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Thermal degradation of segmented polyurethanes
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Abstract Thermal degradation of polyurethane samples was studied by a thermogravimetric method. The effect of soft‐segment length and soft‐segment concentration on activation energy of the degradation process was measured. Three methods of calculation gave activation energies at different stages of the very complex weight loss process. It was shown that at initial stages of the weight loss the process was dominated by hard‐segment degradation. Activation energy of the whole process calculated by the Ozawa–Flynn method did not offer clear insight into the structure–stability relationship of polyurethanes. The second method showed that activation energy of the initial stage of degradation increased with decrease in hard‐segment length. The Flynn method of calculating activation energy produced fairly constant activation energy of the first 40% degradation, at around 150 kJ/mol, for polymers in the C series. Generally, calculation of kinetic parameters of a complex degradation process as in polyurethanes gives results that are not easy to interpret. It has been shown qualitatively that polymers with higher soft‐segment concentration display lower initial weight loss and higher onset temperatures of degradation. © 1994 John Wiley & Sons, Inc.
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“Thermoplastic SMPUs undergo thermal degradation first via decomposition of urethane bonds before soft segments start to decompose [235,236].”
From Review on the Functional Determinants and Durability of Shape Memory Polymers (2010) · cites this paper as [236]
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Metadata
- Authors
- Petrović, Z. S., Zavargo, Z., Flyn, J. H., & Macknight, W. J.
- Affiliations
- University of Novi Sad (RS)
- National Institute of Standards and Technology (US)
- University of Massachusetts Amherst (US)
- Venue
- Journal of Applied Polymer Science
- Publisher
- Wiley
- Published
- 1994-02-07
- Volume
- 51
- Issue
- 6
- Pages
- 1087-1095
- ISSN
- 0021-8995 (ISSN-L)
- 1097-4628
- OpenAlex
- W1973937445
- Cited by
- 404
- References
- 18
- Citations by year
- 2026: 14 · 2025: 14 · 2024: 24 · 2023: 17 · 2022: 19 · 2021: 12 · 2020: 12 · 2019: 22 · 2018: 21 · 2017: 19 · 2016: 25 · 2015: 19 · 2014: 21 · 2013: 17 · 2012: 16
- FWCI
- 2.35
- Type
- journal article
- Language
- en
- Open access
- green
- works.bepress.com
- Locations
- Journal of Applied Polymer Science (publishedVersion)
- ScholarWorks@UMassAmherst (University of Massachusetts Amherst) (submittedVersion)
- Topics
- Physical Sciences › Materials Science › Materials Chemistry › Thermal and Kinetic Analysis
- Physical Sciences › Materials Science › Polymers and Plastics › Polymer Science and PVC
- Physical Sciences › Materials Science › Polymers and Plastics › Polymer crystallization and properties
- Keywords
- segmented polyurethanes, thermal degradation, activation energy, soft segment length, degradation kinetics, structure-stability relationship, weight loss
About these checks
Registry, retraction, Cites and statistics results are computed, not judged, with one exception: a printed reference that no index lists is read once by a model before it counts as a citation error. Claims are extracted by a model and kept only when their quote appears verbatim in the text; each cited source is then checked, with a model’s help, for whether it says what the claim relies on. Those verdicts can be wrong — read the claim’s quote and the cited source before relying on one.
Statistics and arithmetic are recomputed, not judged.
Confidence bands are shown only for fields calibrated on our annotated test set. None is calibrated yet, so no band is shown.
What counts as a claim ›How we measure confidence ›How we check this ›
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