doi:10.1039/c1nr10187k · Cited by 77
Metadata
- Authors
- Cai, W., Piner, R. D., Stadermann, F. J., Park, S., Shaibat, M. A., Ishii, Y., Yang, D., Velamakanni, A., An, S. J., Stoller, M., An, J., Chen, D., & Ruoff, R. S.
- Venue
- Science
- Published
- 2008-09-26
- Volume
- 321
- Issue
- 5897
- Pages
- 1815-1817
- ISSN
- 0036-8075 (ISSN-L)
- 1095-9203
- OpenAlex
- W2147875763
- Cited by
- 1,184
- References
- 1
- FWCI
- 28.29
- Type
- journal article
- Language
- en
- Open access
- closed
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- CoChat. (2026). Citation check: Synthesis and Solid-State NMR Structural Characterization of 13 C-Labeled Graphite Oxide. https://app.cochat.ai/papers/10.1126/science.1162369
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- Cai, W., Piner, R. D., Stadermann, F. J., Park, S., Shaibat, M. A., Ishii, Y., Yang, D., Velamakanni, A., An, S. J., Stoller, M., An, J., Chen, D., & Ruoff, R. S. (2008). Synthesis and Solid-State NMR Structural Characterization of 13 C-Labeled Graphite Oxide. Science. https://doi.org/10.1126/science.1162369
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