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Cited by 14Analytical chemistry methods developmentRadioactive element chemistry and processingSupramolecular Chemistry and Complexes

Supramolecular solvent microextraction of uranium at trace levels from water and soil samples

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KHAN, Mansoor, YILMAZ, Erkan, SOYLAK, Mustafa·2017·TURKISH JOURNAL OF CHEMISTRY
DOI 10.3906/kim-1603-126
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Abstract

A supramolecular solvent microextraction procedure was established for the separation/preconcentration of uranium(VI) (U(VI)) prior to its determination by UV-Vis spectrophotometry. 1-(2-Pyridylazo)-2-naphthol (PAN) was used to form a red chelate (U-PAN) with U(VI) at pH 10. U-PAN was extracted by undecanol in tetrahydrofuran. All the parameters that affect extraction efficiency like solution pH, amount of ligand, type and volume of supramolecular solvent, sample volume, and diverse ion effect were optimized. The preconcentration factor was 17. The detection limit was 0.31 $\mu $g L$^{-1}$. The method was validated using GBW07424 (GSS-10 certified reference material). Microextraction was also applied to water and soil samples.

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  • According to literature, SUPRASs-LPME has been described as a fast, cost effective, and highly efficient extraction technique.

    “According to literature, SUPRASs-LPME has been described as a fast, cost effective, and highly efficient extraction technique [160,161].”

    From Liquid-phase microextraction of polycyclic aromatic hydrocarbons: A review (2020) · cites this paper as [160]

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Authors
KHAN, M., YILMAZ, E., & SOYLAK, M.
Affiliations
  • University of Peshawar (PK)
  • Erciyes University (TR)
ORCID
SOYLAK, Mustafa
Venue
TURKISH JOURNAL OF CHEMISTRY
Publisher
The Scientific and Technological Research Council of Turkey (TUBITAK-ULAKBIM) - DIGITAL COMMONS JOURNALS
Published
2017
Volume
41
Pages
61-69
ISSN
  • 1300-0527 (ISSN-L)
  • 1303-6130
DOI
10.3906/kim-1603-126
OpenAlex
W2590801542
Cited by
14
References
0
Citations by year
2024: 2 · 2023: 2 · 2022: 3 · 2021: 2 · 2020: 3 · 2019: 1 · 2018: 1
FWCI
0.96
Type
journal article
Language
en
Open access
Locations
  • TURKISH JOURNAL OF CHEMISTRY (publishedVersion)
  • DergiPark (Istanbul University) (submittedVersion)
Funders
Türkiye Bilimsel ve Teknolojik Araştırma Kurumu
Topics
  • Physical Sciences › Chemistry › Analytical Chemistry › Analytical chemistry methods development
  • Physical Sciences › Chemistry › Inorganic Chemistry › Radioactive element chemistry and processing
  • Physical Sciences › Chemistry › Organic Chemistry › Supramolecular Chemistry and Complexes
Keywords
uranium(VI), trace uranium determination, 1-(2-pyridylazo)-2-naphthol, preconcentration, water samples, soil sample, tetrahydrofuran extraction, UV-Vis spectroscopy, extraction optimization

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