The DOI matches its Crossref record; 34 of the 34 references it cites were found in a registry or an index.
Characterization of bending behavior of hydroxyapatite/biopolymer porous composite beams
Open accessAbstract
Abstract In this work, porous composite beams of HA/PLLA and HA/PLCL were developed using a combination of the template and freeze-drying methods. Their compositions were examined using Fourier transform infrared spectroscopy and X-ray diffraction spectroscopy. Their bending mechanical and fracture properties were characterized under the three-point bending condition. Their microstructures and the micro mechanisms of deformation and fracture were also examined by scanning electron microscopy. It was confirmed that the presence of polymer material did not affect the crystal structure of HA, and the diffraction pattern of both beams remained the same after sintering. Both composite beams showed dramatically improved flexural mechanical properties compared to a pure HA beam. Their bending fracture behavior was characterized as a crack initiation and growth accompanied by microdamage formation at the center. It was determined that microdamage formation and the subsequent deformation and fracture of the polymer phase was initiated by microfracture of HA struts. It was also found that the addition of PLLA results in a higher modulus and fracture strength, while the addition of PLCL results in a higher fracture energy due to ductile elongation.
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“The elongation at break of PLCL is typically high, ranging from 100 to 500%, especially when the ε-caprolactone proportion is increased, as this significantly enhances the material’s flexibility [57, 58].”
From Application of PLCL as a biodegradable polymer in biomedical engineering (2026) · cites this paper as [58]
Citations
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Research works printed but not linked: 2
- Grumezescu, 2016, vol. 4
- Todo, 2018, Development and characterization of porous hydroxyapatite scaffolds reinforced with polymeric secondary phase for bone tissue engineering, Biomater. Tissue Technol., 2, 1
Cited by
Biosoluble ceramic fiber reinforced poly(L-lactic acid) bone scaffold: degradation and bioactivity
Shuai, C., Wang, Z., Zhang, H., Jia, J., Huang, L., Wang, D., Chen, S., & Feng, P. (2022) · npj Materials Degradation · doi:10.1038/s41529-022-00297-3 · Cited by 16
Liu, G., Li, B., Liu, Z., Dong, J., Kang, X., Feng, Y., Jia, D., & Zhou, Y. (2022) · Composites Communications · doi:10.1016/j.coco.2022.101488 · Cited by 11
Hazwani, F., & Todo, M. (2021) · Composite Structures · doi:10.1016/j.compstruct.2021.114983 · Cited by 11
Self-citationZhao, X., Yang, Z., Wang, W., Jiang, G., Wei, S., Liu, A., Guan, J., & Wang, P. (2021) · Ceramics International · doi:10.1016/j.ceramint.2021.09.147 · Cited by 10
Wang, Y., Meng, F., Zhu, J., Ba, Z., Jiang, D., Wen, X., & Tang, T. (2023) · Colloid & Polymer Science · doi:10.1007/s00396-023-05166-2 · Cited by 9
Metadata
- Authors
- Hazwani, F., & Todo, M.
- Affiliations
- Kyushu University (JP)
- Corresponding author
- Todo, Mitsugu
- Venue
- Composites Communications
- Publisher
- Elsevier BV
- Published
- 2021-06
- Volume
- 25
- Pages
- 100747
- ISSN
- 2452-2139 (ISSN-L)
- OpenAlex
- W3154572448
- Cited by
- 15
- References
- 34
- Citations by year
- 2026: 1 · 2025: 3 · 2024: 2 · 2023: 4 · 2022: 3 · 2021: 2
- FWCI
- 0.84
- Type
- journal article
- Language
- en
- Open access
- bronze
- doi.org
- Licence
- www.elsevier.com/tdm/userlicense/1.0/ (tdm)
- www.elsevier.com/legal/tdmrep-license (tdm)
- www.elsevier.com/open-access/userlicense/1.0/ (am, 684 d)
- doi.org/10.15223/policy-017 (stm-asf)
- doi.org/10.15223/policy-037 (stm-asf)
- doi.org/10.15223/policy-012 (stm-asf)
- doi.org/10.15223/policy-029 (stm-asf)
- doi.org/10.15223/policy-004 (stm-asf)
- Locations
- Composites Communications (acceptedVersion)
- Topics
- Physical Sciences › Engineering › Biomedical Engineering › Bone Tissue Engineering Materials
- Physical Sciences › Engineering › Mechanical Engineering › Cellular and Composite Structures
- Physical Sciences › Materials Science › Ceramics and Composites › Advanced ceramic materials synthesis
- Keywords
- hydroxyapatite, poly(L-lactic acid), PLCL, freeze-drying, template method, three-point bending, flexural properties, fracture behavior, crack initiation and propagation, microdamage, fracture energy, modulus, fracture strength, biopolymer composites
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Bibliographic data: Semantic Scholar, OpenAlex, Crossref.
Contains information from the Semantic Scholar Academic Graph Datasets, made available under the ODC Attribution License (ODC-BY 1.0).
Semantic Scholar’s data is described in: Kinney, R., et al. (2023). The Semantic Scholar Open Data Platform. arXiv:2301.10140.