Non-target analysis of household dust and laundry dryer lint using comprehensive two-dimensional liquid chromatography coupled with time-of-flight mass spectrometry
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Household dust and laundry dryer lint are important indoor environmental matrices that may have notable health effects on humans due to chronic exposure. However, due to the sample complexity the studies conducted on these sample matrices until now were almost exclusively on the basis of target analysis. In this study, comprehensive two-dimensional liquid chromatography coupled with time-of-flight mass spectrometry (LC × LC-ToF MS) was applied, to enable non-target analysis of household dust as well as laundry dryer lint for the first time. The higher peak capacity and good orthogonality of LC × LC, together with reduced ion suppression in the MS enabled rapid identification of environmental contaminants in these complex sample matrices. A number of environmental contaminants were tentatively identified based on their accurate masses and isotopic patterns, including plasticizers, flame retardants, pesticides, drug metabolites, etc. The identity of seven compounds: tris(2-butoxyethyl) phosphate, tris(2-chloropropyl) phosphate, n-benzyl butyl phthalate, dibutyl phthalate, tributyl phosphate, triethyl phosphate and N, N-diethyl-meta-toluamide was confirmed using two-dimensional retention alignment and their concentrations in the samples were semi-quantitatively determined.
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Multidimensional analysis techniques such as GC×GC or LC×LC followed by TOF-MS have been developed for non-target analysis of environmental contaminants in dust samples.
“Multidimensional analysis techniques such as GC Â GC or LC Â LC followed by TOF-MS have been developed for non-target analysis of environmental contaminants in dust samples [95].”
From Worldwide trends in tracing poly- and perfluoroalkyl substances (PFAS) in the environment (2019) · cites this paper as [95]
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- Authors
- Ouyang, X., Weiss, J. M., de Boer, J., Lamoree, M. H., & Leonards, P. E. G.
- Affiliations
- Vrije Universiteit Amsterdam (NL)
- Stockholm University (SE)
- Corresponding author
- Ouyang, Xiyu
- Venue
- Chemosphere
- Publisher
- Elsevier BV
- Published
- 2017-01
- Volume
- 166
- Pages
- 431-437
- ISSN
- 0045-6535 (ISSN-L)
- OpenAlex
- W2528936397
- Cited by
- 68
- References
- 35
- Citations by year
- 2026: 3 · 2025: 4 · 2024: 8 · 2023: 9 · 2022: 7 · 2021: 10 · 2020: 7 · 2019: 12 · 2018: 4 · 2017: 4
- FWCI
- 3.33
- Type
- journal article
- Language
- en
- Open access
- hybrid
- doi.org
- Licence
- Locations
- Chemosphere (publishedVersion, cc-by-nc-nd)
- PubMed (publishedVersion)
- VU Research Portal (publishedVersion, other-oa)
- Data Archiving and Networked Services (DANS) (submittedVersion, other-oa)
- Funders
- Swedish Research Council (210-2012-131)
- Topics
- Physical Sciences › Chemistry › Spectroscopy › Analytical Chemistry and Chromatography
- Physical Sciences › Environmental Science › Health, Toxicology and Mutagenesis › Toxic Organic Pollutants Impact
- Physical Sciences › Chemistry › Analytical Chemistry › Analytical chemistry methods development
- Keywords
- house dust, indoor air quality, non-targeted analysis, environmental pollutants, plasticizers, flame retardants, pesticides, drug metabolites, phthalates, tris(2-butoxyethyl) phosphate, indoor exposure
- MeSH terms
- Chromatography, Liquid, Dust, Environmental Pollutants, Flame Retardants, Housing, Humans, Organophosphorus Compounds, Pesticides, Organophosphates, Phthalic Acids, Plasticizers, Mass Spectrometry, Air Pollution, Indoor
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