Pulse Duration and Wavelength Effects of Laser Ablation on the Oxidation, Hydrolysis, and Aging of Aluminum Nanoparticles in Water
Open accessAbstract
We analyzed the formation of the aluminum (Al) nanoparticles (NPs) with triangular shape obtained by ablating Al bulk in liquid using pulses with different durations (5 ns, 200 ps, and 30 fs) and wavelengths (355 nm, 800 nm, and 1064 nm). We report three stages of synthesis and aging of Al NPs: Formation, transformation, and stable stage. The NPs prepared by different pulses are almost identical at the initial stage. The effects of duration and wavelength of the ablation pulses on the aging of NPs are revealed. Pulse duration is determined to be essential for morphological transformation of NPs, while pulse wavelength strongly influences particle sizes. NPs produced by ultra-short pulses have smaller sizes and narrow size distribution. We demonstrate that oxidation and hydrolysis of Al in water are the results of ablation for all pulse durations and wavelengths, which also strongly modify the preferable reaction path of NPs in water, thus affecting the composition and morphology of triangle NPs. The results of modeling of the NPs generation in water due to a 50 ps laser pulse interacting with a thick Al target are presented. Water-based effects in the formation of NPs, their evolution, and solidification are considered from the mechanical and thermophysical points of view. The detailed analysis of the modeling results allowed for determination of the main mechanism responsible for the ablation process followed by the NPs formation.
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In Zhang et al.'s study, particle size significantly increases with ageing mainly due to coagulation, with a spherical to doughnut-like structure observed.
“The size of the particles significantly increases with ageing mainly due to coagulation with a spherical to doughnut-like structure observed, with a cone structure using ns pulses, a triangular structure using picosecond pulses, and a granular structure with uniform size distribution using fs pulses.”
From Influence of Laser Process Parameters, Liquid Medium, and External Field on the Synthesis of Colloidal Metal Nanoparticles Using Pulsed Laser Ablation in Liquid: A Review (2022) · cites this paper as [108]
Section 3.2 reports that particles produced with 355 nm, 5 ns pulses grew substantially during aging as smaller particles aggregated and coagulated; some later had doughnut-like surfaces. The claim omits that condition and makes the change sound general, whereas the Conclusions say particle size remained similar during aging with 1064 nm, 5 ns pulses. (LLM, conf=0.86)
Experimental — accuracy not yet measuredIn Zhang et al.'s study, suspensions varied in colour (nanosecond pulses white, picosecond light grey, femtosecond brown) due to surface plasmon effects.
“Moreover, the suspensions resulted in variations in colour (nanosecond pulses showed a white colour, picosecond pulses showed a light grey colour, and femtosecond pulses showed a brown colour) due to surface plasmon effects.”
From Influence of Laser Process Parameters, Liquid Medium, and External Field on the Synthesis of Colloidal Metal Nanoparticles Using Pulsed Laser Ablation in Liquid: A Review (2022) · cites this paper as [108]
Section 3.1 reports the stated colours: milky white for nanosecond pulses, light grey for picosecond pulses, and brown for femtosecond pulses. It links the colour differences to absorption extending into the visible range, but does not attribute them to surface plasmon effects. (LLM, conf=0.88)
Experimental — accuracy not yet measuredIn Zhang et al.'s study, ns pulses produced a cone structure, picosecond pulses a triangular structure, and fs pulses a granular structure with uniform size distribution.
“The size of the particles significantly increases with ageing mainly due to coagulation with a spherical to doughnut-like structure observed, with a cone structure using ns pulses, a triangular structure using picosecond pulses, and a granular structure with uniform size distribution using fs pulses.”
From Influence of Laser Process Parameters, Liquid Medium, and External Field on the Synthesis of Colloidal Metal Nanoparticles Using Pulsed Laser Ablation in Liquid: A Review (2022) · cites this paper as [108]
Section 3.2 reports triangles after aging with ps pulses and granular structures with uniform size distribution after aging with fs pulses. It reports only very few conical particles with 1064 nm ns pulses; most remained spherical. Conical structures were prominent in the ps-pulse results, so the claim overstates their association with ns pulses. (LLM, conf=0.90)
Experimental — accuracy not yet measuredZhang et al. analysed ablation of aluminium targets in distilled water at pulse durations of 5 ns, 200 ps, and 30 fs.
“The ablation of aluminium (Al) targets in distilled water was analysed at different pulse durations (i.e., 5 ns, 200 ps, and 30 fs) by Zhang et al. [108].”
Ultrashort pulses resulted in short and homogeneous structures.
“Furthermore, it was shown that ultrashort pulses resulted in short and homogeneous structures.”
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- Authors
- Zhang, K., Ivanov, D. S., Ganeev, R. A., Boltaev, G. S., Krishnendu, P. S., Singh, S. C., Garcia, M. E., Zavestovskaya, I. N., & Guo, C.
- Affiliations
- Chinese Academy of Sciences (CN)
- University of Kassel (DE)
- Theoretical Physics Department, University of Kassel, 34132 Kassel, Germany
- National Research Nuclear University MEPhI (RU)
- Corresponding author
- Guo, Chunlei
- ORCID
- Venue
- Nanomaterials
- Publisher
- MDPI AG
- Published
- 2019-05-18
- Volume
- 9
- Issue
- 5
- Pages
- 767
- ISSN
- 2079-4991 (ISSN-L)
- PMC
- PMC6566421
- OpenAlex
- W2945546116
- Cited by
- 39
- References
- 73
- Citations by year
- 2026: 4 · 2025: 8 · 2024: 2 · 2023: 7 · 2022: 6 · 2021: 3 · 2020: 7 · 2019: 2
- FWCI
- 1.59
- Type
- journal article
- Language
- en
- Open access
- gold
- dx.doi.org
- Licence
- Locations
- Nanomaterials (publishedVersion, cc-by)
- Europe PMC (PubMed Central) (publishedVersion, cc-by)
- PubMed Central (publishedVersion, cc-by)
- PubMed (publishedVersion)
- DOAJ (DOAJ: Directory of Open Access Journals) (submittedVersion, cc-by-sa)
- Funders
- National Key Research and Development Program of China (2017YFB1104700, 2018YFB1107202)
- National Natural Science Foundation of China (NSFC, 91750205, 61774155, 61705227)
- Scientific Research Project of the Chinese Academy of Sciences (QYZDB-SSW-SYS038)
- Jilin Provincial Science & Technology Development Project (20180414019GH)
- The Key Program of the International Partnership Program of CAS (181722KYSB20160015)
- Chinese Academy of Sciences President’s International Fellowship Initiative (2018VSA0001)
- MEPhI Academic Excellence Project (02.a03.21.0005)
- German Science Foundation (DFG IV 122/4-1 and GA 465/15-2)
- Topics
- Physical Sciences › Engineering › Biomedical Engineering › Laser-Ablation Synthesis of Nanoparticles
- Physical Sciences › Engineering › Computational Mechanics › Laser Material Processing Techniques
- Physical Sciences › Engineering › Mechanics of Materials › Energetic Materials and Combustion
- Keywords
- aluminum nanoparticles, laser ablation in liquid, pulse duration, laser wavelength, nanoparticle aging, oxidation, hydrolysis, triangular nanoparticles, nanoparticle morphology, nanoparticle size distribution, ultrafast lasers, nanoparticle formation mechanism, thermophysical modeling
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