Solid phase extraction of metal ions in environmental samples on 1-(2-pyridylazo)-2-naphthol impregnated activated carbon cloth

Alothman, Zeid A.; Yilmaz, Erkan; Habila, Mohamed; Soylak, Mustafa

doi:10.1016/j.ecoenv.2014.10.032

Cited by 74Analytical chemistry methods developmentAdsorption and biosorption for pollutant removalEnvironmental and Analytical Chemistry Studies

Solid phase extraction of metal ions in environmental samples on 1-(2-pyridylazo)-2-naphthol impregnated activated carbon cloth

Alothman, Zeid A., Yilmaz, Erkan, Habila, Mohamed, Soylak, Mustafa·2015·Ecotoxicology and Environmental Safety

DOI 10.1016/j.ecoenv.2014.10.032

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Abstract

1-(2-Pyridylazo)-2-naphthol impregnated activated carbon cloth (PAN-imp-ACC) was prepared as a solid phase sorbent and, for the first time, was used for the simultaneous separation and preconcentration of trace amounts of lead, cadmium and nickel in water, soil and sewage sludge samples prior to determination by flame atomic absorption spectrometry (FAAS). The parameters governing the efficiency of the method were optimized, including the pH, the eluent type and volume, the sample and eluent flow rates, diverse ions effects and the sample volume. A preconcentration factor of 100 was achieved for all the metal ions, with detection limits of 0.1-2.8 µg L(-1) and relative standard deviations below 6.3%. The adsorption capacity of the PAN-imp-ACC for Pb(II), Cd(II) and Ni(II) ions was found to be 45.0 mg g(-1), 45.0 mg g(-1) and 43.2 mg g(-1), respectively. The method was validated by the analysis of the certified reference materials TMDA-64.2 fortified Lake Ontario water and BCR-146R Sewage Sludge Amended Soil (Industrial Origin). The procedure was applied to determine the analytes content in real samples.

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“The limits of detection of 0.008 µg L−1 for the developed DES-ME were between those of the other methods, as shown in Table 5.”
From Deep Eutectic Solvent-Based Microextraction of Lead(II) Traces from Water and Aqueous Extracts before FAAS Measurements (2020) · cites this paper as [21]

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Authors: Alothman, Z. A., Yilmaz, E., Habila, M., & Soylak, M.
Affiliations: King Saud University (SA)
Erciyes University (TR)
Corresponding author: Soylak, Mustafa
ORCID: Alothman, Zeid A.
Habila, Mohamed
Soylak, Mustafa
Venue: Ecotoxicology and Environmental Safety
Publisher: Elsevier BV
Published: 2015-02
Volume: 112
Pages: 74-79
ISSN: 0147-6513 (ISSN-L)
DOI: 10.1016/j.ecoenv.2014.10.032
OpenAlex: W2074867218
Cited by: 74
References: 46
Citations by year: 2026: 2 · 2025: 1 · 2024: 1 · 2023: 3 · 2022: 10 · 2021: 7 · 2020: 7 · 2019: 7 · 2018: 8 · 2017: 5 · 2016: 8 · 2015: 14 · 2013: 1
FWCI: 8.05
Type: journal article
Language: en
Open access: closed
Licence: www.elsevier.com/tdm/userlicense/1.0/ (tdm)
Locations: Ecotoxicology and Environmental Safety (publishedVersion)
PubMed (publishedVersion)
Topics: Physical Sciences › Chemistry › Analytical Chemistry › Analytical chemistry methods development
Physical Sciences › Environmental Science › Water Science and Technology › Adsorption and biosorption for pollutant removal
Physical Sciences › Environmental Science › Water Science and Technology › Environmental and Analytical Chemistry Studies
Keywords: solid-phase extraction, 1-(2-pyridylazo)-2-naphthol, activated carbon cloth, metal ion preconcentration, lead, cadmium, nickel, heavy metal adsorption, sewage sludge, soil sample, water samples, trace metal analysis, flame atomic absorption spectrometry
MeSH terms: Adsorption, Cadmium, Carbon, Environmental Monitoring, Ions, Lead, Metals, Naphthols, Nickel, Ontario, Soil Pollutants, Spectrophotometry, Atomic, Water Pollutants, Chemical, Solid Phase Extraction

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Solid phase extraction of metal ions in environmental samples on 1-(2-pyridylazo)-2-naphthol impregnated activated carbon cloth

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