Cited by 116Laser-Ablation Synthesis of NanoparticlesAdvanced Photocatalysis TechniquesZnO doping and properties

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Laser-Ablated ZnO Nanoparticles and Their Photocatalytic Activity toward Organic Pollutants

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Mintcheva, Neli, Aljulaih, Ali A., Wunderlich, Wilfried, Kulinich, Sergei A., Iwamori, Satoru·2018·Materials

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Abstract

This work aimed to prepare nanostructures of ZnO with various lasers, testing them as photocatalysts, and comparing their morphology and activity in the degradation of organic pollutants in aqueous media. ZnO nanospheres (ns-ZnO) and ZnO nanorods (ms-ZnO) were prepared via the laser ablation of a Zn metal plate in water using nanosecond- and millisecond-pulsed lasers, respectively. The obtained materials were characterized using a set of optical, structural, and surface-science techniques, such as UV-vis spectroscopy, X-ray diffraction (XRD), transmission electron microscopy (TEM), and X-ray photoelectron spectroscopy (XPS). Under visible-light irradiation, both nanostructures were found to be catalytically active toward the oxidation of methylene blue, which was used as a model compound. The ZnO nanorods fabricated with the millisecond laser showed better photocatalytic performance than their spherically shaped counterparts obtained by means of the nanosecond laser, which could be assigned to a larger number of defects on the ms-ZnO surface.

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Authors: Mintcheva, N., Aljulaih, A. A., Wunderlich, W., Kulinich, S. A., & Iwamori, S.
Affiliations: Tokai University (JP)
Corresponding author: Mintcheva, Neli
Kulinich, Sergei A.
ORCID: Mintcheva, Neli
Aljulaih, Ali A.
Wunderlich, Wilfried
Kulinich, Sergei A.
Iwamori, Satoru
Venue: Materials
Publisher: MDPI AG
Published: 2018-07-03
Volume: 11
Issue: 7
Pages: 1127
ISSN: 1996-1944 (ISSN-L)
DOI: 10.3390/ma11071127
PMC: PMC6073525
OpenAlex: W2810077735
Cited by: 115
References: 37
Citations by year: 2026: 12 · 2025: 19 · 2024: 15 · 2023: 15 · 2022: 14 · 2021: 13 · 2020: 16 · 2019: 8 · 2018: 3
FWCI: 4.00
Type: journal article
Language: en
Open access: gold
dx.doi.org
Licence: cc-by
creativecommons.org/licenses/by/4.0/ (vor)
Locations: Materials (publishedVersion, cc-by)
Europe PMC (PubMed Central) (publishedVersion, cc-by)
PubMed Central (publishedVersion, cc-by)
PubMed (publishedVersion)
DOAJ (DOAJ: Directory of Open Access Journals) (submittedVersion, cc-by-sa)
Funders: Hanoi University of Mining and Geology
Japan Society for the Promotion of Science (16K04904)
Topics: Physical Sciences › Materials Science › Materials Chemistry › Laser-Ablation Synthesis of Nanoparticles
Physical Sciences › Energy › Renewable Energy, Sustainability and the Environment › Advanced Photocatalysis Techniques
Physical Sciences › Materials Science › Materials Chemistry › ZnO doping and properties
Keywords: zinc oxide nanoparticles, laser ablation, ZnO nanorods, ZnO nanospheres, photocatalysis, visible light photocatalysis, methylene blue degradation, organic pollutant degradation, nanosecond laser, surface defects, morphology (materials science)

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Laser-Ablated ZnO Nanoparticles and Their Photocatalytic Activity toward Organic Pollutants

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