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The Review of Some Commonly Used Methods and Techniques to Measure the Thermal Conductivity of Insulation Materials
Open accessAbstract
The use of insulation materials is considered as one of the most effective means of conserving energy in various fields. Thermal insulation materials enable systems to achieve energy efficiency. Many different thermal insulation materials have been developed to reduce heat flow by limiting conduction, convection, and/or radiation while performing one or more functions. These functions may vary in the context of thermal design, numerical simulations, and a wide range of engineering problems, such as determining the heat loss, temperature field, isolation, and cooling conservation, and in a variety of other technologies. One of the most effective ways to identify and determine performance is effective thermal conductivity. The thermal measurement performance is usually evaluated in a temperature and signal gradient for single or combined homogeneous/heterogenous materials. The two main categories of thermal conductivity measurement techniques are steady‐state methods and transient methods. The aim of this chapter is to present various measurement methods and to investigate their suitability for method purposes. This chapter presents new and accurate experimental techniques and methods for measuring the thermal conductivity of several most commonly used insulation materials. Some of these methods are commonly used in the field for measuring the thermal property of insulation materials. On the other hand, different insulation measurement practices are presented depending upon the overall structures. The analysis predicting the thermal conductivities of insulation materials is also discussed.
Overview
AI snapshot
Written from the paper’s full text.
TL;DR
This chapter reviews steady-state and transient methods for measuring the thermal conductivity of insulation materials, comparing their temperature ranges, uncertainties, material suitability, and standards. It concludes that no single measurement method or predictive model is universally applicable, so method choice must match material structure and measurement conditions.
Key findings
- Thermal conductivity measurement is divided into steady-state and transient methods; steady-state methods are traditionally considered more accurate for dry materials but are slow, while transient methods are faster and can directly determine thermal diffusivity.
- The guarded hot plate is described as the most commonly used and most effective method for insulation materials and can achieve a relative uncertainty of 2%, but interlaboratory comparisons of 20 different GHPs showed deviations from +13% to -16%.
- The heat-flow meter is comparative/relative and fast for low-conductivity materials; measurement uncertainties are approximately 3% at room temperature and 10–20% at high temperatures, with maximum temperature limits of about 200°C.
- The hot-disk/TPS method covers 0.005–500 W/(m K) over 30–1200 K and usually produces results in under 10 min; for glass fiber, measured conductivities were 20% and 12% higher than claimed values for lower and higher densities, respectively, and for rock wool the higher-density measured value was 8% higher than claimed. Laser flash can achieve 3–5% relative uncertainty at high temperatures.
Methods
- Design: narrative review/book chapter surveying experimental techniques for thermal conductivity measurement of insulation materials, including steady-state methods (guarded hot plate, heat-flow meter, direct heating, pipe) and transient methods (hot wire, hot disk, laser flash, 3-ω, Fitch, photothermal).
- Data or sample: no primary experimental sample is reported; the chapter synthesizes published literature, standards, and a comparison table of methods by temperature range, uncertainty, materials, and advantages/disadvantages.
- Main analysis: descriptive comparison of method suitability, ranges, uncertainties, and limitations, plus a review of predictive models such as series/parallel, geometric mean, Maxwell, effective medium theory, and Russell models.
Limitations
- Stated: no single measurement method is applicable to all thermal conductivity measurements; no single model or prediction procedure is universally applicable; accuracy of any method or model is limited by physical properties and other factors.
- Stated: manufacturers’ claimed thermal property values are sometimes questionable because density and temperature tested are not always reported; predicted thermal conductivities cannot reasonably be expected to be better than 5%.
- Evident: as a review chapter, it does not report a new experimental dataset or primary measurements; method comparisons rely on cited literature and standards.
Model-written summary. Check it against the paper before relying on it.
Integrity signals
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Cites
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Verification
Claims the paper makes
0 of 89 cited sources checked · 0 supported · 0 flagged
- Interpretationnone given
A disadvantage of steady-state methods is lengthy time requirements.
“Two disadvantages of steady-state methods are the lengthy time requirements and the difficulty of determining heat loss, especially at high temperatures.”
Quote in the paperNot a substantial claim - Premisenone given
In the laser flash method, measurement of thermal diffusivity is calculated based on the relative temperature change as a function of time only.
“The measurement of the thermal diffusivity is calculated based on the relative temperature change as a function of time only.”
Quote in the paperNot a substantial claim - Premisecitation
In many cases, it is possible to replace the temperature measurements at two opposite surfaces with a measurement as a function of time at only one position on the specimen.
“In many cases, it is possible to replace the temperature measurements at two opposite surfaces with a measurement as a function of time at only one position on the specimen [7].”
Quote in the paperNot a substantial claim0 of 1 sources checked- cites [7]
Couldn’t be matched to a paper in Crossref, so it can’t be checked.
- Premisecitation
The steady-state method is also in agreement between thermal measurements and practical application of insulations.
“It is also in the agreement between the thermal measurements and practical application of insulations [28].”
Quote in the paperNot a substantial claim0 of 1 sources checked- cites [28]
Couldn’t be matched to a paper in Crossref, so it can’t be checked.
- Premisecitation
The GHP is unsuitable for materials in which there is a potentiality for moisture migration.
“The GHP is most suitable for dry homogeneous specimens [15], but it is unsuitable for materials in which there is a potentiality for moisture migration [16].”
Quote in the paperNot a substantial claim0 of 1 sources checked- cites [16]
Couldn’t be matched to a paper in Crossref, so it can’t be checked.
- Premisecitation
The hot-wire technique can be adapted for measuring the properties of liquids and plastics of relatively low thermal conductivity.
“The technique can be adapted for measuring the properties of liquids and plastics of relatively low thermal conductivity [8].”
Quote in the paperNot a substantial claim0 of 1 sources checked- cites [8]
Couldn’t be matched to a paper in Crossref, so it can’t be checked.
- Premisecitation
For insulation materials at high temperatures, the measurement uncertainties are between 10 and 20%.
“For insulation materials at about room temperature, the measurement uncertainties are approximately 3%, and at high temperatures the uncertainties are between 10 and 20% [7].”
Quote in the paperNot a substantial claim0 of 1 sources checked- cites [7]
Couldn’t be matched to a paper in Crossref, so it can’t be checked.
- Premisereasoning
Even at high temperatures, relative measurement uncertainties in the 3-5% range can be achieved with the laser flash method.
“The main result of this fact is that even at high temperatures the relative measurement uncertainties in the 3-5% range can be achieved [30][31][32].”
Quote in the paperNot a substantial claim0 of 3 sources checked- cites [30]
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- cites [31]
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- cites [32]
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- Premisecitation
By comparing the temperature versus time response in the sensor, thermal conductivity or diffusivity can be calculated accurately.
“By comparing the temper-ature versus the time response in the sensor, thermal conductivity or diffusivity can be calculated accurately [26,27].”
Quote in the paperNot a substantial claim0 of 2 sources checked- cites [26]
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- cites [27]
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- Premisecitation
A modification of the hot-wire method is the hot-strip or disk technique, which can be applied to solid nonelectrically conducting materials in order to measure the thermal diffusivity and conductivity.
“A modification of the hot-wire method is the hot-strip or disk technique, which can be applied to solid nonelectrically conducting materials in order to measure the thermal diffusivity and conductivity [12].”
Quote in the paperNot a substantial claim0 of 1 sources checked- cites [12]
Couldn’t be matched to a paper in Crossref, so it can’t be checked.
- Premisecitation
The individual results of these 20 GHPs diverged significantly from reference values, ranging from +13 to -16%.
“The individual results of these 20 GHPs diverged significantly from reference values, ranging from +13 to -16% [5,11].”
Quote in the paperNot a substantial claim0 of 2 sources checked- cites [5]
Couldn’t be matched to a paper in Crossref, so it can’t be checked.
- cites [11]
Couldn’t be matched to a paper in Crossref, so it can’t be checked.
- Premisecitation
For glass fiber, the measured conductivities by hot-disk analyzer are 20% and 12% higher than the claimed values for the lower and higher densities, respectively.
“For glass fiber, the measured conductivities by hot-disk analyzer are 20 and 12% higher than the claimed values for the lower and higher densities, respectively [12].”
Quote in the paperNot a substantial claim0 of 1 sources checked- cites [12]
Couldn’t be matched to a paper in Crossref, so it can’t be checked.
- Premisecitation
A potential disadvantage of GHP is that contact resistance between the thermocouple and the specimen surface poses a major source of error.
“Other potential disadvantages are that the temperature gradient must be relatively large, the specimen width must be large, and also that the contact resistance between the thermocouple and the specimen surface poses a major source of error [12].”
Quote in the paperNot a substantial claim0 of 1 sources checked- cites [12]
Couldn’t be matched to a paper in Crossref, so it can’t be checked.
- Premisecitation
For insulation materials at about room temperature, the measurement uncertainties are approximately 3%.
“For insulation materials at about room temperature, the measurement uncertainties are approximately 3%, and at high temperatures the uncertainties are between 10 and 20% [7].”
Quote in the paperNot a substantial claim0 of 1 sources checked- cites [7]
Couldn’t be matched to a paper in Crossref, so it can’t be checked.
- Premisecitation
The GHP is most suitable for dry homogeneous specimens.
“The GHP is most suitable for dry homogeneous specimens [15], but it is unsuitable for materials in which there is a potentiality for moisture migration [16].”
Quote in the paperNot a substantial claim0 of 1 sources checked- cites [15]
Couldn’t be matched to a paper in Crossref, so it can’t be checked.
- Premisecitation
The GHP method is standardized in countries such as the United States (ASTM C 177-63), Great Britain (B.S. 874:1965), and Germany (DIN 52612).
“Another advantage is that the GHP method is standardized in countries such as the United States (ASTM C 177-63), Great Britain (B.S. 874:1965), and Germany (DIN 52612) [13].”
Quote in the paperNot a substantial claim0 of 1 sources checked- cites [13]
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- Premisecitation
The hot-disk method only gathers data regarding heat diffusion in the material for its calculations.
“The hot-disk method, on the other hand, only gathers data regarding from heat diffusion in material for its calculations [26].”
Quote in the paperNot a substantial claim0 of 1 sources checked- cites [26]
Couldn’t be matched to a paper in Crossref, so it can’t be checked.
- Interpretationnone given
There are four main types of measurement setups: the guarded hot plate (GHP), the heat-flow meter (HFM), the hot wire, and laser flash diffusivity.
“For measuring thermal conductivity, there are four main types of measurement setups: the guarded hot plate (GHP), the heat-flow meter (HFM), the hot wire, and laser flash diffusivity.”
Quote in the paperNot a substantial claim - Premisereasoning
The laser flash method has the advantage of involving neither temperature nor heat-flow measurements for the determination of a thermal property.
“The laser flash method has the advantage of involving neither temperature nor heat-flow measurements for the determination of a thermal property.”
Quote in the paperNot a substantial claim - Premisecitation
The laser flash method can investigate properties of glasses, metals, and ceramics without significant limitations due to uncertainties of the achievable measurement.
“The method can investigate to properties of glasses, metals, and ceramics without significant limitations due to uncertainties of the achievable measurement [7].”
Quote in the paperNot a substantial claim0 of 1 sources checked- cites [7]
Couldn’t be matched to a paper in Crossref, so it can’t be checked.
- Premisecitation
Interlaboratory comparisons of GHP calculations have revealed discrepancies among 20 different GHPs used at different times.
“However, the accuracy of this method is questionable, interlaboratory comparisons of GHP calculations have revealed discrepancies among 20 different GHPs used at different times [5].”
Quote in the paperNot a substantial claim0 of 1 sources checked- cites [5]
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- Premisereasoning
Even at different conductivity levels, a negative influence is unavoidable with the guarded hot-plate method.
“Even at different conductivity levels, a negative influence is unavoidable with the guarded hot-plate method.”
Quote in the paperNot a substantial claim - Premisecitation
The hot disk requires specimen sizes that are usually much smaller than those used in other techniques.
“Furthermore, the hot disk requires using specimen sizes that are usually much smaller than those used in other techniques [12].”
Quote in the paperNot a substantial claim0 of 1 sources checked- cites [12]
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- Premisecitation
The maximum temperature limit for the heat-flow meter method in practical applications is about 100°C.
“The maximum temperature limits are approximately 200°C for the heat-flow meter method [7] and about 100°C in practical applications [2].”
Quote in the paperNot a substantial claim0 of 1 sources checked- cites [2]
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- Premisecitation
One study of isotropic materials demonstrated that the transient hot-wire method is most dependable due to its high reliability and low amount of effort, time, and cost required.
“On the other hand, one study of the isotropic materials demonstrated that the transient hot-wire method proved to be most dependable due its high reliability and low amount of effort, time, and cost required [28].”
Quote in the paperNot a substantial claim0 of 1 sources checked- cites [28]
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- Premisecitation
The thermal conductivities of metals (approximately up to 500 W/(m K) in a temperature range between about 4 and 1000 K) can be tested via the cylinder method of employing axial heat flow.
“The thermal conductivities of metals (approximately up to 500 W/(m K) in a temperature range between about 4 and 1000 K) can be tested via the cylinder method of employing axial heat flow.”
Quote in the paperNot a substantial claim0 of 1 sources checked- cites [7]
Couldn’t be matched to a paper in Crossref, so it can’t be checked.
- Interpretationnone given
A disadvantage of steady-state methods is the difficulty of determining heat loss, especially at high temperatures.
“Two disadvantages of steady-state methods are the lengthy time requirements and the difficulty of determining heat loss, especially at high temperatures.”
Quote in the paperNot a substantial claim - Premisenone given
The TPS technique can be used to study liquids, solids, pastes, and powders, whether electrically conducting or insulating.
“The TPS technique can be used to study liquids, solids, pastes, and powders (electrically conducting or insulating).”
Quote in the paperNot a substantial claim - Premisecitation
The hot-disk method ensures accurate measurements over a thermal conductivity range from 0.005 to 500 W/(m K) over temperatures from 30 to 1200 K.
“This method ensures accurate measurements over a thermal conductivity range from 0.005 to 500 W/(m K) over temperatures from 30 to 1200 K [25].”
Quote in the paperNot a substantial claim0 of 1 sources checked- cites [25]
Couldn’t be matched to a paper in Crossref, so it can’t be checked.
- Interpretationnone given
The probe method is applied to low-conductivity materials in powder or semirigid form.
“Thus, the probe method is applied to low-conductivity materials in powder or semirigid form.”
Quote in the paperNot a substantial claim - Premisecitation
The cross-wire technique can be used to measure thermal conductivities below 2 W/m K.
“The cross-wire technique can be used to measure thermal conductivities below 2 W/m K [2].”
Quote in the paperNot a substantial claim0 of 1 sources checked- cites [2]
Couldn’t be matched to a paper in Crossref, so it can’t be checked.
- Premisecitation
The guarded hot-plate method can be used to test the thermal properties of nonmetals such as thermal insulation materials, polymers glasses, and ceramics, as well as liquids and gases in the temperature range between about 80 and 800 K.
“The guarded hot-plate method can be used to test the thermal properties of nonmetals such as thermal insulation materials, polymers glasses, and ceramics, as well as liquids and gases in the temperature range between about 80 and 800 K [7].”
Quote in the paperNot a substantial claim0 of 1 sources checked- cites [7]
Couldn’t be matched to a paper in Crossref, so it can’t be checked.
- Premisecitation
The hot-wire method is capable of measuring the thermal conductivity of gases as well as refractories, such as insulating bricks, fibrous, or powder materials.
“The hot-wire method is also capable of measuring the thermal conductivity of gases as well as refractories, such as insulating bricks, fibrous, or powder materials [10].”
Quote in the paperNot a substantial claim0 of 1 sources checked- cites [10]
Couldn’t be matched to a paper in Crossref, so it can’t be checked.
- Premisecitation
There is no single measurement method for all thermal conductivity measurements.
“As a result of the wide range of thermal properties of insulation materials, there is no single measurement method for all thermal conductivity measurements [1].”
Quote in the paperSubstantial claim0 of 1 sources checked- cites [1]
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- Premisecitation
A disadvantage of steady-state technique is that it generally takes a long time to reach the required equilibrium.
“A disadvantage, however, is that it generally takes a long time to reach the required equilibrium [4,5].”
Quote in the paperNot a substantial claim0 of 2 sources checked- cites [4]
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- cites [5]
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- Premisecitation
The thermal conductivity of large specimens of refractory material is measured by using hot-wire systems.
“The thermal conductivity of large specimens of refractory material is measured by using hot-wire systems [2].”
Quote in the paperNot a substantial claim0 of 1 sources checked- cites [2]
Couldn’t be matched to a paper in Crossref, so it can’t be checked.
- Premisenone given
The guarded hot plate is inherently subject to error due to contact resistance between the thermocouple and the specimen surface.
“In contrast, the guarded hot plate is inherently subject to error due to contact resistance between the thermocouple and the specimen surface.”
Quote in the paperNot a substantial claim - Premisecitation
The hot-wire method should not be employed for determining the thermal conductivity of nonisotropic materials such as fiber mats, for which it is totally ineffective in ranges with a low extinction coefficient, i.e. low bulk densities.
“Thus, the hotwire method should not be employed for determining the thermal conductivity of nonisotropic materials (fiber mats), for which this method is totally ineffective in ranges with a low extinction coefficient, i.e., low bulk densities [28].”
Quote in the paperSubstantial claim0 of 1 sources checked- cites [28]
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- Premisecitation
In these kinds of tests, the contact resistances between the specimen and the heater or the cold plate must be considered.
“In these kinds of tests, the contact resistances between the specimen and the heater or the cold plate must be considered [7].”
Quote in the paperNot a substantial claim0 of 1 sources checked- cites [7]
Couldn’t be matched to a paper in Crossref, so it can’t be checked.
- Premisecitation
Insulation materials and polymers (k < 0.3 W/(m K)) are usually tested via the heat-flow meter method.
“Insulation materials and polymers (k < 0.3 W/(m K)) are usually tested via the heat-flow meter method, and sometimes it is used for glasses and ceramics and for other materials with thermal conductivities lower than about 5 W/(m K) [7].”
Quote in the paperNot a substantial claim0 of 1 sources checked- cites [7]
Couldn’t be matched to a paper in Crossref, so it can’t be checked.
- Premisenone given
The advantage of transient techniques over steady-state techniques is that the effect of contact resistance is eliminated in the analysis.
“The advantage of transient technique to steady-state technique is that the effect of the contact resistance is eliminated in the analysis.”
Quote in the paperNot a substantial claim - Premisecitation
In the 3-ω method, since the electrical resistance of the metal heater is proportional to temperature, the temperature oscillation can be measured indirectly by measuring the associated 3ω voltage.
“Since the electrical resistance of the metal heater is proportional (linear) to the temperature, the temperature oscillation can be measured indirectly by measuring the associated 3ω voltage [34].”
Quote in the paperNot a substantial claim0 of 1 sources checked- cites [34]
Couldn’t be matched to a paper in Crossref, so it can’t be checked.
- Interpretationreasoning
There is no single model or prediction procedure that is universally applicable.
“Therefore, there is no single model or prediction procedure to be considered that is universally applicable.”
Quote in the paperSubstantial claim - Premisecitation
The combination between the heater wire width and the thin film thickness determines the measurement sensitivity according to the in-plane and cross-plane thermal properties of the film.
“The combination between the heater wire width and the thin film thickness determines the measurement sensitivity according to the in-plane and cross-plane thermal properties of the film [16].”
Quote in the paperNot a substantial claim0 of 1 sources checked- cites [16]
Couldn’t be matched to a paper in Crossref, so it can’t be checked.
- Premisenone given
The 3-ω method measures the average thermal conductivity in the in-plane and cross-plane directions.
“The method measures the average thermal conductivity in the in-plane and cross-plane directions.”
Quote in the paperNot a substantial claim - Premisereasoning
It has not been possible to know which expression is the most accurate for describing thermal conductivity even in every model of two-phase components/mixes.
“It has not been possible to know which expression is the most accurate for describing the thermal conductivity even in every model of two-phase components/mixes.”
Quote in the paperNot a substantial claim - Interpretationreasoning
The difference of thermal conductivity values between models and methods can be considered due to the lack of structural data.
“The difference of thermal conductivity values between models and methods can be considered due to the lack of structural data.”
Quote in the paperNot a substantial claim - Premisereasoning
In most modeling exercises, the prediction of thermal conductivity involves a trade-off between simplicity and accuracy.
“In most modeling exercises, the prediction of thermal conductivity also involves a trade-off between simplicity and accuracy.”
Quote in the paperNot a substantial claim - Interpretationnone given
These thermal conductivity measurement methods may not be applicable for all materials.
“The first major conclusion that can be drawn is that these methods may not be applicable for all materials.”
Quote in the paperSubstantial claim - Premisecitation
Several proposed models are created specifically for a particular material and contain material-content properties.
“Several models that have been proposed are created specifically for a particular material and contain material-content properties [39].”
Quote in the paperNot a substantial claim0 of 1 sources checked- cites [39]
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- Premisecitation
The accuracy of predicted thermal conductivities cannot be reasonably expected to be better than 5%.
“The accuracy of predicted thermal conductivities cannot be reasonably expected to be better than 5% [39][40][41].”
Quote in the paperNot a substantial claim0 of 3 sources checked- cites [39]
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- cites [40]
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- cites [41]
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- Premisecitation
The structures that affect thermal conductivity values include nonhomogeneity/homogeneity, components, differences in the direction of components, condensation/evaporation of a liquid phase, contact mechanism, size and shape of particles/pores, tortuosity of pores, mixed phases, shape factor, contact, orientation, thickness, and reinforcement.
“The structures include nonhomogeneity/homogeneity, the components, the differences in the direction of components, the condensation/evaporation of a liquid phase, the contact mechanism, the size and shape of particles/pores, the tortuosity of pores, mixed phases, shape factor, contact, orientation,thickness, reinforcement etc. [39,41,42].”
Quote in the paperNot a substantial claim0 of 3 sources checked- cites [39]
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- cites [41]
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- cites [42]
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- Probably not a substantial claim. 70
- It may state two separate claims as one. 34
Probably not a substantial claim. The paper’s conclusions may not depend on it.
PremisecitationThere are two basic techniques for measuring thermal conductivity: steady-state methods and transient or non-steady-state methods.
“In general, there are two basic techniques for measuring thermal conductivity: steady-state methods and transient or non-steady-state methods [1,3].”
Quote in the paperNot a substantial claim0 of 2 sources checked- cites [1]
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- cites [3]
Couldn’t be matched to a paper in Crossref, so it can’t be checked.
Probably not a substantial claim. The paper’s conclusions may not depend on it.
PremisecitationThe laser flash method is often employed for highly conductive ceramics, metals, and some composites.
“The laser flash method is often employed for highly conductive ceramics, metals, and some composites [2].”
Quote in the paperNot a substantial claim0 of 1 sources checked- cites [2]
Couldn’t be matched to a paper in Crossref, so it can’t be checked.
Probably not a substantial claim. The paper’s conclusions may not depend on it. The paper may give no reason why it holds.
InterpretationreasoningThis method is also more appropriate for high moisture content materials because of the signal and response in the specimen.
“This method is also more appropriate for high moisture content materials because of the signal and response in the specimen.”
Quote in the paperNot a substantial claimProbably not a substantial claim. The paper’s conclusions may not depend on it. The paper may give no reason why it holds.
Premisenone givenThe hot-wire and guarded hot-plate techniques considerably require both larger specimens and a precisely known thickness.
“The hot-wire and guarded hot-plate techniques considerably require both larger specimens and a precisely known thickness.”
Quote in the paperNot a substantial claimProbably not a substantial claim. The paper’s conclusions may not depend on it.
Premisenone givenThe hot-strip method is very similar to the hot-wire technique except for an extended strip.
“The hot-strip method is very similar to the hot-wire technique with the exception of an extended strip.”
Quote in the paperNot a substantial claimProbably not a substantial claim. The paper’s conclusions may not depend on it.
Study design and conductnone givenUsing a stabilized electrical power supply ensures that the hot-wire heat source produces a constant output.
“The use of a stabilized electrical power supply ensures that the heat source produces a constant output.”
Quote in the paperNot a substantial claimIt may state two separate claims as one.
Premisenone givenThe main advantages of hot-disk measurement are that it produces results quickly, usually in under 10 min, and that different sensor sizes can accommodate different specimen types.
“The main advantages of the hot-disk measurement are that it produces results quickly (usually in under 10 min), and that different sensor sizes can be used to accommodate different specimen types.”
Quote in the paperNot a substantial claimProbably not a substantial claim. The paper’s conclusions may not depend on it.
Interpretationnone givenUnlike the single-specimen method, the symmetrical setup can be used for investigating solid materials.
“Unlike the single-specimen method, the symmetrical setup can be used for investigating solid materials.”
Quote in the paperNot a substantial claimProbably not a substantial claim. The paper’s conclusions may not depend on it. The paper may give no reason why it holds.
Interpretationnone givenThe hot-wire technique is a good method to determine the thermal conductivity of liquids.
“The hot-wire technique is a good method to determine the thermal conductivity of liquids.”
Quote in the paperNot a substantial claimProbably not a substantial claim. The paper’s conclusions may not depend on it. It may state two separate claims as one.
PremisecitationThe coating materials for the TPS sensor are most commonly Kapton for measuring temperatures between 30 and 450 K, Mica for higher temperatures up to 1200 K, and Teflon.
“The coating materials are most commonly Kapton for measuring temperature ranges between 30 and 450 K, Mica for higher temperatures of up to 1200 K [25], and Teflon.”
Quote in the paperNot a substantial claim0 of 1 sources checked- cites [25]
Couldn’t be matched to a paper in Crossref, so it can’t be checked.
Probably not a substantial claim. The paper’s conclusions may not depend on it.
Interpretationnone givenAmong transient methods, the hot-wire and the laser flash methods are commonly used for measuring the thermal conductivity of different materials provided in Table 1.
“Among transient methods, the hot-wire and the laser flash methods are commonly used for measuring the thermal conductivity of different materials provided in Table 1.”
Quote in the paperNot a substantial claimIt may state two separate claims as one.
PremisecitationThe hot-wire method is practical for foams, fluids, and melted plastics, but it is impractical for solids.
“It is practical for foams, fluids, and melted plastics, but it is impractical for solids [5].”
Quote in the paperNot a substantial claim0 of 1 sources checked- cites [5]
Couldn’t be matched to a paper in Crossref, so it can’t be checked.
Probably not a substantial claim. The paper’s conclusions may not depend on it. It may state two separate claims as one.
PremisecitationAlthough large specimen size is cited as a potential disadvantage, size is usually not a serious issue.
“Although Reference [12] cites large specimen size as a potential disadvantage, size is usually not a serious issue [8].”
Quote in the paperNot a substantial claim0 of 1 sources checked- cites [8]
Couldn’t be matched to a paper in Crossref, so it can’t be checked.
It may state two separate claims as one.
InterpretationreasoningTest time is obtained in a few minutes or a subsecond time intervals for transient methods.
“Therefore, test time is obtained in a few minutes or a subsecond time intervals for transient methods.”
Quote in the paperNot a substantial claimProbably not a substantial claim. The paper’s conclusions may not depend on it.
Interpretationnone givenThe advantages of transient methods are mainly distinguished by the short amount of time needed, so that various thermal values can be determined in the measurement process.
“The advantages of transient methods are mainly distinguished by the short amount time needed, so that various thermal values can be determined in the measurement process.”
Quote in the paperNot a substantial claimProbably not a substantial claim. The paper’s conclusions may not depend on it.
InterpretationreasoningIn the two specimen apparatus, the main advantage is that heat loss from the hot plate can be controlled more effectively due to the symmetrical arrangement of the specimen on each side of the heater.
“In the two specimen apparatus, the main advantage is that heat loss from the hot plate can be controlled more effectively due to the symmetrical arrangement of the specimen on each side of the heater.”
Quote in the paperNot a substantial claimIt may state two separate claims as one.
PremisecitationThe pipe method has the disadvantage of deviations from the radial symmetric temperature field with respect to the wire method, but an adequate mathematical model and evaluation procedure can compensate for this disadvantage.
“Although the pipe method has the disadvantage of deviations from the radial symmetric temperature field with respect to the wire method, adequate mathematical model and evaluation procedure can compensate for this disadvantage [7,23,24].”
Quote in the paperNot a substantial claim0 of 3 sources checked- cites [7]
Couldn’t be matched to a paper in Crossref, so it can’t be checked.
- cites [23]
Couldn’t be matched to a paper in Crossref, so it can’t be checked.
- cites [24]
Couldn’t be matched to a paper in Crossref, so it can’t be checked.
It may state two separate claims as one.
PremisecitationThe steady-state method, i.e. the guarded hot plate, is superior to the hot-wire method for testing nonisotropic materials despite the long duration and higher costs of steady-state measurements, because of its high reliability in the entire temperature range investigated.
“As a result, the test procedure of the steady-state method (i.e., the guarded hot plate) is superior to the hot-wire method for testing nonisotropic materials despite the long duration of those steady-state measurements, the higher costs of the steady-state apparatus due to the high reliability in the entire temperature range investigated [28].”
Quote in the paperSubstantial claim0 of 1 sources checked- cites [28]
Couldn’t be matched to a paper in Crossref, so it can’t be checked.
Probably not a substantial claim. The paper’s conclusions may not depend on it. It may state two separate claims as one.
PremisecitationThe TPS technique is used for measuring the thermal conductivity of insulation materials and electrically conducting materials.
“The TPS technique is used for measuring the thermal conductivity of insulation materials and electrically conducting materials [12].”
Quote in the paperNot a substantial claim0 of 1 sources checked- cites [12]
Couldn’t be matched to a paper in Crossref, so it can’t be checked.
Probably not a substantial claim. The paper’s conclusions may not depend on it.
PremisecitationIn the laser flash method, thermal diffusivity is calculated based on the thickness d of the specimen, typically 2 mm, and the time t1/2.
“The thermal diffusivity is calculated based on the thickness d of the specimen (typically 2 mm) and the time t 1/2 [20].”
Quote in the paperNot a substantial claim0 of 1 sources checked- cites [20]
Couldn’t be matched to a paper in Crossref, so it can’t be checked.
It may state two separate claims as one.
Study design and conductcitationIn the hot-wire method, connecting leads to the ends of the hot wire and using two hot wires of differing lengths in a differential mode eliminates interference from axial conduction via the large-diameter current supply.
“In order to eliminate the interference of axial conduction via the large-diameter current supply, leads are connected to the ends of the hot wire, and also two hot wires of differing lengths are utilized in a differential mode [7].”
Quote in the paperNot a substantial claim0 of 1 sources checked- cites [7]
Couldn’t be matched to a paper in Crossref, so it can’t be checked.
Probably not a substantial claim. The paper’s conclusions may not depend on it. The paper may give no reason why it holds.
Premisenone givenThe transient plane source (TPS) technique is a recent development of the hot-strip method.
“The transient plane source (TPS) technique is a recent development of the hot-strip method.”
Quote in the paperNot a substantial claimProbably not a substantial claim. The paper’s conclusions may not depend on it. The paper may give no reason why it holds. It may state two separate claims as one.
InterpretationreasoningFor this reason, the hot-wire method is avoided in favor of an increasingly popular variation, the hot-strip method, which is used for measurements on solids.
“For this reason, the hot-wire method is avoided in favor of an increasingly popular variation, the hot-strip method, which is used for measurements on solids.”
Quote in the paperNot a substantial claimIt may state two separate claims as one.
PremisecitationThe parallel-wire method is advantageous for anisotropic materials and for materials with thermal conductivity above 2 W/(m K).
“The parallel-wire method is advantageous when applied to anisotropic materials and for materials in the magnitude of a thermal conductivity above 2 W/(m K) [20].”
Quote in the paperNot a substantial claim0 of 1 sources checked- cites [20]
Couldn’t be matched to a paper in Crossref, so it can’t be checked.
It may state two separate claims as one.
InterpretationreasoningThese disadvantages can be overcome by the direct heating method, which can be used for electrically conductive materials such as metals.
“These disadvantages can be overcome by the direct heating method, which can be used for electrically conductive materials such as metals.”
Quote in the paperNot a substantial claimProbably not a substantial claim. The paper’s conclusions may not depend on it.
PremisecitationTransient methods generally employ needle probes or wires.
“Transient methods generally employ needle probes or wires [4].”
Quote in the paperNot a substantial claim0 of 1 sources checked- cites [4]
Couldn’t be matched to a paper in Crossref, so it can’t be checked.
Probably not a substantial claim. The paper’s conclusions may not depend on it.
Premisenone givenSome modifications of the laser flash method have been developed to determine directly the thermal conductivity by performing measurement of the specific heat capacity.
“The some modifications have been developed to determine directly the thermal conductivity by performing measurement of the specific heat capacity.”
Quote in the paperNot a substantial claimProbably not a substantial claim. The paper’s conclusions may not depend on it. The paper may give no reason why it holds.
Interpretationnone givenWith a guarded heater and/or thermal insulation, a relative uncertainty of 2% for thermal conductivity measurements can be achieved.
“With a guarded heater and/or thermal insulation, a relative uncertainty of 2% for thermal conductivity measurements of can be achieved.”
Quote in the paperNot a substantial claimProbably not a substantial claim. The paper’s conclusions may not depend on it.
PremisecitationThe maximum temperature limit for the heat-flow meter method is approximately 200°C.
“The maximum temperature limits are approximately 200°C for the heat-flow meter method [7] and about 100°C in practical applications [2].”
Quote in the paperNot a substantial claim0 of 1 sources checked- cites [7]
Couldn’t be matched to a paper in Crossref, so it can’t be checked.
It may state two separate claims as one.
PremisecitationThe TPS technique can provide values without interference of thermal contact resistance, without prolonged measurement times, and without extensive specimen preparation.
“The TPS technique can provide the values without the interference of thermal contact resistance, without prolonged measurement times, and without extensive specimen preparation [26].”
Quote in the paperNot a substantial claim0 of 1 sources checked- cites [26]
Couldn’t be matched to a paper in Crossref, so it can’t be checked.
Probably not a substantial claim. The paper’s conclusions may not depend on it.
PremisecitationSteady-state methods are considered more accurate than transient methods for testing dry materials.
“Transient heat transfer methods are capable of directly determining thermal diffusivity, whereas steady-state methods are considered to be more accurate than transient methods for testing dry materials [6].”
Quote in the paperNot a substantial claim0 of 1 sources checked- cites [6]
Couldn’t be matched to a paper in Crossref, so it can’t be checked.
Probably not a substantial claim. The paper’s conclusions may not depend on it.
PremisecitationA potential disadvantage of GHP is that the temperature gradient must be relatively large.
“Other potential disadvantages are that the temperature gradient must be relatively large, the specimen width must be large, and also that the contact resistance between the thermocouple and the specimen surface poses a major source of error [12].”
Quote in the paperNot a substantial claim0 of 1 sources checked- cites [12]
Couldn’t be matched to a paper in Crossref, so it can’t be checked.
Probably not a substantial claim. The paper’s conclusions may not depend on it. The paper may give no reason why it holds. It may state two separate claims as one.
InterpretationreasoningThe GHP method is appropriate for these kinds of metal because the determination of the temperature difference is the main challenge when measuring materials with high thermal conductivity (e.g., metals).
“The GHP method is appropriate for these kinds of metal because the determination of the temperature difference is the main challenge when measuring materials with high thermal conductivity (e.g., metals).”
Quote in the paperNot a substantial claimIt may state two separate claims as one.
PremisecitationTransient measurements can be made relatively quickly, which is an advantage over steady-state techniques.
“These measurements can be made relatively quickly, which garners an advantage over steady-state techniques [4,5,7].”
Quote in the paperNot a substantial claim0 of 3 sources checked- cites [4]
Couldn’t be matched to a paper in Crossref, so it can’t be checked.
- cites [5]
Couldn’t be matched to a paper in Crossref, so it can’t be checked.
- cites [7]
Couldn’t be matched to a paper in Crossref, so it can’t be checked.
Probably not a substantial claim. The paper’s conclusions may not depend on it.
PremisecitationThe heat-flow meter method is sometimes used for glasses and ceramics and for other materials with thermal conductivities lower than about 5 W/(m K).
“Insulation materials and polymers (k < 0.3 W/(m K)) are usually tested via the heat-flow meter method, and sometimes it is used for glasses and ceramics and for other materials with thermal conductivities lower than about 5 W/(m K) [7].”
Quote in the paperNot a substantial claim0 of 1 sources checked- cites [7]
Couldn’t be matched to a paper in Crossref, so it can’t be checked.
Probably not a substantial claim. The paper’s conclusions may not depend on it.
PremisecitationFor measuring the conductivity of nonsolid materials, it is necessary to heat the specimen from the top in order to avoid convection.
“For measuring the conductivity of nonsolid materials, it is necessary to heat the specimen from the top in order to avoid convection [7].”
Quote in the paperNot a substantial claim0 of 1 sources checked- cites [7]
Couldn’t be matched to a paper in Crossref, so it can’t be checked.
Probably not a substantial claim. The paper’s conclusions may not depend on it.
PremisecitationTransient heat transfer methods are capable of directly determining thermal diffusivity.
“Transient heat transfer methods are capable of directly determining thermal diffusivity, whereas steady-state methods are considered to be more accurate than transient methods for testing dry materials [6].”
Quote in the paperNot a substantial claim0 of 1 sources checked- cites [6]
Couldn’t be matched to a paper in Crossref, so it can’t be checked.
Probably not a substantial claim. The paper’s conclusions may not depend on it.
Premisenone givenThe laser flash method can measure the property in a temperature range between -100 and about 3000°C.
“The property can be measured in a temperature range between -100 and about 3000°C.”
Quote in the paperNot a substantial claimProbably not a substantial claim. The paper’s conclusions may not depend on it. It may state two separate claims as one.
Premisenone givenThe guarded hot-plate method is time-consuming because it requires a temperature gradient across the specimen, while the hot-disk method provides instant and direct measurement and the reading is obtained in a short amount of time.
“While the guarded hot-plate method is a time-consuming method for requiring a temperature gradient across the specimen, the hot-disk method provides instant and direct measurement and the reading is obtained in a short amount of time.”
Quote in the paperNot a substantial claimProbably not a substantial claim. The paper’s conclusions may not depend on it. The paper may give no reason why it holds.
Premisenone givenThe laser flash method is the most commonly used method for ascertaining the thermal properties of solids.
“The laser flash method is the most commonly used method for ascertaining the thermal properties of solids.”
Quote in the paperNot a substantial claimProbably not a substantial claim. The paper’s conclusions may not depend on it. The paper may give no reason why it holds. It may state two separate claims as one.
Interpretationnone givenThis technique can be modified to collect data over time for the simultaneous measurement of thermal conductivity and thermal diffusivity, and these kinds of transient methods are gaining increased interest.
“This technique can be modified to collect data over time for the simultaneous measurement of thermal conductivity and thermal diffusivity, and these kinds of transient methods are gaining increased interest.”
Quote in the paperNot a substantial claimIt may state two separate claims as one.
PremisecitationIn the hot-wire method, thermal conductivity can be calculated from the temperature rise at two different times, or from the slope of the temperature rise versus the logarithm of time, and from the strength of the heat source.
“Thus, the thermal conductivity can be calculated based on the temperature rise at two different times (or the slope of the temperature rise compared to the logarithm of time) and from the strength of the heat source [16].”
Quote in the paperNot a substantial claim0 of 1 sources checked- cites [16]
Couldn’t be matched to a paper in Crossref, so it can’t be checked.
- The authors state this as an assumption: In the hot-wire method, convection and radiation heat losses are neglected.
It may state two separate claims as one.
PremisecitationHeat-flow meters are accurate and fast apparatuses, and the operation of these apparatuses is easy for measuring the thermal conductivity of low-conductivity materials.
“In contrast, heat-flow meters are accurate and fast apparatuses, and the operation of these apparatuses is easy for measuring the thermal conductivity of low-conductivity materials [2].”
Quote in the paperNot a substantial claim0 of 1 sources checked- cites [2]
Couldn’t be matched to a paper in Crossref, so it can’t be checked.
Probably not a substantial claim. The paper’s conclusions may not depend on it.
PremisecitationThere have been several developments in the laser flash method since its introduction by Parker et al. (1961).
“There have been several developments in the method since its introduction by Parker et al. (1961) [29].”
Quote in the paperNot a substantial claim0 of 1 sources checked- cites [29]
Couldn’t be matched to a paper in Crossref, so it can’t be checked.
Probably not a substantial claim. The paper’s conclusions may not depend on it. It may state two separate claims as one.
PremisereasoningIn the laser flash method, thermal diffusivity α is determined, and if the specific heat capacity and density of a material are given, thermal conductivity can be calculated under adiabatic conditions.
“In this method, the thermal diffusivity α is determined, and if given the specific heat capacity and the density of a material, the thermal conductivity can be calculated by using the following equation (Eq.( 6)) under adiabatic conditions:”
Quote in the paperNot a substantial claim- The authors state this as an assumption: In the laser flash method, the calculation of thermal conductivity from thermal diffusivity, specific heat capacity, and density is under adiabatic conditions.
Probably not a substantial claim. The paper’s conclusions may not depend on it. It may state two separate claims as one.
Interpretationnone givenThe steady-state pipe method is considered a transient radial flow technique, so isotropic specimens are required.
“This technique is considered to be a transient radial flow technique, so isotropic specimens are required.”
Quote in the paperNot a substantial claimProbably not a substantial claim. The paper’s conclusions may not depend on it.
PremisecitationA potential disadvantage of GHP is that the specimen width must be large.
“Other potential disadvantages are that the temperature gradient must be relatively large, the specimen width must be large, and also that the contact resistance between the thermocouple and the specimen surface poses a major source of error [12].”
Quote in the paperNot a substantial claim0 of 1 sources checked- cites [12]
Couldn’t be matched to a paper in Crossref, so it can’t be checked.
Probably not a substantial claim. The paper’s conclusions may not depend on it.
Premisenone givenThe TPS technique is designed to measure both thermal conductivity and thermal diffusivity.
“The technique is designed to measure both thermal conductivity and thermal diffusivity.”
Quote in the paperNot a substantial claimIt may state two separate claims as one.
PremisecitationFor rock wool, the conductivity determined by the hot-disk method harmonizes with the claimed value at lower density, while the measured value is 8% higher than the claimed conductivity at higher density.
“For the lower density, the conductivity determined for the rock wool with the hot-disk method harmonizes with the claimed value; the measured value is 8% higher than the claimed conductivity for the higher density [12].”
Quote in the paperNot a substantial claim0 of 1 sources checked- cites [12]
Couldn’t be matched to a paper in Crossref, so it can’t be checked.
It may state two separate claims as one.
PremisecitationThe guarded hot plate is the most commonly used and most effective method for measuring the thermal conductivity of insulation materials.
“The guarded hot plate, also known as the Poensgen apparatus [11], is the most commonly used and most effective method for measuring the thermal conductivity of insulation materials.”
Quote in the paperNot a substantial claim0 of 1 sources checked- cites [11]
Couldn’t be matched to a paper in Crossref, so it can’t be checked.
Probably not a substantial claim. The paper’s conclusions may not depend on it. It may state two separate claims as one.
PremisecitationMaterials studied with the hot-strip system include metals, alloys, ceramics including high-conducting ceramics like AlN, high critical temperature materials, minerals, polymers, composites, glass, fabrics, paper, glass wool, foam, powder, biomaterial, liquids, and anisotropic materials.
“Materials studied so far with this system include metals, alloys, ceramics including high conducting ceramics like Aluminium nitride (AlN), high critical temperature materials, minerals, polymers, composites, glass, fabrics, paper, glass wool, foam, powder, biomaterial, and liquids, as well as materials with anisotropic thermal properties [25].”
Quote in the paperNot a substantial claim0 of 1 sources checked- cites [25]
Couldn’t be matched to a paper in Crossref, so it can’t be checked.
Probably not a substantial claim. The paper’s conclusions may not depend on it. It may state two separate claims as one.
Interpretationnone givenCompared to the guarded hot-plate method, which is an absolute method, the heat-flow meter method is comparative and thus can be considered to be a relative method.
“Compared to the guarded hot-plate method, which is an absolute method, the heat-flow meter method is comparative and thus can be considered to be a relative method.”
Quote in the paperNot a substantial claimIt may state two separate claims as one.
PremisecitationThe pipe method technique has been modified for use with a variety of solids, ranging from insulation materials (20 mW/(m K)) to metals (200 W/(m K)) and evaluating for temperatures between room temperature and 2770 K.
“This technique has been modified for use with a variety of solids, ranging from insulation materials (20 mW/(m K)) to metals (200 W/(m K)) and evaluating for temperatures between room temperature and 2770 K [7].”
Quote in the paperNot a substantial claim0 of 1 sources checked- cites [7]
Couldn’t be matched to a paper in Crossref, so it can’t be checked.
Probably not a substantial claim. The paper’s conclusions may not depend on it.
Premisenone givenThe 3-ω method is commonly used for measuring the thermal conductivity of thin films and solid materials.
“The method called the 3-ω method is commonly used for measuring the thermal conductivity of thin films and solid materials.”
Quote in the paperNot a substantial claimProbably not a substantial claim. The paper’s conclusions may not depend on it. The paper may give no reason why it holds.
Interpretationnone givenEstimating low thermal conductivity may be determined with adjustable parameters in these methods.
“Estimating low thermal conductivity may be determined with adjustable parameters in these methods.”
Quote in the paperNot a substantial claimProbably not a substantial claim. The paper’s conclusions may not depend on it.
Premisenone givenThe techniques measure a response as a signal or a temperature given in the sample.
“The techniques measure a response as a signal or a temperature given in the sample.”
Quote in the paperNot a substantial claimProbably not a substantial claim. The paper’s conclusions may not depend on it.
Premisenone givenThe Fitch method is generally used for measuring the conductivity of foods and specially small-sized specimens.
“This method is generally used for measuring the conductivity of foods and specially smallsized specimens.”
Quote in the paperNot a substantial claimProbably not a substantial claim. The paper’s conclusions may not depend on it.
PremisecitationA detailed description for a bulk material with a porous medium can be expressed in terms of ancestor, extra parameter, component knowledge, and heat transfer mechanisms in various models.
“A detailed description for a bulk material with a porous medium can be expressed in terms of “ancestor,” “extra parameter,” “component knowledge,” and “heat transfer mechanisms” in various models [39].”
Quote in the paperNot a substantial claim0 of 1 sources checked- cites [39]
Couldn’t be matched to a paper in Crossref, so it can’t be checked.
Probably not a substantial claim. The paper’s conclusions may not depend on it.
Premisenone givenThe principle of the photothermal method is based on ascertaining the light-induced change in the thermal state of a material in solid, liquid, or gaseous state.
“The principle of this method is based on ascertaining the light-induced change in the thermal state of a material in solid, liquid, or gaseous state.”
Quote in the paperNot a substantial claimProbably not a substantial claim. The paper’s conclusions may not depend on it.
PremisecitationThe photothermal technique can be modified by having both surfaces heated simultaneously with a single modulation frequency and taking a measurement of the phase difference between surface signals.
“This technique can be modified by having both surfaces heated simultaneously with a single modulation frequency and taking a measurement of the phase difference between surface signals [20].”
Quote in the paperNot a substantial claim0 of 1 sources checked- cites [20]
Couldn’t be matched to a paper in Crossref, so it can’t be checked.
Probably not a substantial claim. It may be too vague to check against evidence. The paper’s conclusions may not depend on it. The paper may give no reason why it holds.
Interpretationnone givenSome methods are similar or derivative methods regardless of whether the thermal conductivity model being used is similar.
“Some methods are similar or derivative methods regardless of whether the thermal conductivity model being used is similar.”
Quote in the paperNot a substantial claimIt may state two separate claims as one.
Premisenone givenThe 3-ω method has a thermal conductivity range of 0.20-20 W/(m K), and the range can be extended to 77-900 K in the literature.
“The range of thermal conductivity is changed of 0.20-20 W/(m K), and the range can be extended to 77-900 K in literature.”
Quote in the paperNot a substantial claimProbably not a substantial claim. The paper’s conclusions may not depend on it.
PremisecitationIn the 3-ω method, because the current is driven at a frequency ω and the resistance changes at a frequency 2ω, a voltage at 3ω results.
“Because the current is driven at a frequency ω and the resistance changes at a frequency 2ω, a voltage at 3ω results [34].”
Quote in the paperNot a substantial claim0 of 1 sources checked- cites [34]
Couldn’t be matched to a paper in Crossref, so it can’t be checked.
Probably not a substantial claim. The paper’s conclusions may not depend on it. The paper may give no reason why it holds.
Premisenone givenThe Fitch method is not practical for use at high temperatures.
“But the Fitch method is not practical for use at high temperatures.”
Quote in the paperNot a substantial claimProbably not a substantial claim. The paper’s conclusions may not depend on it. It may state two separate claims as one.
PremisecitationSeveral researchers have proposed models derived from a set of equations, usually based on a basic model, but many of these include empirical parameters.
“Several researchers have proposed a number of models derived from a set of equations, usually based on a basic model, but many of these include empirical parameters [1].”
Quote in the paperNot a substantial claim0 of 1 sources checked- cites [1]
Couldn’t be matched to a paper in Crossref, so it can’t be checked.
Probably not a substantial claim. The paper’s conclusions may not depend on it.
Premisenone givenIn the Fitch method, the roles of the heat source and the heat receiver can be changed if the vessel is at a temperature lower than that of the copper block.
“The roles of the heat source and the heat receiver can be changed if the vessel is at a temperature lower than that of the copper block.”
Quote in the paperNot a substantial claimProbably not a substantial claim. The paper’s conclusions may not depend on it. The paper may give no reason why it holds.
Interpretationnone givenThe models show similarities and differences depending on whether it is a steady state.
“The models show similarities and differences depending on whether it is a steady state.”
Quote in the paperNot a substantial claimProbably not a substantial claim. The paper may give no reason why it holds.
Interpretationnone givenThe thermal conductivity value from a method is higher or lower than the value from other methods, depending on the relationships between the heat loss distribution, the surface temperatures, the uniform heat flow over the material, and the signal and its response.
“The thermal conductivity value from the method is higher or lower than the value from other methods, depending on the relationships between the heat loss distribution, the surface temperatures, the uniform heat flow over the material, and the signal and its response.”
Quote in the paperNot a substantial claimProbably not a substantial claim. The paper’s conclusions may not depend on it. The paper may give no reason why it holds.
Premisenone givenThermal conductivity methods are broadly classified as either steady-state methods or transient methods.
“Thermal conductivity methods are broadly classified as either steady-state methods or transient methods.”
Quote in the paperNot a substantial claimProbably not a substantial claim. The paper’s conclusions may not depend on it.
Premisenone givenThe models are based on one or more basic structural models, such as the series and parallel models, the geometric mean model, Maxwell models, effective medium theory (EMT) models, and the Russell model.
“The models are based on one or more basic structural models, such as the series and parallel models, the geometric mean model, Maxwell models (different forms), effective medium theory (EMT) models, and the Russell model.”
Quote in the paperNot a substantial claimIt may state two separate claims as one.
PremisecitationThe literature contains a large number of standard models for predicting the thermal conductivities of homogeneous, heterogeneous, or composite materials, as well as methods of measurement apparatus designed.
“The literature contains a large number of standard models for predicting the thermal conductivities of homogeneous, heterogeneous, or composite materials materials [39], as well as methods of a measurement apparatus designed [40].”
Quote in the paperNot a substantial claim0 of 2 sources checked- cites [39]
Couldn’t be matched to a paper in Crossref, so it can’t be checked.
- cites [40]
Couldn’t be matched to a paper in Crossref, so it can’t be checked.
Probably not a substantial claim. The paper’s conclusions may not depend on it.
Premisenone givenThe Fitch method consists of two components: a heat source and a heat receiver.
“This method consists of two components: a heat source and a heat receiver.”
Quote in the paperNot a substantial claimProbably not a substantial claim. The paper’s conclusions may not depend on it.
PremisecitationThe choice of thermal conductivity models is generally discussed separately in the literature for each of these classes.
“The choice of thermal conductivity models is generally discussed separately in the literature for each of these classes [39].”
Quote in the paperNot a substantial claim0 of 1 sources checked- cites [39]
Couldn’t be matched to a paper in Crossref, so it can’t be checked.
Probably not a substantial claim. It may be too vague to check against evidence. The paper’s conclusions may not depend on it. The paper may give no reason why it holds.
Premisenone givenMany theoretical models, as well as methods, have been proposed by various researchers.
“Many theoretical models, as well as methods, have been proposed by various researchers.”
Quote in the paperNot a substantial claimProbably not a substantial claim. The paper’s conclusions may not depend on it.
PremisecitationThese models are largely dependent on mathematical models derived from the physical laws that govern the process, such as mass and energy balances and thermodynamics.
“These models are largely dependent on mathematical models derived from the physical laws that govern the process (e.g., mass and energy balances, thermodynamics, etc.).”
Quote in the paperNot a substantial claim0 of 1 sources checked- cites [39]
Couldn’t be matched to a paper in Crossref, so it can’t be checked.
Probably not a substantial claim. The paper’s conclusions may not depend on it. It may state two separate claims as one.
Premisenone givenMeasuring thermal diffusivity via the photothermal method is based on the concept of modulating between the heating of a specimen surface and the temperature phase on the opposite sides of the specimen and includes a frequency function.
“Measuring the thermal diffusivity measurement via the photothermal method is based on the concept of modulating between the heating of a specimen surface and the temperature phase on the opposite sides of the specimen and includes a frequency function.”
Quote in the paperNot a substantial claimProbably not a substantial claim. The paper may give no reason why it holds. It may state two separate claims as one.
Interpretationnone givenThe preferable methods are commonly the guarded hot-plate method, the heat-flow method, and then the hot wire/disk and laser flash methods.
“The preferable methods are commonly the guarded hot-plate method, the heat-flow method, and then can be given by the hot wire/disk, laser flash methods.”
Quote in the paperNot a substantial claimProbably not a substantial claim. The paper’s conclusions may not depend on it.
Premisenone givenThe Fitch method is used to measure materials of low thermal conductivity by using a plane source of heat.
“The Fitch method developed by Fitch is used to measure the materials of low thermal conductivity by using a plane source of heat.”
Quote in the paperNot a substantial claimProbably not a substantial claim. The paper’s conclusions may not depend on it.
PremisecitationIn the Fitch method, either a line heat source or one or more heat sources are used.
“In this method, either a line heat source or one or more heat sources are used [16].”
Quote in the paperNot a substantial claim0 of 1 sources checked- cites [16]
Couldn’t be matched to a paper in Crossref, so it can’t be checked.
It may state two separate claims as one.
PremisecitationWhile the hot-wire method is a time-domain transient technique, the 3-ω method has the advantage of being time independent because it measures electrical signals in a specific frequency domain.
“While the hot-wire method is a time domain transient technique, the 3-ω method has the advantage of being time independent because it measures electrical signals in a specific frequency domain [33].”
Quote in the paperNot a substantial claim0 of 1 sources checked- cites [33]
Couldn’t be matched to a paper in Crossref, so it can’t be checked.
Probably not a substantial claim. The paper’s conclusions may not depend on it. It may state two separate claims as one.
Premisenone givenBoth basic mechanisms generally affect in-plane and cross-plane transport differently, so the thermal conductivity of related materials is usually anisotropic.
“Both basic mechanisms generally affect in-plane (x) and cross-plane (z) transport differently, so that the thermal conductivity of related materials is usually anisotropic.”
Quote in the paperNot a substantial claimProbably not a substantial claim.
Premisenone givenThere are various methods for determining the thermal conductivity of insulation materials.
“There are various methods for determining thermal conductivity of insulation materials.”
Quote in the paperSubstantial claimProbably not a substantial claim. The paper’s conclusions may not depend on it. It may state two separate claims as one.
Premisenone givenThe literature also presents an experimental evaluation of the models and a comparison analysis of the existing experimental methods.
“The literature also present an experimental evaluation of the models and a comparison analysis of the existing experimental methods.”
Quote in the paperNot a substantial claimProbably not a substantial claim. The paper may give no reason why it holds.
Interpretationnone givenUnder anisotropic and isotropic conditions, some methods are in good agreement with the claimed values.
“Under the condition of anisotropic and isotropic type, some methods are in good agreement with the claimed values.”
Quote in the paperNot a substantial claimProbably not a substantial claim. The paper’s conclusions may not depend on it.
PremisecitationMany thermal conductivity models are based on one or more basic structural models, such as series and parallel models, the geometric mean model, Maxwell models, effective medium theory (EMT) models, and the Russell model.
“Many thermal conductivity models found in the literature are based on one or more basic structural models, such as the series and parallel models, the geometric mean model, Maxwell models (different forms) and effective medium theory (EMT) models, and the Russell Model [39].”
Quote in the paperNot a substantial claim0 of 1 sources checked- cites [39]
Couldn’t be matched to a paper in Crossref, so it can’t be checked.
Probably not a substantial claim. The paper’s conclusions may not depend on it.
Premisenone givenSimilar models are given in different forms and replace other components instead of a component parameter.
“Similar models are given in different forms and replace the other components instead of a component parameter.”
Quote in the paperNot a substantial claimProbably not a substantial claim. The paper’s conclusions may not depend on it. The paper may give no reason why it holds.
Premisenone givenIn principle, thermal conductivity methods are based on establishing a steady temperature and a signal gradient over a sample.
“In principle, these methods are based on establishing a steady temperature and a signal gradient over a sample.”
Quote in the paperNot a substantial claimProbably not a substantial claim. It may be too vague to check against evidence. The paper’s conclusions may not depend on it. The paper may give no reason why it holds.
Interpretationnone givenThe models may not seem to be a clear explanation of the interior structure and behavior of porous materials.
“The models may not seem to be a clear explanation of the interior structure and behavior of porous materials.”
Quote in the paperNot a substantial claim
The authors state this as an assumption.
The measured heat power rate is transferred across the specimen due to guarded heaters.
“It is assumed that the measured heat power rate is transferred across the specimen due to guarded heaters.”
The authors state this as an assumption.
Lateral effects are insignificant either because the ratio of length to diameter of the test apparatus is large or because guard heaters are used.
“The lateral effects are assumed to be insignificant either because the ratio of length to diameter of the test apparatus is large or because guard heaters are used.”
The authors state this as an assumption.
The surface of the central heater at diameter r1 and the outer specimen surface at diameter r2 reach the same temperature after the steady state is established.
“It is assumed that the surface of the central heater at a diameter r 1 and the outer specimen surface at diameter r 2 reach the same temperature after the steady state is established.”
The paper relies on this without support.
The thermal data for certain materials are often incomplete and lacking in important information.
“The accuracy of manufacturers' claimed values for thermal properties is sometimes questionable since the thermal data for certain materials are often incomplete and lacking in important information.”
The paper relies on this without support.
When values for insulation types are quoted, manufacturers do not always report the density and temperature of the materials tested.
“When values for insulation types are quoted, manufacturers do not always report the density and temperature of the materials tested.”
The paper relies on this without support.
The effective thermal conductivities of materials depend on the constituents and/or voids present in the different characteristics of their structures as well as the density and temperature of the material.
“In general, the “effective” thermal conductivities of the materials depend on the constituents and/or voids present in the different characteristics of their structures as well as the density and temperature of the material.”
The paper relies on this without support.
The accuracy of any method and model is limited by physical properties and other factors.
“The accuracy of any method and model is limited by physical properties and other factors.”
The paper relies on this without support.
Measurement and modeling of thermal conductivity are difficult and require high precision in the determination of the various parameters involved in the calculations.
“However, measurement and modeling of thermal conductivity are difficult and require high precision in the determination of the various parameters involved in the calculations.”
The authors state this as an assumption.
In the Fitch method, the specimen has a uniform temperature distribution.
“It is assumed to have a uniform temperature distribution.”
The authors state this as an assumption.
In the Fitch method, heat transfer from the copper block to insulation, heat storage in the specimen, and surface contact resistance are negligible under a linear temperature profile.
“The heat transfer from the copper block to insulation, the heat storage in the specimen, and the surface contact resistance are assumed to be negligible under a linear temperature profile.”
The authors state this as an assumption.
In the hot-wire method, convection and radiation heat losses are neglected.
“neglecting convection and radiation heat losses.”
The authors state this as an assumption.
In the laser flash method, the calculation of thermal conductivity from thermal diffusivity, specific heat capacity, and density is under adiabatic conditions.
“under adiabatic conditions:”
Self-check
Percentages, sums and reported differences re-computed from the paper’s own numbers.
Each contradiction between two passages listed here was confirmed by an independent check.
Direct-heating temperature ranges differ
MajorThe method summary gives a range of 400-3000 K, while the direct-heating section gives 300-4000 K for the same method, both citing Reference [7].
“Direct heating 400-3000 K [7, 10]”
“the specimen is heated up to temperatures in the range of 300-4000 K [7].”
Pipe method called both steady-state and transient
MinorConsecutive sentences classify the described pipe method as steady-state and then as a transient radial-flow technique, without distinguishing two versions.
“Another use of the method is a steady-state pipe method having a cylindrical specimen geometry and containing radial heat-flow measurements [7,21,22].”
“This technique is considered to be a transient radial flow technique, so isotropic specimens are required.”
Parker paper has the wrong reference number
MinorThe text cites Parker et al. (1961) as Reference [29], but the bibliography lists that paper as Reference 28; Reference 29 is a different paper.
“There have been several developments in the method since its introduction by Parker et al. (1961) [29].”
“28. Parker W J, Jenkins R J, Butler C P, Abbott G L. Flash method of determining thermal diffusivity, heat capacity, and thermal conductivity. Journal of Applied Physics. 1961; 32: 1679-1684.”
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Metadata
- Authors
- Yüksel, N.
- Corresponding author
- Yüksel, Numan
- ORCID
- Yüksel, Numan
- Venue
- Insulation Materials in Context of Sustainability
- Publisher
- InTech
- Published
- 2016-08-31
- OpenAlex
- W2517557791
- Cited by
- 143
- References
- 33
- Citations by year
- 2026: 8 · 2025: 13 · 2024: 20 · 2023: 31 · 2022: 20 · 2021: 20 · 2020: 15 · 2019: 7 · 2018: 4 · 2017: 4 · 2016: 1
- FWCI
- 13.77
- Type
- book chapter
- Language
- en
- Open access
- hybrid
- doi.org
- Licence
- cc-by
- Locations
- InTech eBooks (publishedVersion, cc-by)
- BiblioBoard Library Catalog (Open Research Library) (submittedVersion, cc-by)
- Topics
- Physical Sciences › Materials Science › Materials Chemistry › Thermal properties of materials
- Physical Sciences › Engineering › Computational Mechanics › Heat Transfer and Numerical Methods
- Physical Sciences › Engineering › Mechanics of Materials › Thermography and Photoacoustic Techniques
- Keywords
- thermal conductivity measurement, thermal insulation materials, steady-state method, transient method, energy conservation, heat loss, temperature gradient, heterogeneous materials, thermal conductivity prediction
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