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A Surface Enhanced Roman Scattering Study of the Intermediate and Poisoning Species Formed during the Electrochemical Reduction of CO 2 on Copper
Open accessAbstract
Surface enhanced Raman scattering (SERS) has been used to study the electrochemical reduction of on the copper electrode surface. The effect of different oxidation reduction cycles (ORCs) on the observed SERS has been investigated. A modification of the ORCs has been used to create sites which provide stable SERS, allowing exploration of the mechanism of reduction. The experimental conditions required to observe SERS in this system are described. The time‐dependent decay of the SERS bands and the time‐dependent increase of a new band, attributed to the formation of a poisoning species, have been measured; the intermediate species is CO; the poisoning species is a copper oxide patina.
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Cited by
Progress and perspectives of electrochemical CO2 reduction on copper in aqueous electrolyte
Nitopi, S., Bertheussen, E., Scott, S. B., Liu, X., Engstfeld, A. K., Horch, S., Seger, B., Stephens, I. E. L., Chan, K., Hahn, C., et al. (2019) · Chemical Reviews · doi:10.1021/acs.chemrev.8b00705 · Cited by 5,223
A review of catalysts for the electroreduction of carbon dioxide to produce low-carbon fuels
Qiao, J., Liu, Y., Hong, F., & Zhang, J. (2014) · Chem. Soc. Rev. · doi:10.1039/c3cs60323g · Cited by 2,990
Ren, D., Ang, B. S.-H., & Yeo, B. S. (2016) · ACS Catalysis · doi:10.1021/acscatal.6b02162 · Cited by 721
Gupta, N., Gattrell, M., & MacDougall, B. (2006) · Journal of Applied Electrochemistry · doi:10.1007/s10800-005-9058-y · Cited by 558
On the origin of the elusive first intermediate of CO 2 electroreduction
Chernyshova, I. V., Somasundaran, P., & Ponnurangam, S. (2018) · Proceedings of the National Academy of Sciences · doi:10.1073/pnas.1802256115 · Cited by 555
Metadata
- Authors
- Smith, B. D., Irish, D. E., Kedzierzawski, P., & Augustynski, J.
- Venue
- Journal of The Electrochemical Society
- Publisher
- The Electrochemical Society
- Published
- 1997-12-01
- Volume
- 144
- Issue
- 12
- Pages
- 4288-4296
- ISSN
- 0013-4651 (ISSN-L)
- 1945-7111
- OpenAlex
- W2054030229
- Cited by
- 162
- References
- 0
- FWCI
- 1.87
- Type
- journal article
- Language
- en
- Open access
- bronze
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- CoChat. (2026). Citation check: A Surface Enhanced Roman Scattering Study of the Intermediate and Poisoning Species Formed during the Electrochemical Reduction of CO 2 on Copper. https://app.cochat.ai/papers/10.1149/1.1838180
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- Smith, B. D., Irish, D. E., Kedzierzawski, P., & Augustynski, J. (1997). A Surface Enhanced Roman Scattering Study of the Intermediate and Poisoning Species Formed during the Electrochemical Reduction of CO 2 on Copper. Journal of The Electrochemical Society. https://doi.org/10.1149/1.1838180
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Contains information from the Semantic Scholar Academic Graph Datasets, made available under the ODC Attribution License (ODC-BY 1.0).
Semantic Scholar’s data is described in: Kinney, R., et al. (2023). The Semantic Scholar Open Data Platform. arXiv:2301.10140.
